JPS5669216A - Preparation of noncrystalline silicone - Google Patents

Preparation of noncrystalline silicone

Info

Publication number
JPS5669216A
JPS5669216A JP14415679A JP14415679A JPS5669216A JP S5669216 A JPS5669216 A JP S5669216A JP 14415679 A JP14415679 A JP 14415679A JP 14415679 A JP14415679 A JP 14415679A JP S5669216 A JPS5669216 A JP S5669216A
Authority
JP
Japan
Prior art keywords
discharge
silane
vacuum
noncrystalline
electric field
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP14415679A
Other languages
Japanese (ja)
Other versions
JPS5933531B2 (en
Inventor
Masatoshi Tabei
Kazuhiro Kawajiri
Akio Azuma
Mitsuru Ikeda
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fujifilm Holdings Corp
Original Assignee
Fuji Photo Film Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fuji Photo Film Co Ltd filed Critical Fuji Photo Film Co Ltd
Priority to JP14415679A priority Critical patent/JPS5933531B2/en
Publication of JPS5669216A publication Critical patent/JPS5669216A/en
Publication of JPS5933531B2 publication Critical patent/JPS5933531B2/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/22Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
    • C23C16/24Deposition of silicon only

Landscapes

  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Silicon Compounds (AREA)

Abstract

PURPOSE:To prepare efficiently finely divided particles of noncrystalline silicone having improved photoelectric properties, by introducing a silane (derivative)- containing gas into a vacuum reactor, subjecting it to discharge decomposition in an electric field under specific conditions. CONSTITUTION:A silane (SiH4) or silane derivative (disilane, chlorosilane, etc.)- containing gas introduced into a vacuum reactor is subjected to discharge decomposition with a gas temperature and discharge energy in the reactor maintained in such a way that the produce of the distance between the discharge pillar in the direction of the electric field and the degree of vacuum is 0.1-500 Torr cm, the prepared finely divided partices have a ratio of an absorption peak of infrared absorption spectrum at 2,000cm<-1> to that at 630<-1> not less than 0.06 and a spin concentration in electron spin resonance absorption is made not more than 10<18>cm<-8>. The gas temperature and discharge energy are set by selecting their values from ranges normal temperature to about 450 deg.C and 30 - above 150W respectively.
JP14415679A 1979-11-06 1979-11-06 Method for producing amorphous silicon fine powder Expired JPS5933531B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP14415679A JPS5933531B2 (en) 1979-11-06 1979-11-06 Method for producing amorphous silicon fine powder

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP14415679A JPS5933531B2 (en) 1979-11-06 1979-11-06 Method for producing amorphous silicon fine powder

Publications (2)

Publication Number Publication Date
JPS5669216A true JPS5669216A (en) 1981-06-10
JPS5933531B2 JPS5933531B2 (en) 1984-08-16

Family

ID=15355498

Family Applications (1)

Application Number Title Priority Date Filing Date
JP14415679A Expired JPS5933531B2 (en) 1979-11-06 1979-11-06 Method for producing amorphous silicon fine powder

Country Status (1)

Country Link
JP (1) JPS5933531B2 (en)

Also Published As

Publication number Publication date
JPS5933531B2 (en) 1984-08-16

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