JPS5871370A - Automatic controller for vapor deposition of metal on roll-film - Google Patents

Automatic controller for vapor deposition of metal on roll-film

Info

Publication number
JPS5871370A
JPS5871370A JP16943581A JP16943581A JPS5871370A JP S5871370 A JPS5871370 A JP S5871370A JP 16943581 A JP16943581 A JP 16943581A JP 16943581 A JP16943581 A JP 16943581A JP S5871370 A JPS5871370 A JP S5871370A
Authority
JP
Japan
Prior art keywords
output
voltage
amplifier
vapor deposition
film
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP16943581A
Other languages
Japanese (ja)
Inventor
Kazunari Takahashi
一成 高橋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Electric Industry Co Ltd
Original Assignee
Nippon Electric Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Electric Industry Co Ltd filed Critical Nippon Electric Industry Co Ltd
Priority to JP16943581A priority Critical patent/JPS5871370A/en
Publication of JPS5871370A publication Critical patent/JPS5871370A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/54Controlling or regulating the coating process
    • C23C14/542Controlling the film thickness or evaporation rate
    • C23C14/545Controlling the film thickness or evaporation rate using measurement on deposited material

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physical Vapour Deposition (AREA)

Abstract

PURPOSE:To control vapor deposition of a metal automatically and stably with high accuracy by providing an automatic voltage regulating circuit for an electric power generator consisting of an output voltage setter and an output voltage detector as the 1st loop and an automatic film thickness regulating circuit consisting of a regulator for the rate of deposition of metals and a sensor for the thickness of vapor deposited films as the 2nd loop. CONSTITUTION:If V0 of a setter 8 for the rate of vapor deposition is increased in the case of increasing, for example, the rate of vapor deposition on a film 7, the output V2 of a detecting amplifier 9 increases as well. This voltage V2 is one of the inputs to a voltage amplifier 12, and the voltage V4 corresponding to a difference from the input voltage V3 from a voltage setter 13 is inputted to a main amplifier 14. Therefore the output of the amplifier 14 increases and controls the base of a transistor 17 connected to the magnetic field coil 16 of a high frequency power generator 1, thereby applying a change to the magnetic field current. Here, the output of the generator 1 is picked up with a detector 15 for high frequency output voltage, and the detected voltage V5 is compared with the previously inputted voltage V4. When the V4 and V5 attain equality, the increase in the magnetic field current ceases and the output of the generator 1 is made constant.

Description

【発明の詳細な説明】 高周波誘導炉に投入されて溶融された金属蒸気を真空中
で薄いフィルムに蒸着させる真空蒸着装置において誘導
炉に高周波出力を供給する手段として一般に高周波発電
機が用いられている。
DETAILED DESCRIPTION OF THE INVENTION A high-frequency generator is generally used as a means for supplying high-frequency output to the induction furnace in a vacuum deposition apparatus that deposits melted metal vapor into a thin film in a vacuum in a high-frequency induction furnace. There is.

従来この種の真空蒸着装置においては第1図に示すよう
に、高周波発電機1によって発生される高周波出力は高
周波誘導炉3のコイル4に供給され炉内に置かれた図示
しない金属を加熱溶融して蒸気とする。一方、誘導炉3
の蒸気噴出孔である開口部2には送り出しロール5から
送出され1巻取ロール乙に巻き取られる薄いフィルム7
が一定速度で通過している。この際誘導炉3で加熱溶融
された金属蒸“気は真空中でフィルム7に蒸着定着され
る。
Conventionally, in this type of vacuum evaporation apparatus, as shown in FIG. 1, high-frequency power generated by a high-frequency generator 1 is supplied to a coil 4 of a high-frequency induction furnace 3 to heat and melt metal (not shown) placed in the furnace. and steam. On the other hand, induction furnace 3
A thin film 7 is sent out from the delivery roll 5 and wound onto the first winding roll B at the opening 2 which is a steam ejection hole.
is passing at a constant speed. At this time, the metal vapor heated and melted in the induction furnace 3 is deposited and fixed on the film 7 in a vacuum.

