JPS5820170A - Preparation of sweetener - Google Patents
Preparation of sweetenerInfo
- Publication number
- JPS5820170A JPS5820170A JP56116966A JP11696681A JPS5820170A JP S5820170 A JPS5820170 A JP S5820170A JP 56116966 A JP56116966 A JP 56116966A JP 11696681 A JP11696681 A JP 11696681A JP S5820170 A JPS5820170 A JP S5820170A
- Authority
- JP
- Japan
- Prior art keywords
- sugar
- stevioside
- sweetener
- glycosides
- sweetness
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
Description
【発明の詳細な説明】
零発@紘ステビオずイド系配糖体によシ砂糖の甘味を増
加させ、更に砂糖とステビオサイド系配線体との均質な
配合を常に保持する仁とができる甘味料の製法に関する
ものである。[Detailed Description of the Invention] Zero-Hatsu@Hiro A sweetener that increases the sweetness of sugar by using stevioside glycosides, and further maintains a homogeneous blend of sugar and stevioside glycosides at all times. It is related to the manufacturing method.
砂糖の消費紘文化の尺度とされ、その嗜好性と相俟って
、世界における一糠の消費量は年々増加する傾向を示し
て来ている。Sugar consumption is regarded as a measure of culture, and combined with its palatability, the consumption of Ichibun in the world has been increasing year by year.
しかるに、近時欧米において、砂糖の過多摂取による疾
病が多発している丸め、食事の改善が国家的規模におい
て提唱され、実施されつ\ある。However, in recent years in Europe and America, where diseases caused by excessive intake of sugar have been occurring frequently, improvements in rounding and eating habits have been advocated and implemented on a national scale.
その対策として、砂糖の摂取量を節減することが第1の
課題である。また、我国でも、成人病の発症が急激に高
まり、その11紘欧米履に近付きつ\あると言われてい
る。また児童においても、肥満児の急速な増加、就学時
の児童の殆んどが虫歯の所有者であること、幼児の骨折
の多発等、砂糖の過剰摂取による疾病と見られる疾患も
多発して来ている現状である。従りて、砂糖の過剰摂取
の防止状急務のことである0しかし、1IpIIIは我
々の生活にとシ必須の嗜好品であシ、かつ、甘味の請求
は人にとって強烈であシ、甘味への満足感を出来るだけ
充たしたいという請求社どうしても抑えることができな
い。この相反する問題を解決する九めに、従来、幾多の
人工甘味料が開発されたが、どうしても、天然の?糖に
はその嗜好、風味等が劣シ、かつ、これらのもの紘纏類
でないため、健康保持上は無益のものであった。As a countermeasure, the first challenge is to reduce sugar intake. Furthermore, in our country, the incidence of adult diseases is rapidly increasing, and it is said that we are approaching the number 11 in Japan. In addition, in children, there are many diseases that appear to be caused by excessive sugar intake, such as the rapid increase in the number of obese children, the fact that most of the children who enter school have cavities, and the frequent occurrence of fractures in young children. This is the current situation. Therefore, there is an urgent need to prevent excessive sugar intake.However, 1IpIII is an essential luxury item in our lives, and the demand for sweetness is intense for people. The billing company's desire to satisfy the customer as much as possible cannot be restrained. Many artificial sweeteners have been developed in the past to solve these contradictory problems, but the question remains whether they are natural sweeteners or not. Sugar has inferior taste, flavor, etc., and since it is not a type of sugar, it is useless in terms of maintaining health.
そこ°で、本発明者は、砂糖と甘味料として従来知られ
ているステビオサイド系配糖体との相剰効米により、甘
味において天然の砂糖と殆んど変わらない嗜好、風味を
有し、しかも、ステビオサイドの甘味によシ、砂糖の使
用を減少させても、天然$111と同等の人に対する甘
味の満足感を与え、かつ保健上は十分な砂糖を与えられ
る知見を得た。Therefore, the present inventor has discovered that, due to the synergistic effect of sugar and stevioside glycosides, which are conventionally known as sweeteners, the sweetness has a taste and flavor that is almost the same as natural sugar. Moreover, even if the sweetness of stevioside is improved and the use of sugar is reduced, it has been found that it can give people the same sweet taste satisfaction as natural $111 and provide enough sugar from a health standpoint.
