JPS60237032A - アリルアルコ−ルの精製方法 - Google Patents
アリルアルコ−ルの精製方法Info
- Publication number
- JPS60237032A JPS60237032A JP9175684A JP9175684A JPS60237032A JP S60237032 A JPS60237032 A JP S60237032A JP 9175684 A JP9175684 A JP 9175684A JP 9175684 A JP9175684 A JP 9175684A JP S60237032 A JPS60237032 A JP S60237032A
- Authority
- JP
- Japan
- Prior art keywords
- water
- column
- allyl alcohol
- allyl
- composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 title claims abstract description 58
- 238000000746 purification Methods 0.000 title description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 43
- 239000000203 mixture Substances 0.000 claims abstract description 38
- 239000012071 phase Substances 0.000 claims abstract description 36
- HVAMZGADVCBITI-UHFFFAOYSA-M pent-4-enoate Chemical compound [O-]C(=O)CCC=C HVAMZGADVCBITI-UHFFFAOYSA-M 0.000 claims abstract description 16
- 238000010992 reflux Methods 0.000 claims abstract description 15
- 238000004821 distillation Methods 0.000 claims abstract description 10
- 238000010586 diagram Methods 0.000 claims abstract description 4
- 239000007791 liquid phase Substances 0.000 claims abstract description 4
- 238000000034 method Methods 0.000 claims description 10
- 239000002023 wood Substances 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 abstract 2
- OMOVVBIIQSXZSZ-UHFFFAOYSA-N [6-(4-acetyloxy-5,9a-dimethyl-2,7-dioxo-4,5a,6,9-tetrahydro-3h-pyrano[3,4-b]oxepin-5-yl)-5-formyloxy-3-(furan-3-yl)-3a-methyl-7-methylidene-1a,2,3,4,5,6-hexahydroindeno[1,7a-b]oxiren-4-yl] 2-hydroxy-3-methylpentanoate Chemical compound CC12C(OC(=O)C(O)C(C)CC)C(OC=O)C(C3(C)C(CC(=O)OC4(C)COC(=O)CC43)OC(C)=O)C(=C)C32OC3CC1C=1C=COC=1 OMOVVBIIQSXZSZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000007788 liquid Substances 0.000 description 8
- 238000000605 extraction Methods 0.000 description 6
- 239000002994 raw material Substances 0.000 description 6
- 238000009835 boiling Methods 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 239000008346 aqueous phase Substances 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 230000018044 dehydration Effects 0.000 description 3
- 238000006297 dehydration reaction Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 229910002056 binary alloy Inorganic materials 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9175684A JPS60237032A (ja) | 1984-05-10 | 1984-05-10 | アリルアルコ−ルの精製方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP9175684A JPS60237032A (ja) | 1984-05-10 | 1984-05-10 | アリルアルコ−ルの精製方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS60237032A true JPS60237032A (ja) | 1985-11-25 |
| JPS6328415B2 JPS6328415B2 (enrdf_load_stackoverflow) | 1988-06-08 |
Family
ID=14035380
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP9175684A Granted JPS60237032A (ja) | 1984-05-10 | 1984-05-10 | アリルアルコ−ルの精製方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS60237032A (enrdf_load_stackoverflow) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08268938A (ja) * | 1995-03-29 | 1996-10-15 | Osaka Organic Chem Ind Ltd | アクリル酸メチルまたはメタクリル酸メチルとメタノールの分離方法 |
| JP2007231011A (ja) * | 2006-02-02 | 2007-09-13 | Showa Denko Kk | 共沸蒸留方法 |
| WO2007089036A3 (en) * | 2006-02-02 | 2007-10-18 | Showa Denko Kk | Azeotropic distillation method |
| US9150473B2 (en) | 2013-06-05 | 2015-10-06 | Dairen Chemical Corporation | Method for producing allyl alcohol |
| CN107501047A (zh) * | 2017-09-07 | 2017-12-22 | 太原理工大学 | 一种制备高纯度丙烯醇的方法 |
| CN107698428A (zh) * | 2017-09-27 | 2018-02-16 | 湖北绿色家园材料技术股份有限公司 | 一种分离烯丙醇中水分的方法 |
| JP2018531928A (ja) * | 2015-10-14 | 2018-11-01 | ダウ グローバル テクノロジーズ エルエルシー | メチルメタクリレートの精製のためのプロセス |
-
1984
- 1984-05-10 JP JP9175684A patent/JPS60237032A/ja active Granted
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08268938A (ja) * | 1995-03-29 | 1996-10-15 | Osaka Organic Chem Ind Ltd | アクリル酸メチルまたはメタクリル酸メチルとメタノールの分離方法 |
| JP2007231011A (ja) * | 2006-02-02 | 2007-09-13 | Showa Denko Kk | 共沸蒸留方法 |
| WO2007089036A3 (en) * | 2006-02-02 | 2007-10-18 | Showa Denko Kk | Azeotropic distillation method |
| US8083903B2 (en) | 2006-02-02 | 2011-12-27 | Showa Denko K.K. | Process for producing allyl alcohol |
| US9150473B2 (en) | 2013-06-05 | 2015-10-06 | Dairen Chemical Corporation | Method for producing allyl alcohol |
| JP2018531928A (ja) * | 2015-10-14 | 2018-11-01 | ダウ グローバル テクノロジーズ エルエルシー | メチルメタクリレートの精製のためのプロセス |
| CN107501047A (zh) * | 2017-09-07 | 2017-12-22 | 太原理工大学 | 一种制备高纯度丙烯醇的方法 |
| CN107698428A (zh) * | 2017-09-27 | 2018-02-16 | 湖北绿色家园材料技术股份有限公司 | 一种分离烯丙醇中水分的方法 |
| CN107698428B (zh) * | 2017-09-27 | 2022-09-20 | 湖北绿色家园材料技术股份有限公司 | 一种分离烯丙醇中水分的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6328415B2 (enrdf_load_stackoverflow) | 1988-06-08 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |