JPS568360A - Purification of caprolactam - Google Patents
Purification of caprolactamInfo
- Publication number
- JPS568360A JPS568360A JP8297280A JP8297280A JPS568360A JP S568360 A JPS568360 A JP S568360A JP 8297280 A JP8297280 A JP 8297280A JP 8297280 A JP8297280 A JP 8297280A JP S568360 A JPS568360 A JP S568360A
- Authority
- JP
- Japan
- Prior art keywords
- caprolactam
- purification
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 title 2
- 238000000746 purification Methods 0.000 title 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/16—Separation or purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19792926279 DE2926279A1 (de) | 1979-06-29 | 1979-06-29 | Verfahren zur reinigung von caprolactam |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS568360A true JPS568360A (en) | 1981-01-28 |
| JPH0223544B2 JPH0223544B2 (OSRAM) | 1990-05-24 |
Family
ID=6074484
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP8297280A Granted JPS568360A (en) | 1979-06-29 | 1980-06-20 | Purification of caprolactam |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US4301073A (OSRAM) |
| EP (1) | EP0022161B1 (OSRAM) |
| JP (1) | JPS568360A (OSRAM) |
| CA (1) | CA1138865A (OSRAM) |
| DE (2) | DE2926279A1 (OSRAM) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2016505580A (ja) * | 2012-12-19 | 2016-02-25 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | シクロヘキサノンオキシムのベックマン転位からの精製カプロラクタムの製造方法 |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL8003365A (nl) * | 1980-06-10 | 1982-01-04 | Stamicarbon | Werkwijze voor het zuiveren van 2-pyrrolidon. |
| NL8102280A (nl) * | 1981-05-09 | 1982-12-01 | Stamicarbon | Werkwijze voor het zuiveren van epsilon-caprolactam. |
| IT1173261B (it) * | 1984-02-08 | 1987-06-18 | Snia Bpd Spa | Procedimento di purificazione del caprolattame |
| DE3729853A1 (de) * | 1987-09-05 | 1989-03-23 | Basf Ag | Verfahren zur aufarbeitung von destillationsrueckstaenden, die bei der reinigung von caprolactam anfallen |
| DE3735054A1 (de) * | 1987-10-16 | 1989-04-27 | Basf Ag | Verfahren zur gewinnung von caprolactam aus leichtsiedern oder schwersiedern der caprolactamdestillation oder gemischen derselben |
| US5458740A (en) * | 1994-03-04 | 1995-10-17 | Basf Corporation | Process for the purification of crude caprolactam |
| DE19500041A1 (de) * | 1995-01-03 | 1996-07-04 | Basf Ag | Verfahren zur kontinuierlichen Reinigung von aus 6-Aminocapronitril hergestelltem Roh-Caprolactam |
| US5990306A (en) * | 1997-09-03 | 1999-11-23 | Alliedsignal Inc. | Process for the purification of caprolactam obtained from the depolymerization of polyamide-containing carpet |
| DE10021191A1 (de) * | 2000-05-03 | 2001-11-08 | Basf Ag | Verfahren zur Herstellung eines Polymers unter Verwendung von Caprolactam |
| FR2809395B1 (fr) * | 2000-05-26 | 2002-07-19 | Rhodia Polyamide Intermediates | Procede de purification de lactames |
| US7022844B2 (en) | 2002-09-21 | 2006-04-04 | Honeywell International Inc. | Amide-based compounds, production, recovery, purification and uses thereof |
| DE10253095A1 (de) * | 2002-11-13 | 2004-06-17 | Basf Ag | Verfahren zur Reinigung von Caprolactam |
| US8841445B2 (en) | 2012-12-19 | 2014-09-23 | Basf Se | Process for preparing purified caprolactam from the Beckmann rearrangement of cyclohexane oxime |
| CN104557705B (zh) * | 2013-10-15 | 2017-06-09 | 中国石油化工股份有限公司 | 一种己内酰胺精制的方法和装置 |
| CN111138362A (zh) * | 2020-01-13 | 2020-05-12 | 福建永荣科技有限公司 | 一种己内酰胺精制工序粗苯蒸馏残液处理的方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5337685A (en) * | 1976-09-15 | 1978-04-06 | Bayer Ag | Production of epsilonn caprolactam |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DD79494A (OSRAM) * | ||||
| US2758991A (en) * | 1956-08-14 | Hvvevvtofry | ||
| DE920073C (de) * | 1952-03-01 | 1954-11-11 | Bayer Ag | Verfahren zur Aufarbeitung des Destillationsrueckstandes von Lactamen |
| BE590037A (OSRAM) * | 1959-04-23 | |||
| DE1194863B (de) * | 1961-04-27 | 1965-06-16 | Basf Ag | Verfahren zur gleichzeitigen Gewinnung von reinem Ammoniumsulfat und reinen Lactamen aus Gemischen, die durch Beckmannsche Umlagerung von cycloaliphatischen Ketoximen mit Schwefelsaeure oder Oleum erhalten worden sind |
| DE1770745A1 (de) * | 1968-06-28 | 1971-11-25 | Hansdieter Hofmann | Verfahren zur Herstellung von reinem Caprolactam |
| DE2019431C2 (de) * | 1970-04-22 | 1981-10-15 | Bayer Ag, 5090 Leverkusen | Verfahren zur Reinigung von Caprolactam |
| IT956940B (it) * | 1972-06-28 | 1973-10-10 | Snia Viscosa | Procedimento per l estrazione di lattami da miscele acide di rea zione |
| US3914217A (en) * | 1974-11-13 | 1975-10-21 | Allied Chem | Process for the preparation of lactams |
| DE2656182C3 (de) * | 1976-12-11 | 1979-10-04 | Basf Ag, 6700 Ludwigshafen | Verfahren zur kontinuierlichen Extraktion von Caprolactam aus Wasser enthaltendem Rohlactam |
| NL7700234A (nl) * | 1977-01-12 | 1978-07-14 | Stamicarbon | Werkwijze voor het winnen van epsilon-caprolac- tam uit epsilon-caprolactam- bevattend destil- latieresidu. |
-
1979
- 1979-06-29 DE DE19792926279 patent/DE2926279A1/de not_active Withdrawn
-
1980
- 1980-05-21 DE DE8080102814T patent/DE3061061D1/de not_active Expired
- 1980-05-21 EP EP80102814A patent/EP0022161B1/de not_active Expired
- 1980-06-17 US US06/160,308 patent/US4301073A/en not_active Expired - Lifetime
- 1980-06-20 JP JP8297280A patent/JPS568360A/ja active Granted
- 1980-06-25 CA CA000354720A patent/CA1138865A/en not_active Expired
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5337685A (en) * | 1976-09-15 | 1978-04-06 | Bayer Ag | Production of epsilonn caprolactam |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2016505580A (ja) * | 2012-12-19 | 2016-02-25 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | シクロヘキサノンオキシムのベックマン転位からの精製カプロラクタムの製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0223544B2 (OSRAM) | 1990-05-24 |
| EP0022161A1 (de) | 1981-01-14 |
| DE3061061D1 (en) | 1982-12-16 |
| EP0022161B1 (de) | 1982-11-10 |
| US4301073A (en) | 1981-11-17 |
| CA1138865A (en) | 1983-01-04 |
| DE2926279A1 (de) | 1981-01-08 |
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