JPS58114722A - Powder discharging method in fluidized treating chamber - Google Patents

Powder discharging method in fluidized treating chamber

Info

Publication number
JPS58114722A
JPS58114722A JP21571681A JP21571681A JPS58114722A JP S58114722 A JPS58114722 A JP S58114722A JP 21571681 A JP21571681 A JP 21571681A JP 21571681 A JP21571681 A JP 21571681A JP S58114722 A JPS58114722 A JP S58114722A
Authority
JP
Japan
Prior art keywords
powder
gas
pressurized gas
fluidized
pipeline
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP21571681A
Other languages
Japanese (ja)
Other versions
JPS646814B2 (en
Inventor
Goichi Sagawa
佐川 悟一
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toray Engineering Co Ltd
Original Assignee
Toray Engineering Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Toray Engineering Co Ltd filed Critical Toray Engineering Co Ltd
Priority to JP21571681A priority Critical patent/JPS58114722A/en
Publication of JPS58114722A publication Critical patent/JPS58114722A/en
Publication of JPS646814B2 publication Critical patent/JPS646814B2/ja
Granted legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015Feeding of the particles in the reactor; Evacuation of the particles out of the reactor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)

Abstract

PURPOSE:To discharge powder thoroughly from the inside of a fluidized treating tank by introducing a pressurized gas into a treating chamber through a gas diffusing plate, and ejecting the pressurized gas from agitating vanes in the treating chamber while rotating said vanes thereby fluidizing the powder. CONSTITUTION:A prescribed pressurized gas is supplied through a gas supply pipeline 6 into a pressure chamber 5, and is diffused uniformity with a gas diffusing plate 2 so as to be admitted into a treating chamber 3 and to fluidize powder 8. The powder is treated by maintaining the same at prescribed temp. In discharging the powder 8 after the treatment, a plug body 9 closing a discharge pipeline 7 is removed. In this stage, the powder 8 is fluidized by the pressurized gas from the pipeline 6 and while a agitating vanes 4 are rotated with a prime mover 10, the pressurized gas of the same kind as that of said pressurized gas from a gas supply pipeline 12 is ejected from the vanes 4 through a hollow shaft 11. Then, the entire amt. of the powder 8 in the chamber 3 is fluidized and is fed forcibly into the pipeline 7 opened to the plate 2 through which the powder is discharged.

Description

【発明の詳細な説明】 本発明は流動化処理槽における粉体排出方法に関するも
のである。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a method for discharging powder in a fluidization treatment tank.

従来から流動化処理槽を用いて粉体の乾燥、還元など各
種の処理が行なわれているが、処理後槽内から粉体を排
出する際に残留粉体が発生するのを防止するために、ガ
ス分散板の下方に構成されている圧力室に加圧ガスを供
給して粉体を流動化させながら前記分散板に開口されて
いる排出管路に送り込む方法や、あるいは前記分散板の
上方に構成されている処理室内で攪拌翼を回転させて粉
体を攪拌しなから前記排出管路に送り込む方法など各種
の方法が試みられている。
Various treatments such as drying and reduction of powder have traditionally been carried out using a fluidization treatment tank, but in order to prevent residual powder from being generated when the powder is discharged from the tank after treatment. , a method of supplying pressurized gas to a pressure chamber configured below a gas distribution plate to fluidize the powder and feeding it into a discharge pipe opened in the distribution plate, or a method above the distribution plate. Various methods have been tried, such as a method in which powder is stirred by rotating a stirring blade in a processing chamber configured as described above and then fed into the discharge pipe.

しかしながらこれらいずれの方法においても完全に粉体
を排出することができず、ある程度の量の残留は無視せ
ざるを得なかった。
However, in any of these methods, the powder could not be completely discharged, and a certain amount of residual powder had to be ignored.

