JPS59213798A - グリセロ−ルエステル類の分離方法 - Google Patents
グリセロ−ルエステル類の分離方法Info
- Publication number
- JPS59213798A JPS59213798A JP58088166A JP8816683A JPS59213798A JP S59213798 A JPS59213798 A JP S59213798A JP 58088166 A JP58088166 A JP 58088166A JP 8816683 A JP8816683 A JP 8816683A JP S59213798 A JPS59213798 A JP S59213798A
- Authority
- JP
- Japan
- Prior art keywords
- glycerol esters
- solvent
- fatty acids
- separating
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000002314 glycerols Chemical class 0.000 title claims description 39
- 238000000926 separation method Methods 0.000 title claims description 5
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 40
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 38
- 229930195729 fatty acid Natural products 0.000 claims description 38
- 239000000194 fatty acid Substances 0.000 claims description 38
- 150000004665 fatty acids Chemical class 0.000 claims description 38
- 239000002904 solvent Substances 0.000 claims description 31
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 29
- 238000000034 method Methods 0.000 claims description 26
- 239000000203 mixture Substances 0.000 claims description 20
- 238000002844 melting Methods 0.000 claims description 18
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical group CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 15
- -1 first Chemical class 0.000 claims description 15
- 239000000706 filtrate Substances 0.000 claims description 13
- 238000005194 fractionation Methods 0.000 claims description 11
- 239000007788 liquid Substances 0.000 claims description 11
- 230000008018 melting Effects 0.000 claims description 11
- 239000000126 substance Substances 0.000 claims description 7
- 239000012454 non-polar solvent Substances 0.000 claims description 6
- 239000013078 crystal Substances 0.000 claims description 5
- 239000002798 polar solvent Substances 0.000 claims description 4
- 239000003921 oil Substances 0.000 description 33
- 235000019198 oils Nutrition 0.000 description 33
- 239000002994 raw material Substances 0.000 description 10
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 9
- 239000002253 acid Substances 0.000 description 9
- 238000006243 chemical reaction Methods 0.000 description 9
- 235000019879 cocoa butter substitute Nutrition 0.000 description 7
- 238000005809 transesterification reaction Methods 0.000 description 7
- 238000004458 analytical method Methods 0.000 description 6
- 239000003925 fat Substances 0.000 description 6
- 235000019197 fats Nutrition 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 230000035945 sensitivity Effects 0.000 description 6
- 238000004817 gas chromatography Methods 0.000 description 5
- AFABGHUZZDYHJO-UHFFFAOYSA-N 2-Methylpentane Chemical compound CCCC(C)C AFABGHUZZDYHJO-UHFFFAOYSA-N 0.000 description 4
- 102000004882 Lipase Human genes 0.000 description 4
- 108090001060 Lipase Proteins 0.000 description 4
- 239000004367 Lipase Substances 0.000 description 4
- 235000019421 lipase Nutrition 0.000 description 4
- 244000299461 Theobroma cacao Species 0.000 description 3
- 235000018936 Vitellaria paradoxa Nutrition 0.000 description 3
- 241001135917 Vitellaria paradoxa Species 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- 210000002683 foot Anatomy 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000000704 physical effect Effects 0.000 description 3
- 229940057910 shea butter Drugs 0.000 description 3
- 238000001256 steam distillation Methods 0.000 description 3
- 150000003626 triacylglycerols Chemical class 0.000 description 3
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 3
- 241000235527 Rhizopus Species 0.000 description 2
- 235000021355 Stearic acid Nutrition 0.000 description 2
- 235000005764 Theobroma cacao ssp. cacao Nutrition 0.000 description 2
- 235000005767 Theobroma cacao ssp. sphaerocarpum Nutrition 0.000 description 2
- OGBUMNBNEWYMNJ-UHFFFAOYSA-N batilol Chemical class CCCCCCCCCCCCCCCCCCOCC(O)CO OGBUMNBNEWYMNJ-UHFFFAOYSA-N 0.000 description 2
- 238000004061 bleaching Methods 0.000 description 2
- 235000001046 cacaotero Nutrition 0.000 description 2
- 238000004440 column chromatography Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 2
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 2
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 2
- 239000008117 stearic acid Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 241000282693 Cercopithecidae Species 0.000 description 1