しかるK)たに単に両者を所定の割合で混合し九のでは
、砂糖に対しステビオサイドの使用量が微量であるので
、均質な配合物が得られなかった。However, if the two were simply mixed in a predetermined ratio, a homogeneous blend could not be obtained because the amount of stevioside used was very small compared to the amount of sugar.
そこで、更にその配合方法について種々検討を行った結
果、砂糖粒上にステビオサイド系配糖体の静液を被覆さ
せ、これを破砕し、攪拌することによって上記欠陥を克
服することができた。Therefore, as a result of various studies on the blending method, it was possible to overcome the above-mentioned defects by coating sugar grains with a static solution of stevioside glycosides, crushing and stirring this.
本発明は砂糖の表面にステビオサイド系配糖体を、好適
に紘砂糖0.1〜0.4重量−被覆することにより、砂
糖の風味を減することのない甘味φ増加させた甘味料の
製法である。そして、更に、砂糖の表面にステビオサイ
ド系配糖体を被覆し、後これを破砕し攪拌するととによ
って、砂糖とステビオサイド系配糖体の配合割合が常に
均質な甘味料を得る方法である。The present invention provides a method for producing a sweetener that increases sweetness φ without reducing the flavor of sugar by coating the surface of sugar with stevioside glycosides, preferably by 0.1 to 0.4 weight of sugar. It is. Furthermore, the surface of sugar is coated with stevioside glycosides, which is then crushed and stirred, thereby obtaining a sweetener in which the blending ratio of sugar and stevioside glycosides is always uniform.
本発明に用いる砂糖は、結晶状9粒状等の形状を有する
白糖、双目糖等、何れでも使用することができる。The sugar used in the present invention can be any type of sugar, such as white sugar or double sugar, which has a crystalline nine-grain shape or the like.
本発明に使用するステビオサイド系配糖体は南米産のス
テビア レバクジアナ ベルトニ(St*via r@
baudlana BgRTONI )と呼ばれるキク
科の多年性植吻中に含まれる甘味成分で、ステビオール
をアグリコンとする配糖体で、ステビアの票から熱水、
アルコール、有機溶剤を用いて抽出し、イオン交換樹脂
、脱色樹脂などを用いて色、夷のある成分を除去するか
、又は合成吸着樹脂等Klk着し、溶離する等の方法で
精製される物質で、次の構造を有しているステビオール
をアゲ’)17とする配糖体が含まれる。The stevioside glycoside used in the present invention is Stevia revacdiana Bertoni (St*via r@
It is a sweet ingredient contained in the perennial proboscis of the Asteraceae family called baudlana BgRTONI). It is a glycoside whose aglycone is steviol.
Substances that are purified by extraction using alcohol or organic solvents, removing colored and opaque components using ion exchange resins, decolorizing resins, etc., or by adhering to synthetic adsorption resins, etc., and eluting them. This includes glycosides of steviol (17) having the following structure.
RIR。RIR.
ステビオサイド g l c g 1 /1
g1 cレバウディオ
ズルコサイドA glc gl♂−ham
レバクディオ
レバウディオ
サイドE gl/’glc gl♂’g l
cレパクディオ
ステビオルビオサイド Hg t t”g i
a本発明に用いる場合はこれらの配糖体の1種又は2種
以上の混合物を用いてもよいが、一般には市販のステビ
アの業から抽出した上記配糖体のステビオサイドを主成
分としたこれらステービオサイド系配糖体の混合物を用
いる。Stevioside g l c g 1 /1
g1 c Rebaudio Dulcoside A glc gl♂-ham
Revacdiorebaudioside E gl/'glc gl♂'g l
c Repak Diosteviolbioside Hg t t”g i
aWhen used in the present invention, one type or a mixture of two or more of these glycosides may be used, but in general, stevioside of the above glycosides extracted from commercially available stevia plants is generally used. A mixture of stabioside glycosides is used.