従来この種の真空蒸着装置はフィルム7の蒸着量を均一
にするため、誘導炉3の温度を一定とすると共にフィル
ム7が誘導炉3の開孔部2の面上を通過するときの送り
速度も均一とするl要がある。従って温度及び送り速度
の監視を必要としだ。したがって蒸着膜の厚さを変える
場合には誘導炉の温度と共にフィルム7゛の送り速度を
手動操作によって微細に調整する必要を生じ9作業能率
を低下し、且つ品質の均一を保つことが容易でなかった
Conventionally, in order to make the amount of film 7 deposited uniform, this type of vacuum evaporation apparatus keeps the temperature of the induction furnace 3 constant and adjusts the feed rate when the film 7 passes over the surface of the opening 2 of the induction furnace 3. It is also necessary to make it uniform. Therefore, monitoring of temperature and feed rate is required. Therefore, when changing the thickness of the deposited film, it is necessary to finely adjust the temperature of the induction furnace and the feed speed of the film by manual operation, which reduces work efficiency and makes it difficult to maintain uniform quality. There wasn't.

本発明は従来のかかる欠点を除去しフィルムへの蒸着量
の変更、並びにフィルムの送り速度の変化に対して誘導
炉6の加熱電力を供給する高周波発電機の界磁電流を自
動的に定状化させ。
The present invention eliminates such drawbacks of the conventional technology and automatically stabilizes the field current of the high-frequency generator that supplies heating power for the induction furnace 6 in response to changes in the amount of vapor deposited on the film and changes in the film feeding speed. Let it become.

誘導炉の温度」―昇を自動追従させて所定の膜厚のフィ
ルムを得ると共に能率の向上と製品の均一化を計ること
を目的とする。
The purpose is to automatically follow the temperature rise of the induction furnace to obtain a film of a predetermined thickness, as well as to improve efficiency and make the product uniform.

次に本発明の1実施例を第1図について説明高周波発電
機1は500Hz乃至10KHzの適当な出力であれば
よく、その出力によって高周波誘導炉3内の金属に渦電
流を生ぜしめ、該金属を高温に加熱して蒸気化しフィル
ム7への蒸着を行う。蒸着量を変えるには蒸着量設定器
8によって行ない、かくて設定器れる電圧が検出増幅器
9の1つの入力端子に入力される。また該検出増幅器9
のもう1つの入力端子には誘導炉6の膜厚測定用センサ
ー10の出力が時定数変換部11ヲ経て入力される。検
出増幅器9の出力は高周波発電機の出力電圧設定器13
の設定電圧と共に設定増幅器12に入力される。設定増
幅器12は検出増幅器9の出力V2と出力電圧設定器1
3の設定電圧V、の差v、ヲ出力し、この出力v4は自
動電圧調整用の主増幅器14に入力される。一方、高周
波発電機1の高周波出力電圧を検出する高周波出力電圧
検出器15の出力電圧V、が前記主増幅器14に入力さ
れ、前記V。
Next, one embodiment of the present invention will be explained with reference to FIG. is heated to a high temperature to vaporize it and deposit it on the film 7. The deposition amount is changed by means of a deposition amount setter 8, and the voltage thus set is input to one input terminal of the detection amplifier 9. In addition, the detection amplifier 9
The output of the film thickness measuring sensor 10 of the induction furnace 6 is inputted to the other input terminal via the time constant converter 11. The output of the detection amplifier 9 is the output voltage setter 13 of the high frequency generator.
is input to the setting amplifier 12 together with the setting voltage. The setting amplifier 12 connects the output V2 of the detection amplifier 9 and the output voltage setting device 1.
The difference v between the three set voltages V is output, and this output v4 is input to the main amplifier 14 for automatic voltage adjustment. On the other hand, the output voltage V of the high frequency output voltage detector 15 that detects the high frequency output voltage of the high frequency generator 1 is input to the main amplifier 14, and the output voltage V is input to the main amplifier 14.