- 206010011224 Cough Diseases 0.000 description 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- NHTMVDHEPJAVLT-UHFFFAOYSA-N Isooctane Chemical compound CC(C)CC(C)(C)C NHTMVDHEPJAVLT-UHFFFAOYSA-N 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 244000062730 Melissa officinalis Species 0.000 description 1
- 235000010654 Melissa officinalis Nutrition 0.000 description 1
- 235000019482 Palm oil Nutrition 0.000 description 1
- 235000019484 Rapeseed oil Nutrition 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 235000019219 chocolate Nutrition 0.000 description 1
- 235000005687 corn oil Nutrition 0.000 description 1
- 239000002285 corn oil Substances 0.000 description 1
- 235000012343 cottonseed oil Nutrition 0.000 description 1
- 230000001877 deodorizing effect Effects 0.000 description 1
- JVSWJIKNEAIKJW-UHFFFAOYSA-N dimethyl-hexane Natural products CCCCCC(C)C JVSWJIKNEAIKJW-UHFFFAOYSA-N 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000011005 laboratory method Methods 0.000 description 1
- 239000000865 liniment Substances 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 235000003441 saturated fatty acids Nutrition 0.000 description 1
- 150000004671 saturated fatty acids Chemical class 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 230000002747 voluntary effect Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58088166A JPS59213798A (ja) | 1983-05-19 | 1983-05-19 | グリセロ−ルエステル類の分離方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58088166A JPS59213798A (ja) | 1983-05-19 | 1983-05-19 | グリセロ−ルエステル類の分離方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS59213798A true JPS59213798A (ja) | 1984-12-03 |
| JPH0471119B2 JPH0471119B2 (enrdf_load_stackoverflow) | 1992-11-12 |
Family
ID=13935332
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58088166A Granted JPS59213798A (ja) | 1983-05-19 | 1983-05-19 | グリセロ−ルエステル類の分離方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59213798A (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003057807A3 (en) * | 2001-12-31 | 2003-10-30 | Cargill Inc | Process for oil extraction |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4834907A (enrdf_load_stackoverflow) * | 1971-09-06 | 1973-05-23 | ||
| JPS56127694A (en) * | 1980-03-12 | 1981-10-06 | Asahi Denka Kogyo Kk | Classification of sulseed fat |
| JPS57212299A (en) * | 1981-06-22 | 1982-12-27 | Asahi Denka Kogyo Kk | Fractionation of oil and fat |
-
1983
- 1983-05-19 JP JP58088166A patent/JPS59213798A/ja active Granted
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4834907A (enrdf_load_stackoverflow) * | 1971-09-06 | 1973-05-23 | ||
| JPS56127694A (en) * | 1980-03-12 | 1981-10-06 | Asahi Denka Kogyo Kk | Classification of sulseed fat |
| JPS57212299A (en) * | 1981-06-22 | 1982-12-27 | Asahi Denka Kogyo Kk | Fractionation of oil and fat |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2003057807A3 (en) * | 2001-12-31 | 2003-10-30 | Cargill Inc | Process for oil extraction |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0471119B2 (enrdf_load_stackoverflow) | 1992-11-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DK2388306T3 (en) | The fractionation method for 1,3-disaturated-2-unsaturated triglyceride | |
| Rossell | Fractionation of lauric oils | |
| JP6163530B2 (ja) | ココアバターと類似のハードバターの製造方法 | |
| KR20120104211A (ko) | 제과용 고융점 해바라기 지방 | |
| JPS62134043A (ja) | カカオバター代用脂 | |
| EP0505408A4 (en) | Selective esterification of long chain fatty acid monoglycerides with medium chain fatty acid anhydrides | |
| JP2010209147A (ja) | 油脂の製造方法 | |
| US4247471A (en) | Process for the production of a plurality of edible fractions from natural fatty substances, and the fractions produced in this way | |
| EP2457987A1 (en) | Method for producing tri-saturated fatty acid glyceride-containing fat compositions | |
| EP0531325B1 (en) | Low saturate frying oil with fried flavor | |
| Duns | Palm oil in margarines and shortenings | |
| CN111935987A (zh) | 新型高硬脂酸油料种子硬脂脂肪及其制备方法 | |
| CN111280281B (zh) | 油脂组合物及其制备方法 | |
| EP0426155A2 (en) | Hard butter composition | |
| US5326581A (en) | Chocolates | |
| CN113115830B (zh) | 用于巧克力的油脂组合物 | |
| JP3016688B2 (ja) | ハードバター組成物及びチョコレート様食品 | |
| JPS62201999A (ja) | カカオバタ−代用脂の製造方法 | |
| JPS61242543A (ja) | ハ−ドバタ−の品質改良法 | |
| JPS59213798A (ja) | グリセロ−ルエステル類の分離方法 | |
| JP3502158B2 (ja) | カカオ脂の分別方法及び該方法によって得られる分別脂を含有するチョコレート | |
| JPS62155048A (ja) | ハ−ドバタ−の製造法 | |
| JPH0427813B2 (enrdf_load_stackoverflow) | ||
| JPS594100B2 (ja) | 食用脂肪 | |
| JPH06184589A (ja) | 高安定性油 |