本発明の製法は、前記砂糖の結晶、粒状の原料に、前記
ステビオサイド系配糖体の水又はアルコール等の溶剤に
溶かした溶液を適宜の方法例えば噴霧器等により塗布す
る。なお、この場合、粘着剤として例えばアルギン賊プ
ロピレングリコールエステル、メチルセルローズ等をこ
の溶液中に加えて塗布すると砂糖に対する被蝋性が良好
になる。In the production method of the present invention, a solution of the stevioside glycoside dissolved in a solvent such as water or alcohol is applied to the sugar crystal or granular raw material using an appropriate method such as a sprayer. In this case, if an adhesive such as alginic propylene glycol ester or methyl cellulose is added to this solution and applied, the waxability against sugar will be improved.
なお、この溶液に′くえん酸、酢酸、こはく酸、シんご
酸、酒石酸、アスパラギン酸等の有機鉦、または、食塩
、シんご鍼ソーダ、こはく酸ソーダ、グルタンン酸ソー
ダ、イノシン酸ソーダ、グアニル戚ソーダ等の塩類を甘
味度の増強ないし甘味の質の調整に用いるために加えて
もよい。In addition, organic acid such as citric acid, acetic acid, succinic acid, sinlic acid, tartaric acid, aspartic acid, etc., or salt, ginger soda, sodium succinate, sodium glutanate, sodium inosinate, etc. are added to this solution. Salts such as guanyl-related soda may be added to enhance sweetness or adjust the quality of sweetness.
このステビオサイド系配糖体の使用量は、甘味の増加程
度による適宜変え得るものであるが、一般には砂糖10
0 fに対し0.1〜0.4fii&使用するのが好適
である。The amount of stevioside glycoside used can be changed as appropriate depending on the degree of increase in sweetness, but generally it is 10% sugar.
It is preferable to use 0.1 to 0.4 fii for 0 f.
以上の如くして砂糖表面にステビオナイド系配糖体を被
覆した甘味料は、原料として粒状の砂糖を用いた場合は
適宜の粉砕機により粉砕し粉状にして、これを混合する
と、砂゛糖とステビオサイド系配糖体の均質な混合物と
することができる。The sweetener whose sugar surface is coated with stevionide glycosides as described above can be obtained by pulverizing granular sugar using an appropriate grinder to form a powder, and then mixing it into a powder. and stevioside glycosides.
かくして得られた甘味料は、天然の砂糖とその形状、外
観、感触が殆んど同じであシ、その上、ステビオサイド
系配糖体の砂糖に対し、約200倍の甘味が添加された
ものであるから、従来の砂糖の摂取量の数10分の1で
十分甘味嗜好を満たすことができ、#糖摂取量の諷少、
即ち、砂糖の過剰摂取の防止に極めて有効に用いること
かで鳶る。The sweetener thus obtained has almost the same shape, appearance, and feel as natural sugar, and is about 200 times sweeter than stevioside glycoside sugar. Therefore, it is possible to satisfy the sweet taste preference with just a few tenths of the conventional amount of sugar intake.
In other words, it can be used extremely effectively to prevent excessive intake of sugar.
また、砂糖の表−にステビアサイド系配糖体を被覆して
後破砕した砂糖粉、粒はその表面に一定量のステビナサ
イド系配糖体が被着されているから、そのま\の状態で
使用すれば、常に甘味の増強された砂糖粉粒であり、単
に両者を混合した時イ
生ずるステビナサイド系配糖体の偏在を防止し、ひとつ
ひ≧つ両者を所定量ずつ混合した小包を作り、この単位
で使用する等の繁雑な手段を講する必要がない。In addition, sugar powder or granules that have been coated with steviaside glycosides on the surface and then crushed have a certain amount of steviaside glycosides coated on their surface, so they can be used as they are. When used, the sugar powder granules always have an enhanced sweetness, prevent the uneven distribution of stevinaside glycosides that occurs when simply mixing the two, and create packets in which a predetermined amount of each of the two is mixed. There is no need to take complicated measures such as using this unit.