すなわち前述した加圧ガス供給方法による場合において
は、粉体の残留量が次第に少なくなって来るとガスが部
分的に吹き抜けを起し、残部を完全に排出することかで
きないと共にガス供給量をあまり増加させる・と、この
ガスに粉体が同伴されて運ばれるために排ガス処理が困
難となる欠点かあった。
In other words, in the case of using the pressurized gas supply method described above, when the amount of residual powder gradually decreases, the gas partially blows through, making it impossible to completely exhaust the remaining part and not reducing the amount of gas supplied too much. However, when the amount of waste gas increases, powder is carried along with the gas, making it difficult to treat the exhaust gas.

また前述した攪拌翼回転方法による場合においては、翼
が回転している領域及びその近辺に存在する粉体は排出
することかできても、その他の領域に存在する粉体を排
出することができない欠点があった。
Furthermore, in the case of using the above-mentioned stirring blade rotation method, although it is possible to discharge the powder present in and around the area where the blade is rotating, it is not possible to discharge the powder present in other areas. There were drawbacks.

なお安全上から前記翼をガス分散板にあまり接近させて
配すことができないので、この翼にゴム材等の可撓性材
でスカート部を付設し、これでガス分散板の上面をこす
るようにして排出することも試みられているが、この場
合においてもガス分散板と槽内壁とで形成される角部に
存在する粉体を完全に排出することができず、かつこの
ようなスカート部を付設すると処理に際して粉体の均一
流動化を妨げることになると共に処理中にこの材から異
質のガスが発生する可能があるので広範囲な応用ができ
ないという欠点かあった。
For safety reasons, it is not possible to place the blade too close to the gas distribution plate, so a skirt made of a flexible material such as a rubber material is attached to the blade, and the skirt part is used to rub the top surface of the gas distribution plate. Attempts have been made to discharge the powder in this way, but even in this case, it is not possible to completely discharge the powder present at the corner formed by the gas distribution plate and the inner wall of the tank, and Adding a section to the material impedes uniform fluidization of the powder during processing, and there is a possibility that foreign gas may be generated from the material during processing, so it cannot be used in a wide range of applications.

上述のような流動化処理槽における粉体の残留は、殊に
、流動化性に劣る性質の粉体を処理する場合、及び処理
すると流動化性に劣る性質に変化する粉体などを処理す
る場合において顕著である。
The above-mentioned residual powder in the fluidization treatment tank is particularly important when processing powders with poor fluidization properties, or when processing powders that change to poor fluidization properties upon processing. This is noticeable in some cases.

本発明はこのような従来方法の欠点に鑑みて発明された
ものであり、その目的とするところは、流動化処理槽内
から完全に粉体を排出することができる方法を得ようと
するにある。
The present invention was invented in view of the shortcomings of the conventional methods, and its purpose is to provide a method that can completely discharge powder from the fluidization treatment tank. be.

この目的を達成する本発明に係る流動化処理槽における
粉体排出方法は、ガス分散板の下方に構成されている圧
力室に加圧ガスを供給して前記分散板の上方に構成され
ている処理室内に導入せしめると共に前記処理室内に配
されている攪拌翼を回転させ、かつこの翼から加圧ガス
を噴出させて前記処理室内の粉体を流動化しながら前記
分散板に開口されている排出管路に強制的に送り込むこ
とを特徴とするものである。
A method for discharging powder in a fluidization treatment tank according to the present invention that achieves this objective includes supplying pressurized gas to a pressure chamber configured below a gas distribution plate and configured above the distribution plate. The powder in the processing chamber is introduced into the processing chamber, and a stirring blade disposed in the processing chamber is rotated, and pressurized gas is ejected from the blade to fluidize the powder in the processing chamber while discharging the powder through the dispersion plate. It is characterized by forcibly feeding it into the pipe.

以下、実施例に基づいて本発明を詳述するに第1図にお
いて、流動化処理槽は、円筒状の槽本体(1)内にガス
分散板(21を固定して上下2室に区分し、その上方の
処理室(3)内に攪拌翼+41を配すと共にその下方の
圧力室(5)にガス供給管路(6)を開口し、さらにガ
ス分散板(2)に排出管路(7)を開口している。なお
、処理する粉体(8)は図示しない管路を介して槽本体
(1)の上部から処理室(3)内へ供給される。
Hereinafter, the present invention will be described in detail based on an example. In FIG. 1, a fluidization treatment tank is divided into two upper and lower chambers by fixing a gas distribution plate (21) inside a cylindrical tank body (1). , a stirring blade +41 is arranged in the processing chamber (3) above it, a gas supply pipe (6) is opened in the pressure chamber (5) below it, and a discharge pipe (6) is arranged in the gas distribution plate (2). 7) is opened.The powder (8) to be treated is supplied into the processing chamber (3) from the upper part of the tank body (1) via a pipe line (not shown).

処理するに当って、ガス供給管路(6)から圧力室+5
1へ所定に加圧されたガスが供給されるか、このガスは
処理目的に対応して各種のものが適宜に選択され、たと
えばエアーガス、不活性ガスなどかあげられる。そして
処理室で3)内の粉体(8)はガス分散板(2)で均一
に分散されて処理室(3)内に流入して来る前記ガスに
よって流動化されかつ図示しない加熱手段または冷却手
段により所定温度に保たれて処理される。
During processing, the pressure chamber +5 from the gas supply pipe (6)
1 is supplied with a predetermined pressurized gas, or various gases are appropriately selected depending on the processing purpose, such as air gas, inert gas, etc. Then, in the processing chamber, the powder (8) in 3) is uniformly dispersed by the gas distribution plate (2) and fluidized by the gas flowing into the processing chamber (3), and is heated or cooled by heating means (not shown). It is maintained at a predetermined temperature by a means for processing.

処理後、この粉体(8)を排出するに当り、排出管路(
7)を閉塞している栓体(9)が取り除かれる。
After treatment, to discharge this powder (8), the discharge pipe (
7) is removed.

この際、ガス供給管路(6)から圧力室(5)へ供給さ
れる前記加圧ガスによって粉体(8)が流動化されると
共に、原動装置(IIによって回転される攪拌翼(4)
により攪拌され、かつこの攪拌l114+から前記加圧
ガスと同種の加圧ガスが噴出される。
At this time, the powder (8) is fluidized by the pressurized gas supplied from the gas supply pipe (6) to the pressure chamber (5), and the stirring blade (4) rotated by the prime mover (II)
The same type of pressurized gas as the pressurized gas is ejected from this stirring l114+.

攪拌翼(4)は第2図において詳細構造を示すように、
原動装’ 11(lで回転駆動される中空軸anの下端
に固定された分岐管体(4a)と、これに傾斜(傾斜角
度θ=3°)されて固定された短管体(4b)とで構成
され、中空軸at+内を流れて来る加圧ガスが分岐管体
(4a)を経て短管体(4b)に穿設されているノズル
孔(4C)群から噴出しつるように設けられている。な
お中空軸aD内への加圧ガスの供給はガス供給管路(1
2から行なわれる。第3甲においてその詳細構造を示す
ように、中空軸aUとガス供給管路aりとがグランドバ
ッキングa3、ケーシングaΦなどで構成される軸封機
構を介して係合され、前記ケーシングOaにガス供給管
路α2が螺結されていると共に中空軸回に孔α9が穿設
されているので、前記管路03から回転されている中空
軸aD内へ加圧ガスを供給することかできる。
As the detailed structure of the stirring blade (4) is shown in Fig. 2,
A branch pipe body (4a) fixed to the lower end of a hollow shaft an which is rotationally driven by the prime mover '11 (l), and a short pipe body (4b) fixed at an inclination (angle of inclination θ=3°) to the branch pipe body (4a). The pressurized gas flowing through the hollow shaft at+ is ejected from a group of nozzle holes (4C) bored in the short pipe body (4b) via the branch pipe body (4a). The pressurized gas is supplied into the hollow shaft aD through the gas supply pipe (1
It is carried out from 2. As shown in the detailed structure in Part A, the hollow shaft aU and the gas supply pipe a are engaged via a shaft sealing mechanism composed of a ground backing a3, a casing aΦ, etc. Since the supply pipe α2 is screwed and the hole α9 is bored in the hollow shaft, pressurized gas can be supplied from the pipe 03 into the rotating hollow shaft aD.

而して処理室(3)内の粉体(8)は、ガス分散板+2
1を通過して来る加圧ガスと、攪拌1!tf41による
攪拌と、この翼(41から噴出される加圧ガスとによっ
てその全量が流動化され、ガス分散板(2)に開口され
ている排出管路(7)に強制的に送り込まれて排出され
る。
Therefore, the powder (8) in the processing chamber (3) is
Pressurized gas passing through 1 and stirring 1! The entire amount is fluidized by the stirring by tf41 and the pressurized gas ejected from this blade (41), and is forcibly sent to the discharge pipe (7) opened to the gas distribution plate (2) and discharged. be done.

すなわちガス分散板(2)の下方から処理室(3)内へ
流入して来る加圧ガスによってほとんどの粉体(8)が
流動化されるが、これでは流動化されない粉体が攪拌翼
(4)から噴射される加圧ガスによって流動化され、そ
してこの際、攪拌翼(4)による攪拌により前記・流動
化が促進され、而して残留粉体を発生することなく完全
に排出することができる。
That is, most of the powder (8) is fluidized by the pressurized gas flowing into the processing chamber (3) from below the gas distribution plate (2), but the powder that is not fluidized is The powder is fluidized by the pressurized gas injected from 4), and at this time, the fluidization is promoted by stirring by the stirring blade (4), and the powder is completely discharged without generating any residual powder. I can do it.

なお本発明においては、攪拌翼(4)とガス分散板(2
)との間隙は出来る限り小さくする方が好ましいが、一
般には1(111〜50m位であればよい。また攪拌@
 +41と槽内壁との間隙も出来る限り小さくする方が
好ましいが、一般には10藺〜2011位であればよい
。そして、攪拌翼(4)の回転は一方々向に、あるいは
−・定もしくはランダムサイクルで反対方向に回転させ
てもよく、史に攪拌機を上下動しつるように設けてもよ
い。
In addition, in the present invention, the stirring blade (4) and the gas distribution plate (2
) It is preferable to make the gap as small as possible, but generally it is sufficient if it is 1 (about 111 to 50 m).
It is preferable to make the gap between +41 and the inner wall of the tank as small as possible, but in general, the gap should be between 10 and 2011. The stirring blade (4) may be rotated in one direction or in the opposite direction in a constant or random cycle, or the stirring blade may be provided so as to be able to move up and down.

その他、翼の枚数及び形状、ノズル孔の数などは適宜に
選択される。
In addition, the number and shape of the blades, the number of nozzle holes, etc. are selected as appropriate.

なおノズル孔はガス分散板に対し加圧ガスを吹付けるこ
とかできるように設けるのか好ましく、かつ槽内壁に対
しても吹付けることができるように設ければ史に好まし
い。
Preferably, the nozzle holes are provided so that the pressurized gas can be sprayed onto the gas distribution plate, and it is also preferable if the nozzle holes are provided so that the pressurized gas can also be sprayed onto the inner wall of the tank.

ガス分散板は第1図に示すように排出口に向って傾斜さ
せて設けるのが好ましいか、これに限定されず水平に設
けてもよい。
It is preferable that the gas distribution plate be provided inclined toward the discharge port as shown in FIG. 1, but it is not limited thereto, and may be provided horizontally.

第1図に示す流動化処理槽において、直径か3001の
処理室(3)内に微細なアルミナ粒25Kgを充填し、
ガス供給管路(6)から0.2 Kg/cyjの加圧エ
アーを45 Nrd/Hrで供給すると共に攪拌翼(4
)を100 r、pmで回転させ、かつこの翼(4)か
ら8 Nnf/Hrで0.5象−の加圧エアーを噴出し
、栓体(9)を取り除いて前記アルミナ粒の排出を行っ
たとこる完全に排出することができた。
In the fluidization treatment tank shown in FIG.
Pressurized air of 0.2 Kg/cyj was supplied from the gas supply pipe (6) at 45 Nrd/Hr, and at the same time, the stirring blade (4
) was rotated at 100 r and pm, and 0.5 squares of pressurized air was blown out from the blade (4) at 8 Nnf/Hr to remove the plug (9) and discharge the alumina particles. I was able to completely drain it.

