JPS599535A - Method for testing airtightness of body - Google Patents

Method for testing airtightness of body

Info

Publication number
JPS599535A
JPS599535A JP11905782A JP11905782A JPS599535A JP S599535 A JPS599535 A JP S599535A JP 11905782 A JP11905782 A JP 11905782A JP 11905782 A JP11905782 A JP 11905782A JP S599535 A JPS599535 A JP S599535A
Authority
JP
Japan
Prior art keywords
vacuum
airtightness
degree
vacuum degree
testing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP11905782A
Other languages
Japanese (ja)
Inventor
Hisakazu Kataoka
久和 片岡
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Electric Corp
Original Assignee
Mitsubishi Electric Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Electric Corp filed Critical Mitsubishi Electric Corp
Priority to JP11905782A priority Critical patent/JPS599535A/en
Publication of JPS599535A publication Critical patent/JPS599535A/en
Pending legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01MTESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
    • G01M3/00Investigating fluid-tightness of structures
    • G01M3/02Investigating fluid-tightness of structures by using fluid or vacuum
    • G01M3/26Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors
    • G01M3/32Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for containers, e.g. radiators
    • G01M3/3281Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for containers, e.g. radiators removably mounted in a test cell
    • G01M3/329Investigating fluid-tightness of structures by using fluid or vacuum by measuring rate of loss or gain of fluid, e.g. by pressure-responsive devices, by flow detectors for containers, e.g. radiators removably mounted in a test cell for verifying the internal pressure of closed containers

Abstract

PURPOSE:To perform the judgment of the large leak and the medium leak of a body with excellent reliability, by detecting the change in vacuum degree when the inside of an airtight container, wherein the body having an airtight chamber is enclosed, is evacuated. CONSTITUTION:A semiconductor device 1, which is sealed in a hollow package, is enclosed in a port 2. A leak valve 3 is closed, and the inside of the port 2 is evacuated by a vacuum pump 4. At this time, the temporal change of the vacuum degree is detected by a vacuum gage 5, and the result is displayed on a vacuum degree display device 6. The signal is further processed by a CPU7, and the vacuum degree characteristics are stored in a memory device 8. In the memory device 8, the vacuum degree characteristics for a perfect airtight body which has the same volume as that of the semiconductor 1, are stored. Said characteristics and the measured vacuum degree characteristics are compared, and the quality of the semiconductor device 1 is judged. Since a visual test is not performed, the judgment of the large leak and the medium leak can be performed with excellent reliability.

Description

【発明の詳細な説明】 この発明は、例えばセラミックパッケージ型半導体装置
のような気密室を有する物体の気密性試験、特に試験レ
ベルから言うとグロスリークテストの領域に関するもの
である。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to an airtightness test of an object having an airtight chamber, such as a ceramic packaged semiconductor device, and particularly to the field of gross leakage testing from a test level.

従来この種の試験として、中空パッケージに半導体素子
を気密封止した半導体装置に対して行われるバブルリー
クテストと呼ばれる高温液中への浸漬試験またはグロス
リークテストと呼ばれる液体圧入後の高温液中浸漬試験
があった。バブルリークテス!・は、1〜l X IQ
 Torr lAの漏れを検査するために行うもので、
約130°Cの液中に半導体装置を浸漬し、その気密室
内部のガスの膨張によるガス圧力の増大によって、パッ
ケージの微小穴からガスが液中に吹き出されて生ずる泡
の有無を肉眼で観察して良否判定を行なうものである。
Conventionally, this type of test is conducted on a semiconductor device in which a semiconductor element is hermetically sealed in a hollow package by immersion in a high-temperature liquid called a bubble leak test, or by immersion in a high-temperature liquid after liquid pressurization called a gross leak test. There was an exam. Bubble leak test!・is 1~l X IQ
This is done to check for leakage of Torr lA.
A semiconductor device is immersed in a liquid at approximately 130°C, and as the gas pressure increases due to the expansion of the gas inside the airtight chamber, gas is blown out into the liquid from the microscopic holes in the package, and the presence or absence of bubbles is observed with the naked eye. It is used to judge the quality of the product.

