JPS59123762A - Laminated material for magnetic head - Google Patents

Laminated material for magnetic head

Info

Publication number
JPS59123762A
JPS59123762A JP22722482A JP22722482A JPS59123762A JP S59123762 A JPS59123762 A JP S59123762A JP 22722482 A JP22722482 A JP 22722482A JP 22722482 A JP22722482 A JP 22722482A JP S59123762 A JPS59123762 A JP S59123762A
Authority
JP
Japan
Prior art keywords
laminated material
layer
layers
magnetic head
thickness
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP22722482A
Other languages
Japanese (ja)
Inventor
Kenichiro Momose
百瀬 建一郎
Shizuo Ozeki
大関 静夫
Masahiro Namatame
生田目 真宏
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toshiba Corp
Original Assignee
Toshiba Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Toshiba Corp filed Critical Toshiba Corp
Priority to JP22722482A priority Critical patent/JPS59123762A/en
Publication of JPS59123762A publication Critical patent/JPS59123762A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C8/00Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C8/06Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases
    • C23C8/08Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases only one element being applied
    • C23C8/10Oxidising
    • C23C8/16Oxidising using oxygen-containing compounds, e.g. water, carbon dioxide
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C26/00Coating not provided for in groups C23C2/00 - C23C24/00

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Solid-Phase Diffusion Into Metallic Material Surfaces (AREA)
  • Physical Vapour Deposition (AREA)
  • Magnetic Heads (AREA)

Abstract

PURPOSE:To obtain a laminated material for a magnetic head preventing a loss due to an eddy current by heating a laminated material of an Ni-Fe alloy having an Al layer between layers to a specified temp. to form an insulating layer of Al2O3 between the layers. CONSTITUTION:The surface of a thin Ni-Fe alloy plate is coated with an Al layer by vapor deposition or other method, and laminating and rolling are carried out to obtain a laminated material having an Al layer between layers. The laminated material is heated to 750-1,300 deg.C, preferably 1,000-1,300 deg.C to form an insulating layer of Al2O3 between the layers. The thickness of the Al layer is regulated to <=1/10 times the thickness of the Ni-Fe alloy plate, and it is preferable to heat the laminated material in an atmosphere of wet gaseous hydrogen with <=0 deg.C, preferably <=-40 deg.C dew point. The core of a magnetic head can be formed accurately by using the resulting laminated material.

Description

【発明の詳細な説明】 [発明の技術分野] 本発明はへラドコアとして好適な磁気ヘッド用積層材に
関する。
DETAILED DESCRIPTION OF THE INVENTION [Technical Field of the Invention] The present invention relates to a laminated material for a magnetic head suitable as a helad core.

[発明の技術的背景とその問題点j 磁気ヘッドのコアとしては、従来からNi −Fe合金
等の強磁性体からなる薄板の1枚で形成されたもの、あ
るいはより優れた特性の要求される場合は、前jホの薄
板を複数枚(2〜6枚)積層したちの等か知られている
[Technical background of the invention and its problems j The core of a magnetic head has conventionally been formed of a single thin plate made of a ferromagnetic material such as a Ni-Fe alloy, or a core that is required to have better characteristics. In this case, it is known that a plurality of (2 to 6) thin plates are laminated.

この積層構造のコアにおいては、渦電流を防止するため
積層材の層間を絶縁する必要かあるか、この絶縁方法と
して従来は次のような方法により行われていた。
In the core of this laminated structure, is it necessary to insulate the layers of the laminated material in order to prevent eddy currents? Conventionally, this insulation method has been carried out by the following method.

すなわち、まずNi−Fe台金の薄板を所要形状にプレ
ス加工し、磁性焼鈍した後、この薄板の複数枚を有機接
着材により接着させC積層するとともに層間絶縁されて
いたが、この方法では精度よく積層することか困難で、
また煩雑であった。
That is, first, a thin plate of Ni-Fe base metal was pressed into the desired shape, magnetically annealed, and then a plurality of these thin plates were bonded together using an organic adhesive and laminated with C, and interlayer insulation was achieved. It is difficult to layer well,
It was also complicated.

このため、予め層間絶縁されかつ一体化された積層材を
所要形状に打抜き加工して使用すればこのような問題を
解決することができるか、Ni −「e合金様の間に有
機絶縁物を挾んで層間絶縁し、一体化したちのIは打抜
き後の磁性焼鈍に際して有機絶縁物か劣化、分解しC絶
縁の悪能を消失し、)Lだ絶縁物として無(浅黄を使用
する揚台は、滋す住焼鈍時の加熱に際しては絶縁物の分
解、劣化という問題がないか、無機絶縁物をNニーFe
合金の層間に挿入した場合は圧延し難いという欠点かあ
つ lこ 。
For this reason, it is possible to solve this problem by punching a laminated material that has been interlayer-insulated and integrated into a desired shape, or by adding an organic insulator between the Ni and e alloys. During the magnetic annealing after punching, the organic insulator deteriorates and decomposes, and the bad performance of the C insulation disappears. In order to determine whether there would be any problem of decomposition or deterioration of the insulator during heating during annealing, inorganic insulators were
The disadvantage is that it is difficult to roll when inserted between layers of alloy.