とV、の差が増幅されて界磁電流を増加又は減少せしめ
、それによって発電機の出力電圧は上昇又は低下し+ 
v4とVBの差がほとんど零になったところで安定する
。また主増幅器14の出力は高周波発電機1の界磁線輪
16の電流を制御するためのトランジスタ、サイリスタ
の如き半導体素子17のベースに接続されている。
The difference between and V is amplified and causes the field current to increase or decrease, thereby increasing or decreasing the generator output voltage +
It stabilizes when the difference between v4 and VB becomes almost zero. Further, the output of the main amplifier 14 is connected to the base of a semiconductor element 17 such as a transistor or a thyristor for controlling the current of the field wire ring 16 of the high frequency generator 1.

次に上述した本発明の動作につりで説明する。Next, the operation of the present invention described above will be explained in detail.

各入出力部分の電圧値に示すように、まず出力電圧設定
器13の電圧V、によって高周波発電機1の出力電圧が
設定され、高周波誘導炉3の温度が規定された値に保た
れているものとする。
As shown in the voltage values of each input/output section, the output voltage of the high frequency generator 1 is first set by the voltage V of the output voltage setting device 13, and the temperature of the high frequency induction furnace 3 is maintained at a specified value. shall be taken as a thing.

いまフィルム7の蒸着量を増した膜厚フィルムを得よう
とするために温度を上げる例について述べる。
An example of increasing the temperature in order to obtain a thick film with an increased amount of evaporated film 7 will now be described.

いまフィルム蒸着量設定器8の電圧V。全増加器12の
1つの入力となシ、既に設定されている電圧設定器16
からの入力電圧v3と共に前記設定増幅器12に入力さ
れる。電圧設定増幅器12はこの2人力の差を出力し、
出力電圧はv2−v3に相当する電圧v4となる。この
とき電圧V4i 1つの入力とする主増幅器14の出力
は増加し、高周波発電機1の界磁線輪16に接続されて
いるトランジスタ17のベースを制御して界磁電流に変
化を与える。すなわち蒸着量設定器8の電圧V。全増加
させると界磁電流も増加し、この界磁電流の増加は高周
波出力電圧を上昇させる。ここで高周波発電機1の出力
は高周波変圧器によって構成された高周波出力電圧検出
器15によってピックアップされ、その検出電圧V、は
主増幅器14の入力に加えられ先に入力された電圧v4
と比較され、v4の値にV、の値がほぼ等しくなったと
き界磁電流の増加は止まり高周波発電機の出力電圧はほ
ぼ一定となる。
Now the voltage V of the film deposition amount setting device 8. One input of the total increaser 12 and the already set voltage setter 16
It is input to the setting amplifier 12 together with the input voltage v3 from . The voltage setting amplifier 12 outputs the difference between these two forces,
The output voltage becomes a voltage v4 corresponding to v2-v3. At this time, the output of the main amplifier 14 which receives the voltage V4i as one input increases, and the base of the transistor 17 connected to the field wire ring 16 of the high frequency generator 1 is controlled to change the field current. That is, the voltage V of the vapor deposition amount setting device 8. When the total is increased, the field current also increases, and this increase in field current increases the high frequency output voltage. Here, the output of the high-frequency generator 1 is picked up by a high-frequency output voltage detector 15 constituted by a high-frequency transformer, and the detected voltage V is added to the input of the main amplifier 14, and the previously input voltage v4
When the value of V becomes approximately equal to the value of v4, the field current stops increasing and the output voltage of the high frequency generator becomes approximately constant.

即ち、蒸着量設定器8の設定を上げると発電機1の出力
電圧が上昇し、出力電流が増加し。
That is, when the setting of the vapor deposition amount setting device 8 is increased, the output voltage of the generator 1 increases, and the output current increases.

誘導炉3の温度が上昇し、金属蒸気が増加し。The temperature of the induction furnace 3 rises, and metal vapor increases.