次に本発明の実施例を示す。Next, examples of the present invention will be shown.
例
双目糖1kfを減圧装置を備えた容器に入れ、別に、ス
テビオサイド2,3を及びアルギン鍼プロピレン□グリ
コール1Of および食塩適量を水に溶かし丸線20
t を作り、この溶液を双目糖中に噴霧しつ\容器
内温を40〜60℃に加温し、減圧下で乾燥すると製品
1kfを得る。Example: Put 1 kf of sugar in a container equipped with a pressure reducing device, and separately, dissolve 2 and 3 stevioside, algin acupuncture propylene □ glycol 1 Of, and an appropriate amount of salt in water and make a round wire 20
t is prepared, this solution is sprayed into double sugar, the internal temperature of the container is heated to 40-60°C, and the product is dried under reduced pressure to obtain 1 kf of product.
爽に、このものを破砕機にかけ細粒化して製品とする。Afterwards, this material is crushed into fine particles and made into a product.
Claims (1)
とを41像とする甘味料の製法。 2、砂糖の表面にステビオナイド系配糖体を被覆し、後
これを破砕し攪拌することを特徴とする甘味料の製法。[Scope of Claims] 1. A method for producing a sweetener, which involves coating the surface of sugar with a stevioside glycoside. 2. A method for producing a sweetener, which comprises coating the surface of sugar with a stevionide glycoside, and then crushing and stirring this.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP56116966A JPS5820170A (en) | 1981-07-24 | 1981-07-24 | Preparation of sweetener |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP56116966A JPS5820170A (en) | 1981-07-24 | 1981-07-24 | Preparation of sweetener |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS5820170A true JPS5820170A (en) | 1983-02-05 |
Family
ID=14700151
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP56116966A Pending JPS5820170A (en) | 1981-07-24 | 1981-07-24 | Preparation of sweetener |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5820170A (en) |
Cited By (32)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS62220167A (en) * | 1986-03-20 | 1987-09-28 | Shinko Seito Kk | Low-caloric sugar containing stevia sweetener and production thereof |
EP2100519A1 (en) * | 2008-03-04 | 2009-09-16 | Tiense Suikerraffinaderij N.V. | Particle containing a high-intensity sweetener, process for preparation and use |
US20100227034A1 (en) * | 2005-10-11 | 2010-09-09 | Purkayastha Siddhartha | Process for Manufacturing a Sweetener and Use Thereof |
US20100255171A1 (en) * | 2005-10-11 | 2010-10-07 | Purkayastha Siddhartha | Process for Manufacturing a Sweetener and Use Thereof |
WO2011048616A3 (en) * | 2009-10-19 | 2011-06-16 | Intas Pharmaceuticals Limited | Healthy sugar and process for preparation of the same |
US20110244094A1 (en) * | 2010-03-31 | 2011-10-06 | Purecircle Sdn Bhd | Low calorie composite sweetener as sugar alternative and methods for producing the same |
WO2013082019A1 (en) * | 2011-11-28 | 2013-06-06 | Tate & Lyle Ingredients Americas Llc | Improved flavor natural table top sweetener |
US9615599B2 (en) | 2011-02-17 | 2017-04-11 | Purecircle Sdn Bhd | Glucosyl stevia composition |
US9752174B2 (en) | 2013-05-28 | 2017-09-05 | Purecircle Sdn Bhd | High-purity steviol glycosides |
US9771434B2 (en) | 2011-06-23 | 2017-09-26 | Purecircle Sdn Bhd | Products from stevia rebaudiana |
US9877501B2 (en) | 2011-06-03 | 2018-01-30 | Purecircle Sdn Bhd | Stevia composition |