し発明の目的1 本発明省らはこのような欠点を解消する1こめ鋭意研究
を准めた結果、層間にΔρ図の形成されたNi−Fc含
金の積層材を熱処理すれは、A 、Q層が溶り、一部△
β203となって層間か絶縁されることを見出した。
Purpose of the Invention 1 The Ministry of the Invention and others have carried out intensive research to eliminate such drawbacks, and as a result, we have found that when heat treating a Ni-Fc metal laminated material with a Δρ diagram formed between the layers, A. Q layer melts, some parts △
It was found that β203 was obtained and insulation was achieved between the layers.

本発明はこのような知見に基づいてなされたもので、N
i−にe金合金居間か絶縁された磁気ヘッド用積層材を
提供することを目的とする。
The present invention was made based on such knowledge, and N
The object of the present invention is to provide a laminated material for a magnetic head that is insulated from gold alloy.

[発明の概要] すなわら本発明の磁気ヘッド用積層材は、積層し・たN
i−Fe合金板の間にA℃層が形成されている積層材を
750−1300’Cで加熱して層間に絶縁層を形成し
てなることを特徴とげる。
[Summary of the Invention] In other words, the laminated material for a magnetic head of the present invention has
It is characterized in that a laminated material in which an A°C layer is formed between i-Fe alloy plates is heated at 750-1300'C to form an insulating layer between the layers.

本発明において層間にA2層の形成されたN1−「e合
金板の積層材は例えば次のようにして製造される。
In the present invention, a laminate of N1-e alloy plates with an A2 layer formed between the layers is manufactured, for example, as follows.

Ni−Fe合金の薄板の表面に熱着、PVD法(物理蒸
着法)あるいはCVD法(化学蒸着法)によりA2層を
被覆し、これを複数枚、Aj2層が層間にくるように積
層して圧延するが、あるいは少数枚のNニーFe合金の
薄板の間にA1層を密盾しC高温で圧延、あるいはA2
層を鋳造圧延しでクラッドさせることにより得られる。
The A2 layer is coated on the surface of a Ni-Fe alloy thin plate by heat deposition, PVD (physical vapor deposition), or CVD (chemical vapor deposition), and multiple layers are stacked with the AJ2 layer between the layers. rolled, or A1 layer is tightly shielded between a few N-Fe alloy thin plates and rolled at high temperature, or A2
It is obtained by cladding the layers by casting and rolling.

なお、積層材におけるA℃層の厚さはNi−Fe合金板
の厚さの1/10以下とするようにする。この値を越え
ると磁気特性の劣化が大となる。
Note that the thickness of the A°C layer in the laminated material is set to 1/10 or less of the thickness of the Ni-Fe alloy plate. If this value is exceeded, the magnetic properties will deteriorate significantly.

次にこのようにして得られた積層材は、加熱され−C活
性化し、材料中又は雰囲気の酸素と結びついて居間に八
β203の絶縁層が形成される。なお、この熱処理の前
に所要形状に打抜き加工を施+iは、この熱処理時に磁
性焼鈍されることになる。
Next, the laminated material thus obtained is heated to activate -C, which combines with oxygen in the material or in the atmosphere to form an insulating layer of 8β203 in the living room. Note that, before this heat treatment, the punched material into a desired shape will be magnetically annealed during this heat treatment.

熱処理のン品度は750〜1300°C好ましくは10
00〜1300’Cが通しており、また加熱時の雰囲気
は露点か○°C以下好ましくは一40℃以下の湿潤水素
カス雰囲気か望ましい。熱処理温度を上述のように限定
したのは、750℃未満ではA2層が溶融しないのてA
ρ203を形成することが困河となり、また1300℃
を越えると工業的(こはむずかしくなる。また雰囲気の
露点を上述のように限定したlu田は、n点がO’C’
&越えると磁気特性劣化が大となるからである。
The quality of heat treatment is 750-1300°C, preferably 10
00 to 1300'C, and the atmosphere during heating is preferably a wet hydrogen scum atmosphere with a dew point of 0°C or below, preferably -40°C or below. The heat treatment temperature was limited as mentioned above because the A2 layer does not melt below 750°C.
It is difficult to form ρ203, and 1300℃
If the dew point of the atmosphere is limited as described above, the n point becomes O'C'.
This is because if the value exceeds .

E le明の実施例] 次に本発明の実施例につい−C説明づる。Example of E le Ming] Next, embodiments of the present invention will be explained.