グロスリークテストとは、バブルリークテスト前に半導
体装置を真空に引き(MIL規格では1O−3Torr
 )、この後バブルリークテストに使用する液より十分
に沸点の低い液体に浸漬し、さらにこのまま圧力をかけ
てバブルリークテストの検出感度を上げたものであり、
感度としては1〜1 x 10”−6Torr l/s
と言われている。もし気密性を有するパッケージに微小
穴があると、この中に沸点の低い液体が圧入され、この
状態でバブルリークテストと同様に130°0の液中に
浸漬されると、圧入された液体が気化11、この気密室
内部の圧力変化はバブルリークテストの場合よりはるか
に大きいので、検出感度が上がることになる。なお’I
’orr l/Aの単位は、ある真空度において1秒間
に何Iの漏れがあるかということである。
A gross leak test is a test in which the semiconductor device is evacuated (1O-3 Torr according to the MIL standard) before the bubble leak test.
), then immersed in a liquid with a boiling point sufficiently lower than the liquid used for the bubble leak test, and then pressurized as it is to increase the detection sensitivity of the bubble leak test.
Sensitivity: 1 to 1 x 10”-6Torr l/s
It is said that If an airtight package has microholes, a liquid with a low boiling point is injected into the holes, and if the liquid is immersed in a liquid at 130° as in the bubble leak test, the injected liquid will Vaporization 11: Since the pressure change inside this airtight chamber is much larger than in the case of a bubble leak test, the detection sensitivity increases. Nao'I
'orr The unit of l/A is how many I leak in one second at a certain degree of vacuum.

しかるに」二記の方法によるときは、気密室の微小穴か
らガスが吹き出されて生じる小さな気泡の有無をいずれ
も人間が目で見て良否を判定するので、見のがしが発生
し試験の信頼性が悪くなるという欠点があった。
However, when using the second method, humans visually check for the presence or absence of small bubbles that are generated when gas is blown out from microscopic holes in the airtight chamber, which can lead to oversights and reduce the reliability of the test. The drawback was that it got worse.

この発明は上記のような従来の方法の欠点を除去するた
めになされたもので、気密室を有する物体が収められた
気密容器内を排気装置で排気し、前記気密容器内の真空
度の変化に基づいて前記物体の気密性試験を行なうこと
により、肉眼にたよる試験で起こる見落しによる信頼性
の低下をきたすことがなく、バブルリークまたはグロス
リークと呼ばれる大リーク・中リークの判定を信頼度良
く行なうことができる方法を提供することを目的として
いる。
This invention was made in order to eliminate the drawbacks of the conventional method as described above, and the present invention was made in order to eliminate the drawbacks of the conventional method. By conducting the airtightness test of the object based on the above, there is no reduction in reliability due to oversights that occur in tests that rely on the naked eye, and the judgment of large and medium leaks called bubble leaks or gross leaks can be trusted. The purpose is to provide a method that can be used efficiently.

以下、この発明の一実施例を図について説明する。第1
図においてfi+は半導体素子が中空セラミックパッケ
ージ内に封止され、0.1 d以上の空間を有する気密
室を持つ半導体装置で、気密性試験を行なう物体である
。(21はこの判導体装置(1)を内部に格納する容積
が100ffl以下の気密筐体のポートであり、気密容
器を構成する。(3)はこの気密容器(2)の排気口に
開口の一端が取り付けられたリークバルブ、(41はこ
のリークバルブ(3)の気密容器(2)側の開口と連通
ずる開口に取り付けられ気密容器(2)内を排気する真
空ポンプすなわち排気装置、(i5)は気密容器(2)
の開口部に取り付けられ真空度を検出し信号を電圧変換
する真空計、(61はこの真空計(51に接続され真空
度を表示する真空度表示器、α(至)ハマイクロコンピ
ュータであり、真空計(5)からの信号を処理するO 
P U (71と、このOP U (71で処理された
データを記憶する記憶装置(8)と、CPU(7)に接
続された出力装置(9)および入力装置(1(1で構成
されている。
An embodiment of the present invention will be described below with reference to the drawings. 1st
In the figure, fi+ is a semiconductor device in which a semiconductor element is sealed in a hollow ceramic package and has an airtight chamber having a space of 0.1 d or more, and is an object to be tested for airtightness. (21 is a port of an airtight casing with a volume of 100 ffl or less for storing this conductor device (1) inside, and constitutes an airtight container. (3) is a port of an airtight case that stores the conductor device (1) inside. A leak valve (41) is attached to one end of the leak valve (3) and communicates with the opening on the side of the airtight container (2). ) is an airtight container (2)
a vacuum gauge that is attached to the opening of the vacuum gauge to detect the degree of vacuum and convert the signal to voltage, (61 is a vacuum degree indicator connected to this vacuum gauge (51 and displays the degree of vacuum, O that processes the signal from the vacuum gauge (5)
P There is.

」二記のように構成されたものにおいて、半導体装置(
])をポー1−121に収容し、リークバルブ(3)を
閉じた状態でボート(2)内を真空ポンプ141によっ
て排気する。このとき時間の経過と共に変化する真空度
が真空計(5)によって検出され、この検出された情報
は信号に変換されて真空度表示器(6)に表示される。
” In a device configured as described in Section 2, the semiconductor device (
]) is accommodated in the port 1-121, and the inside of the boat (2) is evacuated by the vacuum pump 141 with the leak valve (3) closed. At this time, the degree of vacuum, which changes over time, is detected by a vacuum gauge (5), and this detected information is converted into a signal and displayed on a degree of vacuum indicator (6).

またその信号はOP U (71にも送られて処理され
た後、記憶装置(8月こ入力されて、例えば第2図にα
υで示す真空度特性が記憶される。ここで上記半導体装
置illと同じ体積の完全気密性物体または気密室を持
たない物体を同じ条件で排気して得た例えば第2図に(
121で示す真空度特性を、入力装置+91を用いて予
め記憶装置(8)に基準として記憶させておく。この記
憶された2つの真空度特性を読み出してa p U (
71で比較させ、例えば所定排気時間t□における真空
度に差があるかどうかによって半導体装置(11の気密
性の良否判定を行ない、データ・結果等を出力装置口0
に出力させる。このように真空度の変化に基づいて気密
性試験を行なうので、従来のような誤りが生じやすい目
視試験がなく信頼性の高い試験ができ、またコンピュー
タを使用しているので真空度の変化の読み取り・記憶・
比較・出力、他のデータの入力等を即座に正確に行なう
ことができる。また高価なリーク試験液も不要となる。
The signal is also sent to the OP U (71) and processed, and then inputted to the storage device (August 2011) and stored in the α
The vacuum characteristic indicated by υ is memorized. For example, as shown in FIG.
The vacuum characteristic shown by 121 is previously stored in the storage device (8) as a reference using the input device +91. These two stored vacuum degree characteristics are read out and a p U (
For example, the airtightness of the semiconductor device (11) is judged based on whether there is a difference in the degree of vacuum at a predetermined evacuation time t□, and the data and results are output to the output device port 0.
Output to . Since the airtightness test is performed based on changes in the degree of vacuum in this way, there is no visual test that is prone to errors as in conventional methods, making it possible to perform highly reliable tests.Also, since a computer is used, it is possible to perform airtightness tests based on changes in the degree of vacuum. reading/memory/
Comparison/output, input of other data, etc. can be performed immediately and accurately. Also, expensive leak test liquid is not required.

。 なお上記実施例では、所定時間経過後の真空度に基づい
て試験するようにしたが、例えば第2図に示す所定真空
度1′0に達するまでの時間t1基準の特性0′IJに
おける時間t、oと比較させる試験であってもよく、要
するに排気する時間の峰過につれて変化していく真空度
特性Ql)を求め、真空度特性の基準(1つと比較させ
る試験であればよい。
. In the above embodiment, the test was carried out based on the degree of vacuum after a predetermined time has elapsed, but for example, the time t at the characteristic 0'IJ based on the time t1 until reaching the predetermined degree of vacuum 1'0 shown in FIG. , o. In short, it may be a test in which the degree of vacuum characteristic (Ql) that changes as the evacuation time peaks is determined and compared with a standard (one) of the degree of vacuum characteristic.

また比較はo p U 171に行なわせたが、出力装
置001に出力された真空度の変化を読み取って比較を
してもよく、また真空度の変化はコンピュータ0.ll
lによって処理させたが、表示装置161に表示された
真空度の変化を読み取って比較してもよい。
Further, the comparison was made by the op U 171, but the change in the degree of vacuum outputted to the output device 001 may be read and compared, and the change in the degree of vacuum can be detected by the computer 0. ll
1, but the change in the degree of vacuum displayed on the display device 161 may be read and compared.

さらにポート(2)の排気は真空ポンプを使用して行な
ったが、他の排気装置で排気してもよく、また排気条件
をコンピュータ等を使用した制御装置で制御してもよく
、排気装置を制御する場合排気条件をより安定に保つこ
とができ試験精度を向上させることができる。
Furthermore, although the port (2) was evacuated using a vacuum pump, it may be evacuated using other evacuation equipment, or the evacuation conditions may be controlled by a control device using a computer or the like. When controlled, exhaust conditions can be kept more stable and test accuracy can be improved.

さらに−に記実施例ではポート(2)内に1つの半導体
装置(1)を収容したが、複数個を同時に収容してもよ
く、またポート(2)は1つであったが複数個のポート
を設け、それぞれのポートを1つの排気装置で排気して
真空度の変化を求めてもよく、この場合試験の処理能力
を向上させることができる。
Furthermore, although one semiconductor device (1) was housed in the port (2) in the embodiment described in -, it is also possible to house a plurality of semiconductor devices at the same time. Ports may be provided and each port may be evacuated by one exhaust device to determine changes in the degree of vacuum. In this case, the throughput of the test can be improved.