フィルムへの蒸着量が多くなり、蒸着膜厚が厚くなる。The amount of vapor deposited on the film increases, and the thickness of the vapor deposited film increases.

この膜厚値を膜厚センサー10で検出し。This film thickness value is detected by a film thickness sensor 10.

時定数変換部11ヲ経て電圧値v1として検出増幅器9
に入力させる。この自動制御回路は膜厚値v1が設定蒸
着量V。とほぼ等しくなったところで平衡安定する。
After passing through the time constant converter 11, the voltage value v1 is output to the detection amplifier 9.
input. In this automatic control circuit, the film thickness value v1 corresponds to the set deposition amount V. Equilibrium is stabilized when it becomes approximately equal to .

時定数変換部11ば、何らかの理由そフィルム7の速度
が変ったときに、蒸着膜厚を一定に保つのに有効に作用
する。時定数変換部11は比例積分増幅器の一種で、入
力の変化に対して出力はある時間をかけて徐々に変化す
るものである。
The time constant converter 11 effectively acts to keep the deposited film thickness constant when the speed of the film 7 changes for some reason. The time constant converter 11 is a type of proportional-integral amplifier, and the output gradually changes over a certain period of time in response to a change in the input.

いま、フィルム速度が上昇した場合を例にとって説明す
ると、この場合には蒸気量が一定であるからフィルム蒸
着量が減り、膜厚が薄くなる。
Taking as an example the case where the film speed increases, in this case, since the amount of vapor is constant, the amount of film evaporated decreases and the film thickness becomes thinner.

そこで膜厚センサーの検出値は薄くなった分だけ減少し
て時定数変換部11に入力するが、その出力v1は徐々
に減少し、従って検出増幅器91の出力v2も徐々に増
大し、それによって発電機出力電圧、出力電流を徐々に
増加せしめる。発電機出力電圧、電流を徐々に増加する
と9発電機電圧と誘導炉温度、すなわち蒸気量、蒸着量
Therefore, the detected value of the film thickness sensor decreases by the amount of thinning and is input to the time constant converter 11, but its output v1 gradually decreases, and therefore the output v2 of the detection amplifier 91 also gradually increases. Gradually increase the generator output voltage and output current. When the generator output voltage and current are gradually increased, 9 generator voltage and induction furnace temperature, i.e. steam amount, vapor deposition amount.

膜厚との時間おくれがなくなるので、オーバーシュート
して膜厚が設定値を越えることはない。
Since there is no time lag between the film thickness and the film thickness, the film thickness will not exceed the set value due to overshoot.

もし時定数変換部11がないとすると1発電機電圧が急
激に変化するので1発電機電圧と誘導炉温度、蒸気量、
蒸着量、膜厚との間に時間おくれが現われ、設定値に対
して膜厚がオーバーシュートすることになる。
If there is no time constant converter 11, the voltage of one generator will change rapidly, so the voltage of one generator, the temperature of the induction furnace, the amount of steam,
A time lag appears between the deposition amount and the film thickness, and the film thickness overshoots with respect to the set value.

以上述べたように9本発明は第1のループとして出力電
圧設定器と出力電圧検出器による発電機の自動電圧調整
回路を有し、第2のループとして金属蒸着量設定器と蒸
着膜厚センサーによる自動膜厚調整回路を有し、自動膜
厚調整回路の出力は自動電圧調整回路の出力電圧設定を
補正する形になっている。そして9時定数変換回路を設
け、自動膜厚調整回路の出力を徐々に増減することによ
り、膜厚調整におけるオーバーシュートを防止している
。従って本装置により安定で精度の高い金属蒸着自動制
御が可能と残った。
As described above, the present invention has a generator automatic voltage adjustment circuit using an output voltage setting device and an output voltage detector as the first loop, and a metal deposition amount setting device and a deposition film thickness sensor as the second loop. The automatic film thickness adjustment circuit has an automatic film thickness adjustment circuit whose output corrects the output voltage setting of the automatic voltage adjustment circuit. A time constant conversion circuit (9) is provided to gradually increase/decrease the output of the automatic film thickness adjustment circuit, thereby preventing overshoot in film thickness adjustment. Therefore, it remains possible to perform stable and highly accurate automatic metal deposition control using this device.