US9894922B2 (en) | 2011-05-18 | 2018-02-20 | Purecircle Sdn Bhd | Glucosyl rebaudioside C |
US10004245B2 (en) | 2009-11-12 | 2018-06-26 | Purecircle Sdn Bhd | Granulation of a stevia sweetener |
US10021899B2 (en) | 2011-05-31 | 2018-07-17 | Purecircle Sdn Bhd | Stevia composition |
US10058112B2 (en) | 2014-11-21 | 2018-08-28 | Eco Sweeteners Llc | Sweetener composition including enzymatically processed stevia and method of manufacturing |
US10362797B2 (en) | 2011-02-10 | 2019-07-30 | Purecircle Sdn Bhd | Stevia composition |
KR20190128523A (en) * | 2018-05-08 | 2019-11-18 | 주식회사 삼양사 | Sugar composition including dietary fiber and method of preparing for the same |
US10480019B2 (en) | 2011-08-10 | 2019-11-19 | Purecircle Sdn Bhd | Process for producing high-purity rubusoside |
US10485257B2 (en) | 2012-05-22 | 2019-11-26 | Purecircle Sdn Bhd | Method of making steviol glycosides |
US10531683B2 (en) | 2005-10-11 | 2020-01-14 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
US10696706B2 (en) | 2010-03-12 | 2020-06-30 | Purecircle Usa Inc. | Methods of preparing steviol glycosides and uses of the same |
US10743572B2 (en) | 2011-02-17 | 2020-08-18 | Purecircle Sdn Bhd | Glucosylated steviol glycoside as a flavor modifier |
US10780170B2 (en) | 2013-06-07 | 2020-09-22 | Purecircle Sdn Bhd | Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier |
US10952458B2 (en) | 2013-06-07 | 2021-03-23 | Purecircle Usa Inc | Stevia extract containing selected steviol glycosides as flavor, salty and sweetness profile modifier |
US11202461B2 (en) | 2014-09-02 | 2021-12-21 | Purecircle Sdn Bhd | Stevia extracts |
US11291232B2 (en) | 2010-12-13 | 2022-04-05 | Purecircle Sdn Bhd | Highly soluble Rebaudioside D |
US11464246B2 (en) | 2011-09-07 | 2022-10-11 | Purecircle Sdn Bhd | Highly soluble Stevia sweetener |
US11647771B2 (en) | 2015-10-26 | 2023-05-16 | Purecircle Usa Inc. | Steviol glycoside compositions |
US11653686B2 (en) | 2015-12-15 | 2023-05-23 | Purecircle Usa Inc. | Steviol glycoside compositions |
US11678685B2 (en) | 2011-02-17 | 2023-06-20 | Purecircle Sdn Bhd | Glucosyl stevia composition |
US11690391B2 (en) | 2011-02-17 | 2023-07-04 | Purecircle Sdn Bhd | Glucosylated steviol glycoside as a flavor modifier |
US11871771B2 (en) | 2011-02-17 | 2024-01-16 | Purecircle Sdn Bhd | Glucosyl Stevia composition |
-
1981
- 1981-07-24 JP JP56116966A patent/JPS5820170A/en active Pending
Cited By (50)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS62220167A (en) * | 1986-03-20 | 1987-09-28 | Shinko Seito Kk | Low-caloric sugar containing stevia sweetener and production thereof |
US20100227034A1 (en) * | 2005-10-11 | 2010-09-09 | Purkayastha Siddhartha | Process for Manufacturing a Sweetener and Use Thereof |
US20100255171A1 (en) * | 2005-10-11 | 2010-10-07 | Purkayastha Siddhartha | Process for Manufacturing a Sweetener and Use Thereof |
US10531683B2 (en) | 2005-10-11 | 2020-01-14 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
US8334006B2 (en) * | 2005-10-11 | 2012-12-18 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
US8337927B2 (en) * | 2005-10-11 | 2012-12-25 | Purecircle Sdn Bhd | Process for manufacturing a sweetener and use thereof |