なお、回転している前記具(4)から加圧エアーを噴出
させない場合においてはtSW残留した。
In addition, when pressurized air was not blown out from the rotating tool (4), tSW remained.

また前記具(4)を回転させないと共にこれから   
  1加圧エアーを噴出させない場合においては3.2
即残留した。
Also, do not rotate the tool (4) and
1 3.2 when pressurized air is not blown out
It remained immediately.

以上述べたように、本発明によれば流動化処理槽内から
完全に粉体を排出することができる方法が得られる。
As described above, according to the present invention, a method is provided in which powder can be completely discharged from the fluidization treatment tank.

【図面の簡単な説明】[Brief explanation of drawings]

第1図は流動化処理槽の概略構成因、第2図は攪拌@ 
141の詳細図、第3図は中空軸onとガス供給管路a
2との係合部の詳細図である。 (2):ガス分散板、(31:処理室 (4):攪拌翼  、+51:圧力室 +61 、 a2:ガス供給管路、+71:排出管路第
1図
Figure 1 shows the schematic structure of the fluidization treatment tank, Figure 2 shows the stirring @
Detailed view of 141, Figure 3 shows the hollow shaft on and gas supply pipe a
FIG. 2 is a detailed view of the engaging portion with . (2): Gas distribution plate, (31: Processing chamber (4): Stirring blade, +51: Pressure chamber +61, a2: Gas supply pipe, +71: Discharge pipe Fig. 1)

Claims (1)

【特許請求の範囲】[Claims] (1)ガス分散板の下方に構成されている圧力室に加圧
ガスを供給して前記分散板の上方に構成されている処理
室内へ導入せしめると共に、前記処理室内に配されてい
る攪拌翼を回転させ、かつこの翼から加圧ガスを噴出さ
せて前記処理室内の粉体を流動化しながら 前記分散板
に開口されている排出管路に強制的に送り込むことを特
徴とする流動化処理槽における粉体排出方法。
(1) Pressurized gas is supplied to a pressure chamber configured below the gas distribution plate and introduced into the processing chamber configured above the distribution plate, and a stirring blade disposed within the processing chamber. The fluidization processing tank is characterized in that the powder in the processing chamber is fluidized by rotating and jetting pressurized gas from the blades, while forcibly feeding the powder into a discharge pipe opened in the dispersion plate. powder discharge method.
JP21571681A 1981-12-28 1981-12-28 Powder discharging method in fluidized treating chamber Granted JPS58114722A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP21571681A JPS58114722A (en) 1981-12-28 1981-12-28 Powder discharging method in fluidized treating chamber

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP21571681A JPS58114722A (en) 1981-12-28 1981-12-28 Powder discharging method in fluidized treating chamber

Publications (2)

Publication Number Publication Date
JPS58114722A true JPS58114722A (en) 1983-07-08
JPS646814B2 JPS646814B2 (en) 1989-02-06

Family

ID=16676987

Family Applications (1)

Application Number Title Priority Date Filing Date
JP21571681A Granted JPS58114722A (en) 1981-12-28 1981-12-28 Powder discharging method in fluidized treating chamber

Country Status (1)

Country Link
JP (1) JPS58114722A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63274448A (en) * 1987-04-30 1988-11-11 Nitta Zerachin Kk Method of supplying powder
JPH02157033A (en) * 1988-12-09 1990-06-15 Nisshin Flour Milling Co Ltd Powder diffuser
CN115228389A (en) * 2022-07-26 2022-10-25 青岛海湾化工设计研究院有限公司 Reactor capable of improving heat transfer capacity

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63274448A (en) * 1987-04-30 1988-11-11 Nitta Zerachin Kk Method of supplying powder
JPH02157033A (en) * 1988-12-09 1990-06-15 Nisshin Flour Milling Co Ltd Powder diffuser
CN115228389A (en) * 2022-07-26 2022-10-25 青岛海湾化工设计研究院有限公司 Reactor capable of improving heat transfer capacity

Also Published As

Publication number Publication date
JPS646814B2 (en) 1989-02-06

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