以下余白Margin below

Claims (1)

【特許請求の範囲】 1、高周波発電機とその出力によって加熱される誘導炉
によって該誘導炉の開孔に近接して移動するロールフィ
ルムに前記誘導炉内に投入された金属を溶融して蒸着せ
しめる真空蒸着装置において、前記高周波発電機の出力
検出器の検出値と出力電圧設定、器の設定値を比較増幅
する主増幅器とからなる第1のループと、前記ロールフ
ィルムの蒸着膜厚を検出する膜厚センサーと。 その出力を入力する時定数変換部と、前記フィルムの蒸
着量を設定する蒸着量設定器と、前記時定数変換部出力
と蒸着量設定器の設定値とを比較増幅する検出増幅器と
、その検出増幅器の出力と前記出力電圧設定器の設定値
とを比較増幅する電圧設定増幅器によって構成された第
2のループと、前記主増幅器の出力により前記高周波発
電機の界磁線輪電流が制御される界磁線輪回路により前
記第1ループ第2ループを完了することを特徴とするロ
ールフィルムの金属蒸着自動制御装置。
[Scope of Claims] 1. Metal introduced into the induction furnace is melted and vapor deposited onto a roll film that moves close to the opening of the induction furnace by an induction furnace heated by a high-frequency generator and its output. In the vacuum evaporation apparatus, the first loop includes a main amplifier that compares and amplifies the detected value of the output detector of the high-frequency generator, the output voltage setting, and the set value of the device, and detects the evaporated film thickness of the roll film. with a film thickness sensor. a time constant converter that inputs the output thereof; a vapor deposition amount setter that sets the vapor deposition amount of the film; a detection amplifier that compares and amplifies the output of the time constant converter and the set value of the vapor deposition amount setter; A second loop constituted by a voltage setting amplifier that compares and amplifies the output of the amplifier and the setting value of the output voltage setting device, and the field coil current of the high frequency generator is controlled by the output of the main amplifier. An automatic control device for metal vapor deposition of a roll film, characterized in that the first loop and the second loop are completed by a field wire loop circuit.
JP16943581A 1981-10-24 1981-10-24 Automatic controller for vapor deposition of metal on roll-film Pending JPS5871370A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP16943581A JPS5871370A (en) 1981-10-24 1981-10-24 Automatic controller for vapor deposition of metal on roll-film

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP16943581A JPS5871370A (en) 1981-10-24 1981-10-24 Automatic controller for vapor deposition of metal on roll-film

Publications (1)

Publication Number Publication Date
JPS5871370A true JPS5871370A (en) 1983-04-28

Family

ID=15886542

Family Applications (1)

Application Number Title Priority Date Filing Date
JP16943581A Pending JPS5871370A (en) 1981-10-24 1981-10-24 Automatic controller for vapor deposition of metal on roll-film

Country Status (1)

Country Link
JP (1) JPS5871370A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6059064A (en) * 1983-08-20 1985-04-05 ライボルト・アクチエンゲゼルシャフト Method and device for controlling local evaporation power of evaporator on manufacturing thin layer on substrate by vacuum evaporation process
EP0166960A2 (en) * 1984-05-28 1986-01-08 Nisshin Steel Co., Ltd. Method of rapidly changing deposition amount in a continuous vacuum deposition process

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6059064A (en) * 1983-08-20 1985-04-05 ライボルト・アクチエンゲゼルシャフト Method and device for controlling local evaporation power of evaporator on manufacturing thin layer on substrate by vacuum evaporation process
EP0166960A2 (en) * 1984-05-28 1986-01-08 Nisshin Steel Co., Ltd. Method of rapidly changing deposition amount in a continuous vacuum deposition process

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