JPS5669216A - Preparation of noncrystalline silicone - Google Patents
Preparation of noncrystalline siliconeInfo
- Publication number
- JPS5669216A JPS5669216A JP14415679A JP14415679A JPS5669216A JP S5669216 A JPS5669216 A JP S5669216A JP 14415679 A JP14415679 A JP 14415679A JP 14415679 A JP14415679 A JP 14415679A JP S5669216 A JPS5669216 A JP S5669216A
- Authority
- JP
- Japan
- Prior art keywords
- discharge
- silane
- vacuum
- noncrystalline
- electric field
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/22—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
- C23C16/24—Deposition of silicon only
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Silicon Compounds (AREA)
Abstract
PURPOSE:To prepare efficiently finely divided particles of noncrystalline silicone having improved photoelectric properties, by introducing a silane (derivative)- containing gas into a vacuum reactor, subjecting it to discharge decomposition in an electric field under specific conditions. CONSTITUTION:A silane (SiH4) or silane derivative (disilane, chlorosilane, etc.)- containing gas introduced into a vacuum reactor is subjected to discharge decomposition with a gas temperature and discharge energy in the reactor maintained in such a way that the produce of the distance between the discharge pillar in the direction of the electric field and the degree of vacuum is 0.1-500 Torr cm, the prepared finely divided partices have a ratio of an absorption peak of infrared absorption spectrum at 2,000cm<-1> to that at 630<-1> not less than 0.06 and a spin concentration in electron spin resonance absorption is made not more than 10<18>cm<-8>. The gas temperature and discharge energy are set by selecting their values from ranges normal temperature to about 450 deg.C and 30 - above 150W respectively.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14415679A JPS5933531B2 (en) | 1979-11-06 | 1979-11-06 | Method for producing amorphous silicon fine powder |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14415679A JPS5933531B2 (en) | 1979-11-06 | 1979-11-06 | Method for producing amorphous silicon fine powder |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5669216A true JPS5669216A (en) | 1981-06-10 |
JPS5933531B2 JPS5933531B2 (en) | 1984-08-16 |
Family
ID=15355498
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP14415679A Expired JPS5933531B2 (en) | 1979-11-06 | 1979-11-06 | Method for producing amorphous silicon fine powder |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5933531B2 (en) |
-
1979
- 1979-11-06 JP JP14415679A patent/JPS5933531B2/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
JPS5933531B2 (en) | 1984-08-16 |
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