JPS58116480A - ２−メチル−２（４′−フルオロフエニル）−４−イソプロピル−５，５−ジチメル−１，３−ジオキサンおよびその製法 - Google Patents
２−メチル−２（４′−フルオロフエニル）−４−イソプロピル−５，５−ジチメル−１，３−ジオキサンおよびその製法Info
- Publication number
- JPS58116480A JPS58116480A JP56214417A JP21441781A JPS58116480A JP S58116480 A JPS58116480 A JP S58116480A JP 56214417 A JP56214417 A JP 56214417A JP 21441781 A JP21441781 A JP 21441781A JP S58116480 A JPS58116480 A JP S58116480A
- Authority
- JP
- Japan
- Prior art keywords
- oil
- dimethyl
- methyl
- fluorophenyl
- isopropyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- VUFAESJFUZNFBG-UHFFFAOYSA-N 2-(4-fluorophenyl)-2,5,5-trimethyl-4-propan-2-yl-1,3-dioxane Chemical compound O1CC(C)(C)C(C(C)C)OC1(C)C1=CC=C(F)C=C1 VUFAESJFUZNFBG-UHFFFAOYSA-N 0.000 title 1
- 150000001875 compounds Chemical class 0.000 claims abstract description 10
- ZDPAWHACYDRYIW-UHFFFAOYSA-N 1-(4-fluorophenyl)ethanone Chemical compound CC(=O)C1=CC=C(F)C=C1 ZDPAWHACYDRYIW-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000000034 method Methods 0.000 claims abstract 2
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 150000002009 diols Chemical class 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract description 15
- 238000006297 dehydration reaction Methods 0.000 abstract description 6
- 239000002904 solvent Substances 0.000 abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 3
- 239000000654 additive Substances 0.000 abstract description 2
- 230000000996 additive effect Effects 0.000 abstract description 2
- 238000009835 boiling Methods 0.000 abstract description 2
- 230000018044 dehydration Effects 0.000 abstract description 2
- 239000012530 fluid Substances 0.000 abstract description 2
- 238000007710 freezing Methods 0.000 abstract description 2
- 230000008014 freezing Effects 0.000 abstract description 2
- 238000010438 heat treatment Methods 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 abstract description 2
- 239000000463 material Substances 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 abstract 2
- JCTXKRPTIMZBJT-UHFFFAOYSA-N 2,2,4-trimethylpentane-1,3-diol Chemical compound CC(C)C(O)C(C)(C)CO JCTXKRPTIMZBJT-UHFFFAOYSA-N 0.000 abstract 1
- KTPJXHGORSBVNN-UHFFFAOYSA-N 2-(4-fluorophenyl)-5,5-dimethyl-4-propan-2-yl-1,3-dioxane Chemical compound FC1=CC=C(C=C1)C1OCC(C(O1)C(C)C)(C)C KTPJXHGORSBVNN-UHFFFAOYSA-N 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000000314 lubricant Substances 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 5
- 239000003849 aromatic solvent Substances 0.000 description 3
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- -1 cyclic acetal Chemical class 0.000 description 2
- 230000032050 esterification Effects 0.000 description 2
- 238000005886 esterification reaction Methods 0.000 description 2
- 238000004817 gas chromatography Methods 0.000 description 2
- 239000000976 ink Substances 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- 239000012159 carrier gas Substances 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 239000010687 lubricating oil Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
Landscapes
- Lubricants (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP56214417A JPS58116480A (ja) | 1981-12-28 | 1981-12-28 | ２−メチル−２（４′−フルオロフエニル）−４−イソプロピル−５，５−ジチメル−１，３−ジオキサンおよびその製法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP56214417A JPS58116480A (ja) | 1981-12-28 | 1981-12-28 | ２−メチル−２（４′−フルオロフエニル）−４−イソプロピル−５，５−ジチメル−１，３−ジオキサンおよびその製法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS58116480A true JPS58116480A (ja) | 1983-07-11 |
| JPS6245232B2 JPS6245232B2 (enrdf_load_stackoverflow) | 1987-09-25 |
Family
ID=16655438
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP56214417A Granted JPS58116480A (ja) | 1981-12-28 | 1981-12-28 | ２−メチル−２（４′−フルオロフエニル）−４−イソプロピル−５，５−ジチメル−１，３−ジオキサンおよびその製法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS58116480A (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100727997B1 (ko) | 2005-10-10 | 2007-06-13 | 삼성전자주식회사 | 고리형 디에테르 화합물 또는 고리형 디티오란 화합물을포함하는 잉크젯 잉크 조성물 |
-
1981
- 1981-12-28 JP JP56214417A patent/JPS58116480A/ja active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100727997B1 (ko) | 2005-10-10 | 2007-06-13 | 삼성전자주식회사 | 고리형 디에테르 화합물 또는 고리형 디티오란 화합물을포함하는 잉크젯 잉크 조성물 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6245232B2 (enrdf_load_stackoverflow) | 1987-09-25 |
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