JPS60183107A - Manufacture of light-weight material - Google Patents

Manufacture of light-weight material

Info

Publication number
JPS60183107A
JPS60183107A JP2079185A JP2079185A JPS60183107A JP S60183107 A JPS60183107 A JP S60183107A JP 2079185 A JP2079185 A JP 2079185A JP 2079185 A JP2079185 A JP 2079185A JP S60183107 A JPS60183107 A JP S60183107A
Authority
JP
Japan
Prior art keywords
resin
class
micro
spheres
fluid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2079185A
Other languages
Japanese (ja)
Inventor
ハンスヨヒム、ブルガー
フーベルト、シユスター
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Siemens Schuckertwerke AG
Siemens AG
Original Assignee
Siemens Schuckertwerke AG
Siemens AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Siemens Schuckertwerke AG, Siemens AG filed Critical Siemens Schuckertwerke AG
Publication of JPS60183107A publication Critical patent/JPS60183107A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C39/00Shaping by casting, i.e. introducing the moulding material into a mould or between confining surfaces without significant moulding pressure; Apparatus therefor
    • B29C39/02Shaping by casting, i.e. introducing the moulding material into a mould or between confining surfaces without significant moulding pressure; Apparatus therefor for making articles of definite length, i.e. discrete articles
    • B29C39/04Shaping by casting, i.e. introducing the moulding material into a mould or between confining surfaces without significant moulding pressure; Apparatus therefor for making articles of definite length, i.e. discrete articles using movable moulds not applied
    • B29C39/08Introducing the material into the mould by centrifugal force
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/58Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising fillers only, e.g. particles, powder, beads, flakes, spheres
    • B29C70/66Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising fillers only, e.g. particles, powder, beads, flakes, spheres the filler comprising hollow constituents, e.g. syntactic foam
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29KINDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2063/00Use of EP, i.e. epoxy resins or derivatives thereof, as moulding material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29KINDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2105/00Condition, form or state of moulded material or of the material to be shaped
    • B29K2105/0076Microcapsules
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29KINDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2105/00Condition, form or state of moulded material or of the material to be shaped
    • B29K2105/04Condition, form or state of moulded material or of the material to be shaped cellular or porous
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29KINDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2105/00Condition, form or state of moulded material or of the material to be shaped
    • B29K2105/06Condition, form or state of moulded material or of the material to be shaped containing reinforcements, fillers or inserts
    • B29K2105/16Fillers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29KINDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2105/00Condition, form or state of moulded material or of the material to be shaped
    • B29K2105/06Condition, form or state of moulded material or of the material to be shaped containing reinforcements, fillers or inserts
    • B29K2105/16Fillers
    • B29K2105/165Hollow fillers, e.g. microballoons or expanded particles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29KINDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR MOULDS, REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS
    • B29K2709/00Use of inorganic materials not provided for in groups B29K2703/00 - B29K2707/00, for preformed parts, e.g. for inserts
    • B29K2709/08Glass

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Composite Materials (AREA)
  • Mechanical Engineering (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)

Abstract

The invention relates to a process for producing a lightweight material, in particular for use as matching layer material in ultrasonic transducers. The lightweight material consists of a lightweight filling material, preferably hollow glass micro beads (microballoons), which is bound by means of resins, preferably epoxy or polyester resins. To this end the filling material is introduced into a centrifuge and covered by the low viscosity resin. It is especially advantageous to apply to the glass beads a filter material which is pressed by a weight onto the glass beads and through which the low viscosity resin can be filtered, so that no contaminants in the resin can penetrate between the glass beads.

Description

【発明の詳細な説明】 11¥:蕉」、の団ノ1j分1Ilf 1本発明5J、
IQ1脂7j J:り結きされる軽率な充填H本1から
成る一1ifnf i、l拐の棟1貨方去V(四する。
[Detailed description of the invention] 11 yen: Shō”, Group No. 1j 1 Ilf 1 Present invention 5J,
IQ1 fat 7j J: A careless filling H book 1 made of 1ifnfi, 1 piece left V (4 pieces).

