JPS6041537A - Apparatus for removing automatically deposited product - Google Patents

Apparatus for removing automatically deposited product

Info

Publication number
JPS6041537A
JPS6041537A JP15008683A JP15008683A JPS6041537A JP S6041537 A JPS6041537 A JP S6041537A JP 15008683 A JP15008683 A JP 15008683A JP 15008683 A JP15008683 A JP 15008683A JP S6041537 A JPS6041537 A JP S6041537A
Authority
JP
Japan
Prior art keywords
reaction
discharge passage
resilient body
product
inside wall
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP15008683A
Other languages
Japanese (ja)
Inventor
Masanobu Yoshida
吉田 公信
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Electric Industries Ltd
Original Assignee
Sumitomo Electric Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Electric Industries Ltd filed Critical Sumitomo Electric Industries Ltd
Priority to JP15008683A priority Critical patent/JPS6041537A/en
Publication of JPS6041537A publication Critical patent/JPS6041537A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/002Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/012Manufacture of preforms for drawing fibres or filaments
    • C03B37/014Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
    • C03B37/0144Means for after-treatment or catching of worked reactant gases

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Cleaning In General (AREA)
  • Glass Melting And Manufacturing (AREA)
  • Manufacture, Treatment Of Glass Fibers (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

PURPOSE:To strip off and remove easily excessive product of reaction deposited to inside wall of discharge passage by providing a coil shaped resilient body to the inside wall of a discharge passage for discharging excessive product of the reaction from a reaction vessel and twisting the resilent body and returning quickly to the original state. CONSTITUTION:A seed bar 3 is suspended in a reaction vessel 1 and gaseous raw material for glass is ejected from an oxyhydrogen burner 2 at the bottom of the reaction vessel 1 to cause deposition of base material 4 for optical fiber by flame hydrolytic reaction to the top of the seed bar 3. In this case, excessive reaction product is cooled quickly when it is discharged through a discharge passage 5 of the vessel 1 and deposits and accumulates on the inside wall of the discharge passage 5 to make the passage 5 narrow and cause clogging of the passage finally. A coil shaped resilient body 13 is fitted to the inside wall of the discharge pipe 11 of the excessive product and an end of the resilient body is fixed to a rotatable ring 14 and the other end is fixed to a friction ring 12. By the revolution of a roller 16 by the driving of a motor 15, the rotatable ring 14 contacting with the roller is revolved and the resilient body 13 is twisted, but the resilient body restores its original shape quickly by the rotation of the friction ring 12. Deposited product is stripped off by the vibration in this stage, and recovered easily.

Description

【発明の詳細な説明】 が排気路に付着堆積するのを防止する堆積物自動除去装
置δに関干る。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to an automatic deposit removal device δ that prevents deposits from being deposited in an exhaust passage.

反応容器内に反応に必要な原料並びに反応媒体を供給し
所定の反応物を得る際には、反応余剰物を生じるため、
この反応余剰物等全圧送,吸引あるいけ自然流動にて排
気するための排出路が一般に設けられている。このよう
な反応容器としてVAD法により光フアイバ母材を製造
する反応装置を第1図に示す。同図に示されるように反
応容器i内にはシード棒3が垂直に吊り下げられ、該シ
ード棒3に対向して酸水素炎バーナ2がその底面に設置
されている。この酸水素炎バーナ2からガラス原料等を
噴出させてこれらを火炎加水分解反応させ、生成したガ
ラス微粒子をシード棒3に付着堆積させ、同時にシード
棒3を引き上げて多孔質母材4金製造している。この時
,ガラス原料。
When supplying the raw materials and reaction medium necessary for the reaction into the reaction vessel to obtain the desired reactant, a reaction surplus is generated.
Generally, a discharge passage is provided for exhausting the reaction surplus by pressure, suction, or natural flow. As such a reaction vessel, a reaction apparatus for producing an optical fiber preform by the VAD method is shown in FIG. As shown in the figure, a seed rod 3 is suspended vertically within the reaction vessel i, and an oxyhydrogen flame burner 2 is installed on the bottom face of the seed rod 3, facing the seed rod 3. Glass raw materials, etc. are ejected from this oxyhydrogen flame burner 2 to cause a flame hydrolysis reaction, and the generated glass particles are deposited on the seed rod 3. At the same time, the seed rod 3 is pulled up to produce a porous base material of 4 gold. ing. At this time, glass raw material.

ガラス微粒子等は全て反応に参加し、シード棒3に付着
堆積するとは限らず、これらの残部を反応余剰物として
排出するための排出路5が反応容器1に接続されている
。この排出路5は図示省略の余剰物 処理装置に接続さ
れており、大半の反応余剰物はこの排出路5を通じて余
剰物処理装置に吸引されることとなる。しかし、火炎加
水分解反応直後の反応余剰物は微細かつ高温でめるため
胡出路5内部を通過する際に冷却され、排出路5の内壁
に徐々に付着堆積し、ついには排七路5の閉塞に到るこ
とすらある。VAD法による光フアイバ母材の製造方法
において特に重要なことは、酸水素炎バーナ2とシード
棒3に至るまでの空間内のガラス微粒子の分布が所定の
屈折率分布が得られるように形成され、このガラス微粒
子の分布が所定の時間変動せずに維持されることである
。しかし、上述のように排出路5に反応余剰物が堆積物
6として付着堆積して排出路5の径が狭まシ、排出路5
が閉塞すると、反応余剰物の排出量等が変化し、ガラス
微粒子の分布を上記のように維持することができず所定
の屈折率分布を得ることが困難となるばかりでなく、V
AD法の特長である連続製造を不可能としている。
All of the glass particles participate in the reaction and do not necessarily adhere to and accumulate on the seed rod 3, and a discharge path 5 is connected to the reaction vessel 1 to discharge the remainder as a reaction surplus. This discharge path 5 is connected to a surplus treatment device (not shown), and most of the reaction surplus is sucked into the surplus treatment device through this discharge path 5. However, since the reaction surplus immediately after the flame hydrolysis reaction is fine and solidified at a high temperature, it is cooled while passing through the inside of the discharge passage 5, gradually adheres and accumulates on the inner wall of the discharge passage 5, and finally ends up in the discharge passage 5. It may even lead to blockage. What is particularly important in the method for producing an optical fiber base material by the VAD method is that the distribution of glass particles in the space between the oxyhydrogen flame burner 2 and the seed rod 3 is formed so that a predetermined refractive index distribution is obtained. , the distribution of the glass particles is maintained without fluctuation for a predetermined period of time. However, as described above, the reaction surplus adheres and accumulates in the discharge passage 5 as deposits 6, and the diameter of the discharge passage 5 becomes narrow.
If the V
This makes continuous production, which is a feature of the AD method, impossible.

このように従来のVAD法による光フアイバ母材の反応
装置では、排出路5に反応余剰物が付着堆積するため、
反応容器内の反応条件を一定に維持できず、所定の屈折
率分布を有する光フアイバ母材を連続して製造すること
ができなかった。
In this way, in the conventional VAD-based optical fiber base material reaction device, reaction surplus adheres and accumulates in the discharge path 5.
It was not possible to maintain the reaction conditions in the reaction vessel constant, and it was not possible to continuously produce an optical fiber preform having a predetermined refractive index distribution.

本発明は、上記実情に鑑み、排出路に反応余剰物が付着
堆積するの全防止し、反応容器内の反応条件を一定に維
持することを目的とする。斯かる目的を達成する本発明
の構成は反応容器から反応余剰物を排気する排出路にお
いて、該排出路の内壁に沿って弾性体が装着されると共
に該弾性体を捩った後急激に元の状態に回復させる振動
機構が設けられ、該弾性体から前記反応余剰物の堆積物
を剥離させることを特徴とする。
In view of the above circumstances, it is an object of the present invention to completely prevent reaction surpluses from adhering and accumulating in the discharge channel, and to maintain constant reaction conditions within the reaction vessel. The structure of the present invention that achieves such an object is that an elastic body is installed along the inner wall of the discharge passage for exhausting the reaction surplus from the reaction vessel, and after the elastic body is twisted, it suddenly returns to its original state. The present invention is characterized in that a vibration mechanism is provided to restore the state to the above state, and the deposits of the reaction surplus are peeled off from the elastic body.

以下、本発明の堆積物自動除去装置を実施例に基づいて
詳細に説明する。
EMBODIMENT OF THE INVENTION Hereinafter, the automatic deposit removal device of the present invention will be described in detail based on examples.

第2図に本発明の一実施例を示す。同図に示すように、
反応容器(図示省略)に排出路として接続する排気管1
1の内壁に沿ってコイル状の弾性体13が装着さ九てい
る。更に、このコイル状の弾性体13を捩った復元の状
態に回復させる振動機構が設けられている。即ち、該排
気管11の一端内周には該弾性体13の一端と摩擦接触
する摩擦リング12が嵌着され、摩擦抵抗以下のトルク
に対しては該弾性体13の一端は摩擦リング12に固定
されることとなる。一方、排気管11 、11’の間に
は回転リング14が回転自在に介装されると共にこの回
転リング14にコイル状の弾性体13の他端が固定され
ている。この回転リング14はモータ15に直結したロ
ーラ16と摩擦接触している。従って、該モータ15を
駆動しローラ16を介して回転リング14を回転させル
ば、コイル状の弾性体13が次第に捩れることとなる。
FIG. 2 shows an embodiment of the present invention. As shown in the figure,
Exhaust pipe 1 connected to the reaction vessel (not shown) as a discharge path
A coil-shaped elastic body 13 is attached along the inner wall of 1. Further, a vibration mechanism is provided for restoring the coiled elastic body 13 to its twisted state. That is, a friction ring 12 that comes into frictional contact with one end of the elastic body 13 is fitted on the inner periphery of one end of the exhaust pipe 11, and one end of the elastic body 13 contacts the friction ring 12 when the torque is less than the frictional resistance. It will be fixed. On the other hand, a rotary ring 14 is rotatably interposed between the exhaust pipes 11 and 11', and the other end of a coiled elastic body 13 is fixed to the rotary ring 14. This rotating ring 14 is in frictional contact with a roller 16 directly connected to a motor 15. Therefore, if the motor 15 is driven to rotate the rotary ring 14 via the rollers 16, the coiled elastic body 13 will be gradually twisted.

しかも、回転リング14の回転を更に進めると、該弾性
体13に加わるトルクが該弾性体13の一端と摩擦リン
グ12との間の摩擦抵抗を越え、これらの間で滑りを起
こし、急激にコイル状の弾性体13が元の状態に回復す
ることとなる。−尚、図面中、11′は排気管11と余
剰物処理装置(図示省略)とを連通ずる排気管でるる。
Moreover, as the rotating ring 14 further rotates, the torque applied to the elastic body 13 exceeds the frictional resistance between one end of the elastic body 13 and the friction ring 12, causing slippage between them, causing the coil to suddenly The shaped elastic body 13 will recover to its original state. - In the drawing, reference numeral 11' indicates an exhaust pipe that communicates the exhaust pipe 11 with a surplus processing device (not shown).

上記構成を有する本発明の堆積物自動除去装置において
は、排気管11 、11’を通じて反応装置力≧ら余剰
物処理装置に反応余剰物を吸気する際、反応余剰物はコ
イル状の弾性体13に付着し堆積する。このとき、回転
リング14を回転させてコイル状の弾性体13を捩れば
、堆積面が歪むこととなり、堆積物は該弾性体13さら
剥離もしくは剥離し易い状態となる。更に、回転リング
14の回転を進めると、該弾性体13は歪を放出して急
激に元の状態に回復し、この時堆積物は完全に該弾性体
13から剥離することとなる。この剥離した堆積物は吸
気にて除去され、余剰物処理装置にて処理されることと
なる。このため、排気量等の排気条件が時間的に変化す
ることなく、反応容器内の反応条件を一定に維持するこ
とができる。尚、上記実施例では弾性体13としてコイ
ル状のものを使用していたが、本発明ではコイル状のも
のに限らず円筒状の弾性体でも同様に使用でき、上記と
同様の作用効果を奏する。
In the automatic deposit removal device of the present invention having the above configuration, when the reaction surplus is sucked into the surplus processing device through the exhaust pipes 11 and 11' from the reaction device force≧, the reaction surplus is removed from the coiled elastic body 13. It adheres to and accumulates on the surface. At this time, if the rotating ring 14 is rotated to twist the coil-shaped elastic body 13, the deposition surface will be distorted, and the deposit will be in a state where the elastic body 13 is easily peeled off or peeled off. Further, as the rotating ring 14 continues to rotate, the elastic body 13 releases the strain and rapidly recovers to its original state, and at this time, the deposits are completely peeled off from the elastic body 13. This peeled deposit is removed by suction air and processed by a surplus processing device. Therefore, the reaction conditions in the reaction vessel can be maintained constant without the evacuation conditions such as the amount of evacuation changing over time. In the above embodiment, a coil-shaped elastic body is used as the elastic body 13, but in the present invention, not only a coil-shaped elastic body but also a cylindrical elastic body can be used in the same manner, and the same effect as described above can be achieved. .