さらにまた上記実施例ではポート(2)の容積は100
d以下、半導体装置(1)の気密室の容積は0.】2以
上すなわち容積比は1000:1より小としたがこれに
限るものでなく、また被試験物体を半導体装置としたが
これに限るものでもないことは言うまでもない。
Furthermore, in the above embodiment, the volume of port (2) is 100
d or less, the volume of the airtight chamber of the semiconductor device (1) is 0. 2 or more, that is, the volume ratio is smaller than 1000:1, but the present invention is not limited to this, and although the object to be tested is a semiconductor device, it goes without saying that the present invention is not limited to this.

さらに上記実施例では半導体装置(11は前処理されて
いないが、予め気体中で大気圧以上に加圧されていても
よく、また予め大気圧以下に減圧された後、加熱によっ
て気化する性質を持つ液体中で大気圧以上に加圧されて
いてもよく、また真空度の変化は半導体装置(11の常
温状態で求めたが加熱状態で求めてもよく、加熱する場
合気体の体積が膨張するので試験感度を向上させること
ができる。
Furthermore, in the above embodiment, the semiconductor device (11) is not pretreated, but it may be pressurized above atmospheric pressure in advance, or it may have the property of being vaporized by heating after being previously reduced to below atmospheric pressure. It may be pressurized to above atmospheric pressure in the liquid it holds, and changes in the degree of vacuum can be determined in a semiconductor device (11) at room temperature, but it may also be determined in a heated state; when heated, the volume of the gas expands. Therefore, test sensitivity can be improved.

また上記実施例はポート(2)内を排気している間に求
めた真空度の変化であったが、所定の真空度に到達後排
気を停止させた状態で放置し、放置時間中に求めた真空
度の変化であってもよい。
In addition, in the above example, the change in the degree of vacuum was determined while the inside of port (2) was being evacuated. It may also be a change in the degree of vacuum.

以上のように、この発明によれば気密室を有する物体が
収められている気密容器内を排気したときの前記気密容
器内の真空度の変化に基づいて前記物体の気密性試験を
行なうようにしたので、従来の液体中の気泡を目視する
作業はなく、したがって気泡の見落しによる試験の信頼
性低下の要因はなく、物体の大リーク・中リークの判定
を信頼度良く行なうことができるという効果がある。
As described above, according to the present invention, the airtightness test of the object having an airtight chamber is performed based on the change in the degree of vacuum in the airtight container when the airtight container in which the object is housed is evacuated. As a result, there is no need to visually check for bubbles in the liquid as in the past, so there is no risk of unreliability in the test due to overlooked bubbles, and it is possible to determine whether an object has a large leak or a medium leak with high reliability. effective.

【図面の簡単な説明】[Brief explanation of drawings]

第1図はこの発明の一実施例を示す概念図、第2図はこ
の発明を説明するための真空度特性図である。 図において、(1)は物体、(2)は気密容器、(4)
は排気装置である。 代理人 葛野信− IQ+ 第1図 第2図 手続補正書(自発) 21発明の名称 物体の気密性試験方法 3、補正をする者 事件との関係   特許出願人 住 所     東京都千代田区丸の内二丁目2番3号
名 称(601)   三菱電機株式会社代表者片由仁
八部 4、代理人 住 所     東京都千代田区丸の内二丁目2番3号
三菱電機株式会社内 5、補正の対象 明細書の発明の詳細な説明の欄 6、 補正の内容 明細書@8頁第4行及び第18行1こ「180℃」 と
あるのを「125℃」と訂正する。 以上
FIG. 1 is a conceptual diagram showing an embodiment of this invention, and FIG. 2 is a vacuum degree characteristic diagram for explaining this invention. In the figure, (1) is the object, (2) is the airtight container, and (4)
is an exhaust system. Agent Makoto Kuzuno - IQ+ Figure 1 Figure 2 Procedural amendment (voluntary) 21 Name of the invention Method for testing the airtightness of objects 3, Relationship to the case of the person making the amendment Patent applicant address 2-chome Marunouchi, Chiyoda-ku, Tokyo No. 2 and 3 Name (601) Mitsubishi Electric Co., Ltd. Representative: Katayuni Yabu 4, Agent address: 5, 2-2-3 Marunouchi, Chiyoda-ku, Tokyo Mitsubishi Electric Co., Ltd. Invention of the specification subject to amendment Column 6 of the detailed explanation of the amendment @ page 8, line 4 and line 18, ``180℃'' is corrected to ``125℃.''that's all