[従来の技lドj1 ・時にたとえば超イ波範囲内の高度の要求条件が課せら
t+、ル応ill vc h) (、−(は、高い強度
、約0.5に9 / (:m3の低い密度、均質な組織
、良好な水密性、良好な1制熱性および高い溶剤1ij
j性を有する舒計何1”lが必要とされる。中空球の低
い見掛C・す密度は条件トjきでのみ攪11ミ器内での
・胴脂との箱師を許す。
[Conventional technique l de j1 ・Sometimes, for example, altitude requirements in the ultraviolet range are imposed t+, le ill vch) (, -( is high intensity, about 0.5 to 9 / (: m3 low density, homogeneous structure, good watertightness, good heat resistance and high solvent resistance
A diameter of 1"l having a certain property is required. The low apparent density of the hollow sphere allows for mixing with body fat in a stirrer only under certain conditions.

IF) I′I’ 優程での真空のL7・(、川も中空
球の間の空気の駆逐の際に望ましい結果をもたらさない
IF) I'I' Vacuum L7.

「発明が厘「決しようとする問題点J 本発明の目的はに記の問題点を解決することである。``The problem that invention is trying to solve'' The purpose of the present invention is to solve the problems mentioned below.

〔問題点を解決するための手段1 この目的は、本発明によれば、充j+Q il′A’ 
F)が遠心分離機1’i i/ζ導入され、また流動性
の樹脂trcx、りおおわれ、またその後に両要素が混
合に至るまで、また場合によっては硬化に至るまで遠心
分離機にかけられることにより達成される。」−記の必
映とされる特性は、充填・目r゛)の導入後にフィルタ
材料およびおもりが相次いで光填rA科の上に載すられ
、また訃もりの」二に流動性の樹j指が遠心分ばtの前
て載せられ、−まだおもりが館脂に利する)li孔を有
するならば、一層間々fに・構成される。その際、充填
・i’A’ f’lとしてマイクロ中空球か、特にガラ
ス中空球が用いられることは有利である。流動性のツ!
1脂としてエボキ7ドまたはポリエステル樹脂1脂が用
いられることは特に望ましい。
[Means for solving the problem 1 According to the present invention, this purpose is to satisfy j+Q il'A'
F) is introduced into the centrifuge 1'i i/ζ and covered with the free-flowing resin trcx, and then both elements are centrifuged until mixing and possibly hardening. This is achieved by The essential characteristic of this is that after the introduction of the filling material and the weight, the filter material and the weight are successively placed on top of the light filling material, and that the fluidity of the material is If the finger j is placed in front of the centrifugal part t and has a li hole (the weight still serves the fat), it will be more closely configured to f. In this case, it is advantageous if micro-hollow spheres or, in particular, glass hollow spheres are used as the filling material. The point of liquidity!
It is particularly desirable to use epoxy resin or polyester resin as the resin.

前記の問題点をノずt決するだめの他の方法でりす、マ
イクロ中空ガラス球が細粉化された反応呻叱明n旨と箱
外され、型のなかに満たされ、軽度におもしをのせられ
また好ましくVi紹冴彼により硬化され、またそのすぐ
後(で流動性の反Lb樹脂で満たされ、この反応樹J指
がi:i’Yし)て硬化する。、この場合にも反応硬化
樹脂としてエポキシドまだはポリエステル樹脂を使J1
1fることは有「りである。寸だ充填されていない多孔
性の焼、情体はこの場1年約092ないL (1,37
・’ (7ff3の密度を刊する。水密性および強度を
高めるlζめの流動(〆I:の反応明脂の充填は補助手
段なしにR,空Vこより、または遠心外部((よっても
行なわF′L得る1、たいていの場合には、流動性の樹
脂を焼結体の上にたらぜば十分である。硬化は室幅また
はそれ以上に高められた温度で行なわへ得る。仕上り祠
引の密度は好ましくは約05ないし0.67 / nn
:(である。fI!比された材料は充填前(lこ型から
鷹出され得る。しかし、それは型のなかでも充填されイ
0も。いずれの場合にも、ポリメグ−ルペノテンから+
)y、る型の;史用シ・ま、離型剤なしでの濶を型が+
jJ能である点で有4′11である。軽駐桐材の製造l
・まピエゾセラミクスなどのようなトy合部分上の接着
によっても同時に行なわれ得る。軽は何11が色を有す
るものとして製造されるべきであれば、流動性の含浸樹
脂が着色され得る1、 〔実施I+lIJ 図面により本方法を一層詳細に説明する、。
In order to solve the above problems, in another method, the micro hollow glass spheres are pulverized, removed from the box, filled into a mold, and lightly sprinkled. It is also preferably cured by Vishaohe, and immediately thereafter (filled with a flowable anti-Lb resin, this reaction tree is i:i'Y) and cured. In this case as well, epoxide or polyester resin is used as the reaction curing resin.
It is possible that 1f will occur.The porous pottery, which has not been completely filled, has been in this place for about 092 years (1,37
・' (Publishes a density of 7ff3. Filling with reaction resin of lζ to increase watertightness and strength (〆I: can be carried out without any auxiliary means by R, empty V, or centrifugal external ((F) In most cases, it is sufficient to pour the fluid resin onto the sintered body.Curing is carried out at an elevated temperature of chamber width or higher. The density is preferably about 0.05 to 0.67/nn
:(.fI! The compared material can be ejected from the mold before filling. However, it can also be filled in the mold. In either case, +
) y, mold's; historic use, ma, mold without mold release agent
It is 4'11 in that it is jJ ability. Manufacture of light paulownia wood
- At the same time, it can also be carried out by adhesion on a joint part such as piezoceramics. If the light material is to be produced as having a color, the flowable impregnated resin can be colored.

図面には、遠心分離機内にたとえば個1線2のまわりに
回転’=J能に支えらILでいる容器1が示されている
。容2;1は底3を有する中空円筒とし−〔構成されて
いる。先ずこの容器内にマイクロ・ガラス中空球4が充
填され、これらのガラス中空球が伜としてたとえば焼結
されたフェロゲラストパウダーから成るフィルタ材料の
1全5でZ−S−われる。
The drawing shows a container 1 which is supported in a centrifuge, for example around a single line 2, with a rotation '=J function. The container 2; 1 is constructed as a hollow cylinder with a bottom 3. The container is first filled with micro glass hollow spheres 4 which are then coated with a filter material 5 consisting of, for example, sintered ferrogellast powder.

このフィルタ祠ぜ1の上におもり6がgすられる。A weight 6 is placed on top of this filter bowl 1.

このひもりは容器1の全横断面を満たしてふ・らず、ま
た場合によっては追加的に貝dll・I’L7を有し、
これらの貫通孔を、その後に注入される流動性の樹脂8
が通過しイiる。いま容器1が回転させられると、遠心
力の作用によりフィルタ1全5がさらにガラス球の上に
押され、樹脂がフィルタ栓を通過して、ガラス中空球の
!d1の空所を満たす。II!J!量材料の硬化ばlす
]転の間にまたは適当な[E縮の後に行なわれ得る。こ
うして硬性された材料は超a−波変換器(でおいてマツ
チング層@科として有利に4り用される。
This string does not fill the entire cross section of the container 1, and in some cases additionally has a shell dll/I'L7,
These through holes are then filled with fluid resin 8.
passes through. Now, when the container 1 is rotated, the centrifugal force will push the filter 1 all 5 further onto the glass bulb, and the resin will pass through the filter stopper and out of the glass hollow bulb! Fill in the blank in d1. II! J! This can be carried out during the curing of the material or after appropriate shrinkage. The material thus hardened is advantageously used as a matching layer in ultra-a-wave transducers.

【図面の簡単な説明】[Brief explanation of the drawing]

図面は本発明による方法を説明するための図である。 1・・・容器、2・・軸線、6−底、4・・・ガラス中
空球、5・・フィルタ栓、6・・・おもり、7 ・W曲
孔。
The drawings are diagrams for explaining the method according to the invention. DESCRIPTION OF SYMBOLS 1... Container, 2... Axis line, 6-Bottom, 4... Glass hollow sphere, 5... Filter stopper, 6... Weight, 7 - W curved hole.

Claims (1)