以上、実施例に基づいて具体的に説明したように本発明
では排出路の内壁に沿って弾性体を装着し、該弾性体の
急激なねじり回復を利用して該弾性体から堆積物を剥離
させるようにしたので、排出路に対する反応余剰物の付
着堆積を防止することができる。このため、排気量等の
排気条件が変化することもなく、反応容器内の反応条件
を一定に維持できるようになった。特に、本発明をVA
D法による光フアイバ母材の反応容器に適用した場合に
は、排気条件が不変なため、酸水素炎パーナからシード
棒に至るまでの空間のガラス微粒子の分布を時間変動さ
せずに一定に維持でき、所定の屈折率分布を有する光フ
アイバ母材を連続して製造することが可能となる。
As described above in detail based on the embodiments, in the present invention, an elastic body is attached along the inner wall of the discharge passage, and deposits are peeled off from the elastic body by utilizing rapid torsional recovery of the elastic body. Therefore, it is possible to prevent the reaction surplus from adhering to and depositing on the discharge path. Therefore, the reaction conditions in the reaction vessel can now be maintained constant without changing the exhaust conditions such as the exhaust amount. In particular, the present invention
When applied to a reaction vessel with an optical fiber base material using the D method, the exhaust conditions remain unchanged, so the distribution of glass particles in the space from the oxyhydrogen flame parner to the seed rod can be maintained constant without changing over time. This makes it possible to continuously manufacture optical fiber preforms having a predetermined refractive index distribution.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図はVAD法による光フアイバ母材の反応装置の概
略構造図、第2図は本発明の堆積物自動除去装置の一実
施例の断面図である。 図 而 中、 11.11’は排気管 12は摩擦リング 13はコイル状の弾性体 14は回転リング 15はモータ 16はローラである。 特許出願 人 住友電気工業株式会社 代理人 弁理士 光石士部(他1名)
FIG. 1 is a schematic structural diagram of a reactor for reacting an optical fiber base material using the VAD method, and FIG. 2 is a sectional view of an embodiment of the automatic deposit removal device of the present invention. In the figure, 11.11' is an exhaust pipe 12, a friction ring 13, a coiled elastic body 14, a rotating ring 15, and a motor 16 is a roller. Patent applicant: Sumitomo Electric Industries, Ltd. agent Patent attorney: Shibu Mitsuishi (1 other person)

Claims (1)

【特許請求の範囲】[Claims] 反応容器から反応余剰物を排気する排出路において、該
排出路の内壁に沿って弾性体が装着されると共に該弾性
体を捩った後急激に元の状態に回復させる振動機構が設
けられ、該弾性体から前記反応余剰物のj#!積物を剥
離させることを特徴とする堆積物自動除去装置。
An elastic body is installed along the inner wall of the discharge passage for exhausting reaction surplus from the reaction vessel, and a vibration mechanism is provided to twist the elastic body and then rapidly restore it to its original state, j# of the reaction surplus from the elastic body! An automatic deposit removal device characterized by peeling off deposits.
JP15008683A 1983-08-16 1983-08-16 Apparatus for removing automatically deposited product Pending JPS6041537A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP15008683A JPS6041537A (en) 1983-08-16 1983-08-16 Apparatus for removing automatically deposited product

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP15008683A JPS6041537A (en) 1983-08-16 1983-08-16 Apparatus for removing automatically deposited product

Publications (1)

Publication Number Publication Date
JPS6041537A true JPS6041537A (en) 1985-03-05

Family

ID=15489203

Family Applications (1)

Application Number Title Priority Date Filing Date
JP15008683A Pending JPS6041537A (en) 1983-08-16 1983-08-16 Apparatus for removing automatically deposited product

Country Status (1)

Country Link
JP (1) JPS6041537A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60246232A (en) * 1984-05-18 1985-12-05 Nippon Sheet Glass Co Ltd Manufacture of optical fiber preform
EP0845442A1 (en) * 1996-12-02 1998-06-03 Alcatel Apparatus for manufacturing an optical fibre preform
CN108356055A (en) * 2018-02-11 2018-08-03 深圳市联铭发科技有限公司 The recovery method of cover sheet

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS60246232A (en) * 1984-05-18 1985-12-05 Nippon Sheet Glass Co Ltd Manufacture of optical fiber preform
EP0845442A1 (en) * 1996-12-02 1998-06-03 Alcatel Apparatus for manufacturing an optical fibre preform
FR2756556A1 (en) * 1996-12-02 1998-06-05 Alsthom Cge Alcatel INSTALLATION FOR MANUFACTURING AN OPTICAL FIBER PREFORM
CN108356055A (en) * 2018-02-11 2018-08-03 深圳市联铭发科技有限公司 The recovery method of cover sheet

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