厚さ1節の81%N1−5.5%MOFe合金の薄板2
枚の間に厚さ0.05uのへβ層を挿入し、圧延して厚
さ約0.6imの積層材を製造した。これを打抜きプレ
スにより所定形状にプレス加工し、次いで露点か−4,
0’C以下の湿潤水素カス雰囲気中で1050°Cで6
0分間加熱すること。
Thin plate 2 of 81% N1-5.5% MOFe alloy with a thickness of 1 node
A β layer with a thickness of 0.05 μ was inserted between the sheets and rolled to produce a laminate with a thickness of about 0.6 mm. This is pressed into a predetermined shape using a punching press, and then the dew point is -4,
6 at 1050°C in a wet hydrogen gas atmosphere below 0'C.
Heat for 0 minutes.

により、層間に八β203の絶縁層を形成するとともに
磁性焼鈍を行なった。
An insulating layer of 8β203 was formed between the layers, and magnetic annealing was performed.

このようにして得られたヘッドコアは、高周波における
透磁率か向上し、渦電流による損失が減少していた。
The thus obtained head core had improved magnetic permeability at high frequencies and reduced loss due to eddy currents.

[発明の効果] 以上説明したように本発明の磁気ヘッド用積層材は、予
め層間に絶縁層か形成された一体化した積層材であるの
で、精度よくヘッドコアを形成することかでき、またこ
の積層材を使用したヘッドコアは渦電流による損失が少
ない。
[Effects of the Invention] As explained above, since the laminated material for a magnetic head of the present invention is an integrated laminated material with an insulating layer formed between the layers in advance, the head core can be formed with high precision. Head cores using laminated materials have less loss due to eddy currents.

代理人弁理士   則 近 憲 佑 (ほか1名)Representative Patent Attorney Noriyuki Chika (1 other person)

Claims (1)

【特許請求の範囲】 〈1)積層したNi−Fe合金板の間(こA、C層が形
成されでいる積層材を、750〜1300℃で加熱して
層間に絶縁層を形成してなることを特徴とする磁気ヘッ
ド用積層材。 (2)へβ層の厚さは1\1−Fe合金板の厚さの1/
10以トである特許請求の範囲第1■p記載の磁気ヘッ
ド用積層材。 (3)A、f2層はクラン1〜法により形成される特許
請求の範囲第1項または第2項記載の看気ヘツ1へ用積
層材。 (4> AJ2層はPVD法あるいはCVD法により形
成される特許請求の範囲第1項または第2項記載の磁気
ヘッド用積層材。 (5)加熱温度(よ1000〜1300°Cである特許
請求の範囲第11JIJ〜第3項のいずれか1項記載の
磁気ヘラ1−組積層材。
[Claims] <1) An insulating layer is formed between the laminated Ni-Fe alloy plates by heating the laminated material in which the A and C layers are formed at 750 to 1300°C. Features of laminated material for magnetic heads. (2) The thickness of the β layer is 1/1/1 of the thickness of the 1-Fe alloy plate.
10 or more, the laminated material for a magnetic head according to claim 1(p). (3) The laminated material for the air vent 1 according to claim 1 or 2, wherein the A and f2 layers are formed by the clan method. (4> A laminated material for a magnetic head according to claim 1 or 2, in which the AJ2 layer is formed by a PVD method or a CVD method. (5) A patent claim in which the heating temperature is 1000 to 1300°C. A magnetic spatula 1-set laminate material according to any one of the range No. 11 JIJ to No. 3.
JP22722482A 1982-12-28 1982-12-28 Laminated material for magnetic head Pending JPS59123762A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP22722482A JPS59123762A (en) 1982-12-28 1982-12-28 Laminated material for magnetic head

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP22722482A JPS59123762A (en) 1982-12-28 1982-12-28 Laminated material for magnetic head

Publications (1)

Publication Number Publication Date
JPS59123762A true JPS59123762A (en) 1984-07-17

Family

ID=16857439

Family Applications (1)

Application Number Title Priority Date Filing Date
JP22722482A Pending JPS59123762A (en) 1982-12-28 1982-12-28 Laminated material for magnetic head

Country Status (1)

Country Link
JP (1) JPS59123762A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7938956B2 (en) 2003-03-13 2011-05-10 Millipore Corporation Water purification system and method, and module for the system

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS502198A (en) * 1973-05-03 1975-01-10
JPS57138022A (en) * 1981-02-20 1982-08-26 Mitsumi Electric Co Ltd Magnetic head

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS502198A (en) * 1973-05-03 1975-01-10
JPS57138022A (en) * 1981-02-20 1982-08-26 Mitsumi Electric Co Ltd Magnetic head

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7938956B2 (en) 2003-03-13 2011-05-10 Millipore Corporation Water purification system and method, and module for the system

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