【特許請求の範囲】 1)樹脂によシ結合される軽緻な充填材料から成る督1
■」の製造方法において、充填材料(4)が遠・已分離
1−9(1)内に導入され、また流動性の樹脂(8)に
よりおひわれ、またその後に両−決素が、昆汁に至るま
で、また場合によってv′1fii141ヒに至るまで
遠心分離1幾にかけられることを特徴とするi#¥@′
伺科の模造方法。 2〕光塙I′A科(4ンの、・4人後にフィルタ1オ料
(5)およびkもり(6)が相次いで九填倒科(4)の
」二にl1ii!せられ、またおもり(6)の上に流動
性の樹脂(8)が遠心分離の前に載せられ、ま/ヒおも
り(6)が樹脂(8)に対rる貞1lLL (7)を有
することを特徴とする特許請求の範囲第1頃1(d域の
方法。 6ン 光jH@r)(4Jとしてマイクロ中空球が用い
られることを特徴とする特許請求のi#iΣ囲渠1項ま
たは第2項記載の方法。 4)マイクロ中空球がガラス中空球であることを特徴と
する特許請求の範囲第う項記載の方法。 5)樹脂としてエポキシドまたはポリエステル樹脂が用
いられることを特徴とする特許請求の範囲41項ないし
第4項のいずれかに記載の方法。 6)樹脂、好ましくはエポキシドまたはポリエステル樹
脂により結合されるマイクロ中空ガラス球の形態の軽量
な充填+A科から成る軽M。 1Δl’)の製作方法であって、マイクロ中空ガラス球
が細粉化された反応硬化樹脂と混きされ、型のなかに満
たされ、軽度に2もしをの、ピられまた好ましくは超音
波((より硬化されまたそのすぐ後に流動性の反応樹脂
で溝だされ、この反応樹脂が続いて硬化することを特徴
とする特許請求の範囲rxc 4 J/j記戦記載法。 7)硬化された桐材が充填前に型から取出されることを
特徴とする特W「請求の範囲第6項記載の方法。 8)型がポリメヂルベ/テンから成っていることを特徴
とする特許請求の範囲第6項または第yimll記載の
方法。
[Claims] 1) An article 1 consisting of a light filler material bonded to a resin.
In the manufacturing method of ``2'', the filler material (4) is introduced into the far/deep separation 1-9 (1), and is covered with the fluid resin (8), and after that the double-determined element is i#¥@' characterized by being subjected to centrifugation until it reaches konju, and in some cases until it reaches v′1fii141hi.
How to imitate Ikushina. 2] Mitsunawa I'A class (4th class, after 4 people, filter 1 o charge (5) and k mori (6) were successively placed in the 9th class class (4)'s second l1ii!, and A fluid resin (8) is placed on the weight (6) before centrifugation, and the weight (6) has a ratio of 11LL (7) to the resin (8). Claim 1 (method in the d region. 4) The method according to claim 1, wherein the micro hollow spheres are glass hollow spheres. 5) The method according to claim 1, wherein epoxide or polyester resin is used as the resin. The method according to any one of Range 41 to 4. 6) Light M consisting of a lightweight filling in the form of micro hollow glass spheres bonded by a resin, preferably an epoxide or polyester resin + family A. 1Δl'), in which micro-hollow glass spheres are mixed with pulverized reaction-curing resin, filled into a mold, lightly heated, cracked, and preferably ultrasonicated ( (Claim RXC 4 J/J War Description Method, characterized in that it is further cured and immediately thereafter grooved with a fluid reactive resin, and this reactive resin is subsequently cured. 7) Cured. 8) A method according to claim 6, characterized in that the paulownia wood is removed from the mold before filling. The method described in Section 6 or Section yimll.
JP2079185A 1984-02-08 1985-02-05 Manufacture of light-weight material Pending JPS60183107A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE3404479.5 1984-02-08
DE19843404479 DE3404479A1 (en) 1984-02-08 1984-02-08 Process for producing a lightweight material
DE3424474.3 1984-07-03

Publications (1)

Publication Number Publication Date
JPS60183107A true JPS60183107A (en) 1985-09-18

Family

ID=6227152

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2079185A Pending JPS60183107A (en) 1984-02-08 1985-02-05 Manufacture of light-weight material

Country Status (2)

Country Link
JP (1) JPS60183107A (en)
DE (1) DE3404479A1 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4325398C1 (en) * 1993-07-29 1994-07-21 Grieshaber Vega Kg Piezo-electric sound transducer
DE10254253A1 (en) * 2002-11-20 2004-06-09 Brandt, Jochen, Prof. Production of a flat glassy or ceramic molded body for architectural purposes comprises shaking a charge of pearls made from glass or ceramic onto a flat heat-resistant substrate forming a pearl layer, heating and removing the substrate
DE102007047013A1 (en) * 2007-10-01 2009-04-02 Robert Bosch Gmbh Reaction resin and two-component system for producing the same
EP2202264B1 (en) * 2008-12-24 2018-04-18 Safran Aero Boosters SA Method for manufacturing by moulding a structural element of a machine with an abradable surface

Also Published As

Publication number Publication date
DE3404479A1 (en) 1985-08-08

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