Claims (9)

【特許請求の範囲】[Claims] (1)気密室を有する物体が収められている気密容器内
を排気装置で排気し、前記気密容器内の真空度の変化に
基づいて前記物体の気密性試験を行なうことを特徴とす
る物体の気密性試験方法。
(1) An airtight container containing an object having an airtight chamber is evacuated by an exhaust device, and the airtightness of the object is tested based on a change in the degree of vacuum in the airtight container. Airtightness test method.
(2)気密性試験は、所定の排気時間に対応する真空度
に基づいて行なわれる特許請求の範囲第1項記載の物体
の気密性試験方法。
(2) The airtightness test method for an object according to claim 1, wherein the airtightness test is performed based on a degree of vacuum corresponding to a predetermined evacuation time.
(3)気密性試験は、所定の真空度に対応する排気時間
に基づいて行なわれる特許請求の範囲第1項記載の物体
の気密性試験方法。
(3) The airtightness test method for an object according to claim 1, wherein the airtightness test is performed based on an evacuation time corresponding to a predetermined degree of vacuum.
(4)真空度の変化は表示手段に出力される特許請求の
範囲第1項記載の物体の気密性試験方法。
(4) The method for testing the airtightness of an object according to claim 1, wherein the change in the degree of vacuum is output to a display means.
(5)真空度の変化は信号に変換されて記憶装置に入力
される特許請求の範囲第1項記載の物体の気密性試験方
法。
(5) The method for testing the airtightness of an object according to claim 1, wherein the change in the degree of vacuum is converted into a signal and input into a storage device.
(6)真空度の変化は基準と比較される特許請求の範囲
第1項記載の物体の気密性試験方法。
(6) The airtightness testing method for an object according to claim 1, wherein the change in the degree of vacuum is compared with a reference.
(7)基準は信号に変換され、記憶装置に入力される特
許請求の範囲第6項記載の物体の気密性試験方法。
(7) The method for testing the airtightness of an object according to claim 6, wherein the reference is converted into a signal and input into a storage device.
(8)比較はコンピュータによって行なわれ出力装置に
出力される特許請求の範囲第6項記載の気密性試験方法
(8) The airtightness testing method according to claim 6, wherein the comparison is performed by a computer and output to an output device.
(9)気密容器の容積と物体の気密室の容積の比は10
00:1より小である特許請求の範囲第1項記載の物体
の気密性試験方法。 曲物体は半導体装置である特許請求の範囲第1項に記載
の物体の気密性試験方法。
(9) The ratio of the volume of the airtight container to the volume of the airtight chamber of the object is 10
A method for testing the airtightness of an object according to claim 1, wherein the airtightness is smaller than 00:1. 2. The method for testing the airtightness of an object according to claim 1, wherein the curved object is a semiconductor device.
JP11905782A 1982-07-06 1982-07-06 Method for testing airtightness of body Pending JPS599535A (en)

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JP11905782A JPS599535A (en) 1982-07-06 1982-07-06 Method for testing airtightness of body

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Application Number Priority Date Filing Date Title
JP11905782A JPS599535A (en) 1982-07-06 1982-07-06 Method for testing airtightness of body

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JPS599535A true JPS599535A (en) 1984-01-18

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Cited By (4)

* Cited by examiner, † Cited by third party
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JP2009165935A (en) * 2008-01-15 2009-07-30 Tlv Co Ltd Reduced-pressure steam-heating apparatus
JP2010117376A (en) * 1997-05-26 2010-05-27 Martin Lehmann Method and apparatus for leak testing
US8459099B2 (en) 1997-05-27 2013-06-11 Wilco Ag Method for leak testing and leak testing apparatus
CN104296945A (en) * 2013-07-15 2015-01-21 珠海格力电器股份有限公司 Evaporator leak detection system and leak detection method

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010117376A (en) * 1997-05-26 2010-05-27 Martin Lehmann Method and apparatus for leak testing
JP2010151846A (en) * 1997-05-26 2010-07-08 Martin Lehmann Method and apparatus for leak testing
US9091612B2 (en) 1997-05-26 2015-07-28 Wilco Ag Method for leak testing and leak testing apparatus
US8459099B2 (en) 1997-05-27 2013-06-11 Wilco Ag Method for leak testing and leak testing apparatus
JP2009165935A (en) * 2008-01-15 2009-07-30 Tlv Co Ltd Reduced-pressure steam-heating apparatus
CN104296945A (en) * 2013-07-15 2015-01-21 珠海格力电器股份有限公司 Evaporator leak detection system and leak detection method

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