JPS5773195A - Production of aluminum powder - Google Patents
Production of aluminum powderInfo
- Publication number
- JPS5773195A JPS5773195A JP55147561A JP14756180A JPS5773195A JP S5773195 A JPS5773195 A JP S5773195A JP 55147561 A JP55147561 A JP 55147561A JP 14756180 A JP14756180 A JP 14756180A JP S5773195 A JPS5773195 A JP S5773195A
- Authority
- JP
- Japan
- Prior art keywords
- electrolytic bath
- powder
- mixture
- bath
- electrolytic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
- C01B21/072—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with aluminium
- C01B21/0722—Preparation by direct nitridation of aluminium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Electrolytic Production Of Metals (AREA)
- Solid-Phase Diffusion Into Metallic Material Surfaces (AREA)
- Ceramic Products (AREA)
Abstract
PURPOSE: To produce Al powder having properties meeting applications at a low cost by electrolyzing a molten salt electrolytic bath consisting essentially of AlCl3 at low temps. to deposit Al, mixing this with the inside of the electrolytic bath and filtering the same then refining this by filtration using a specific solvent.
CONSTITUTION: A molten salt electrolytic bath consisting essentially of AlCl3 is electrolyzed at low temps. to deposit Al on cathode. The deposited Al is separated from the electrode by circulating the electrolytic bath or giving impact to the electrode, and is mixed with the inside of the electrolytic bath. This mixture is filtered, whereby the cake-like Al stuck with the bath component as residual material on the filter film is obtained. Next, the residual materials are mixed in a solvent dissolving only the stuck bath components without dissolving the Al, and the mixture is agitated vigorously. After the agitation, the mixture is again filtered, whereby the second residual material is obtained. This is refined and dried, whereby Al powder is produced. In this method, the suitable Al powder meeting applications is obtained by controlling electrolytic conditions and electrolytic bath components.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55147561A JPS5773195A (en) | 1980-10-23 | 1980-10-23 | Production of aluminum powder |
DE19863641754 DE3641754A1 (en) | 1980-10-23 | 1986-12-06 | Process for preparing aluminium nitride powder |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55147561A JPS5773195A (en) | 1980-10-23 | 1980-10-23 | Production of aluminum powder |
DE19863641754 DE3641754A1 (en) | 1980-10-23 | 1986-12-06 | Process for preparing aluminium nitride powder |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS5773195A true JPS5773195A (en) | 1982-05-07 |
Family
ID=39327296
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP55147561A Pending JPS5773195A (en) | 1980-10-23 | 1980-10-23 | Production of aluminum powder |
Country Status (2)
Country | Link |
---|---|
JP (1) | JPS5773195A (en) |
DE (1) | DE3641754A1 (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH01104793A (en) * | 1987-10-15 | 1989-04-21 | Nisshin Steel Co Ltd | Vatting method for nonaqueous electrolytic aluminizing bath |
JP2014077188A (en) * | 2012-10-12 | 2014-05-01 | Sumitomo Electric Ind Ltd | Method and apparatus for producing aluminum powder, and aluminum powder |
CN103966631A (en) * | 2014-03-28 | 2014-08-06 | 郭昭华 | High-purity aluminum powder preparation equipment and method for preparing high-purity aluminum powder by same |
CN110846689A (en) * | 2019-11-05 | 2020-02-28 | 东北大学 | Method for preparing aluminum powder by taking aluminum/aluminum alloy as raw material |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR900007723A (en) * | 1988-11-29 | 1990-06-01 | 뽈 제이 레미욱스 | Aluminium Nitride And Method Of Manufacturing The Same |
DE69636580T2 (en) * | 1996-12-26 | 2007-08-23 | Toyota Jidosha Kabushiki Kaisha, Toyota | PROCESS FOR PREPARING ALUMINUM NITRIDE |
CA2247339C (en) * | 1996-12-26 | 2001-10-16 | Toyota Jidosha Kabushiki Kaisha | Process for producing aluminum nitride |
JP4729180B2 (en) * | 2001-02-02 | 2011-07-20 | 株式会社茨木研究所 | Method for producing aluminum nitride |
JP3891076B2 (en) * | 2001-11-13 | 2007-03-07 | 株式会社茨木研究所 | Method for producing aluminum nitride |
CN105271139B (en) * | 2015-04-21 | 2017-07-11 | 四川展祥特种合金科技有限公司 | A kind of atomization prepares the device of aluminium nitride powder |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS4843774A (en) * | 1971-10-07 | 1973-06-23 | ||
JPS52143909A (en) * | 1976-05-26 | 1977-11-30 | Yoshishige Tsumura | Modification of low temperature aluminium electrolysis |
-
1980
- 1980-10-23 JP JP55147561A patent/JPS5773195A/en active Pending
-
1986
- 1986-12-06 DE DE19863641754 patent/DE3641754A1/en not_active Withdrawn
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS4843774A (en) * | 1971-10-07 | 1973-06-23 | ||
JPS52143909A (en) * | 1976-05-26 | 1977-11-30 | Yoshishige Tsumura | Modification of low temperature aluminium electrolysis |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH01104793A (en) * | 1987-10-15 | 1989-04-21 | Nisshin Steel Co Ltd | Vatting method for nonaqueous electrolytic aluminizing bath |
JP2623482B2 (en) * | 1987-10-15 | 1997-06-25 | 日新製鋼株式会社 | Building equipment for non-aqueous solution electric aluminum plating bath |
JP2014077188A (en) * | 2012-10-12 | 2014-05-01 | Sumitomo Electric Ind Ltd | Method and apparatus for producing aluminum powder, and aluminum powder |
CN103966631A (en) * | 2014-03-28 | 2014-08-06 | 郭昭华 | High-purity aluminum powder preparation equipment and method for preparing high-purity aluminum powder by same |
CN103966631B (en) * | 2014-03-28 | 2016-09-07 | 郭昭华 | High-purity aluminium powder producing equipment and the method utilizing its high purity aluminium powder |
CN110846689A (en) * | 2019-11-05 | 2020-02-28 | 东北大学 | Method for preparing aluminum powder by taking aluminum/aluminum alloy as raw material |
Also Published As
Publication number | Publication date |
---|---|
DE3641754A1 (en) | 1988-06-16 |
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