EP2100519A1 (en) * | 2008-03-04 | 2009-09-16 | Tiense Suikerraffinaderij N.V. | Particle containing a high-intensity sweetener, process for preparation and use |
WO2011048616A3 (en) * | 2009-10-19 | 2011-06-16 | Intas Pharmaceuticals Limited | Healthy sugar and process for preparation of the same |
US10004245B2 (en) | 2009-11-12 | 2018-06-26 | Purecircle Sdn Bhd | Granulation of a stevia sweetener |
US10696706B2 (en) | 2010-03-12 | 2020-06-30 | Purecircle Usa Inc. | Methods of preparing steviol glycosides and uses of the same |
US11155570B2 (en) | 2010-03-12 | 2021-10-26 | Purecircle Usa Inc. | Methods of preparing steviol glycosides and uses of the same |
US11773125B2 (en) | 2010-03-12 | 2023-10-03 | Purecircle Usa Inc. | Methods of preparing steviol glycosides and uses of the same |
US8591980B2 (en) | 2010-03-31 | 2013-11-26 | Purecircle Sdn Bhd | Low calorie composite sweetener as sugar alternative and methods for producing the same |
US8357417B2 (en) * | 2010-03-31 | 2013-01-22 | Purecircle Sdn Bhd | Low calorie composite sweetener as sugar alternative and methods for producing the same |
US20110244094A1 (en) * | 2010-03-31 | 2011-10-06 | Purecircle Sdn Bhd | Low calorie composite sweetener as sugar alternative and methods for producing the same |
US11950611B2 (en) | 2010-12-13 | 2024-04-09 | Purecircle Sdn Bhd | Highly soluble Rebaudioside D |
US11291232B2 (en) | 2010-12-13 | 2022-04-05 | Purecircle Sdn Bhd | Highly soluble Rebaudioside D |
US11856974B2 (en) | 2011-02-10 | 2024-01-02 | Purecircle Sdn Bhd | Highly soluble stevia sweetener |
US11812771B2 (en) | 2011-02-10 | 2023-11-14 | Purecircle Sdn Bhd | Stevia composition |
US10362797B2 (en) | 2011-02-10 | 2019-07-30 | Purecircle Sdn Bhd | Stevia composition |
US10743572B2 (en) | 2011-02-17 | 2020-08-18 | Purecircle Sdn Bhd | Glucosylated steviol glycoside as a flavor modifier |
US11871771B2 (en) | 2011-02-17 | 2024-01-16 | Purecircle Sdn Bhd | Glucosyl Stevia composition |
US9615599B2 (en) | 2011-02-17 | 2017-04-11 | Purecircle Sdn Bhd | Glucosyl stevia composition |
US11690391B2 (en) | 2011-02-17 | 2023-07-04 | Purecircle Sdn Bhd | Glucosylated steviol glycoside as a flavor modifier |
US11678685B2 (en) | 2011-02-17 | 2023-06-20 | Purecircle Sdn Bhd | Glucosyl stevia composition |
US11229228B2 (en) | 2011-02-17 | 2022-01-25 | Purecircle Sdn Bhd | Glucosyl stevia composition |
US9894922B2 (en) | 2011-05-18 | 2018-02-20 | Purecircle Sdn Bhd | Glucosyl rebaudioside C |
US11950610B2 (en) | 2011-05-18 | 2024-04-09 | Purecircle Sdn Bhd | Glucosyl Rebaudioside C |
US10021899B2 (en) | 2011-05-31 | 2018-07-17 | Purecircle Sdn Bhd | Stevia composition |
US11712055B2 (en) | 2011-05-31 | 2023-08-01 | Purecircle Sdn Bhd | Stevia composition |
US11825867B2 (en) | 2011-06-03 | 2023-11-28 | Purecircle Sdn Bhd | Stevia composition |
US9877501B2 (en) | 2011-06-03 | 2018-01-30 | Purecircle Sdn Bhd | Stevia composition |
US9771434B2 (en) | 2011-06-23 | 2017-09-26 | Purecircle Sdn Bhd | Products from stevia rebaudiana |
US11279773B2 (en) | 2011-06-23 | 2022-03-22 | Purecircle Sdn Bhd | Products from Stevia rabaudiana |
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