JPS5641226A - Preparation of aqueous emulsion - Google Patents
Preparation of aqueous emulsionInfo
- Publication number
- JPS5641226A JPS5641226A JP11576879A JP11576879A JPS5641226A JP S5641226 A JPS5641226 A JP S5641226A JP 11576879 A JP11576879 A JP 11576879A JP 11576879 A JP11576879 A JP 11576879A JP S5641226 A JPS5641226 A JP S5641226A
- Authority
- JP
- Japan
- Prior art keywords
- emulsion
- emulsifying
- rosin
- emulsifier
- derivative
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000839 emulsion Substances 0.000 title abstract 5
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- 239000003995 emulsifying agent Substances 0.000 abstract 3
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 abstract 2
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 abstract 2
- 230000001804 emulsifying effect Effects 0.000 abstract 2
- 238000004513 sizing Methods 0.000 abstract 2
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical group C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 abstract 1
- 239000005977 Ethylene Substances 0.000 abstract 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 abstract 1
- -1 NaOH) Chemical class 0.000 abstract 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 abstract 1
- 238000012644 addition polymerization Methods 0.000 abstract 1
- 125000002877 alkyl aryl group Chemical group 0.000 abstract 1
- 125000003118 aryl group Chemical group 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 239000006185 dispersion Substances 0.000 abstract 1
- 238000005187 foaming Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 150000007522 mineralic acids Chemical class 0.000 abstract 1
- 150000007524 organic acids Chemical class 0.000 abstract 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 abstract 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Chemical group CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 abstract 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 abstract 1
- 238000007127 saponification reaction Methods 0.000 abstract 1
- 238000010008 shearing Methods 0.000 abstract 1
- 238000006277 sulfonation reaction Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paper (AREA)
Abstract
PURPOSE: To obtain an aqueous emulsion useful as a sizing agent for paper, having good dispersion stability and excellent sizing property, and slightly foaming during sheeting, by emulsifying a rosin (derivative thereof) by use of a specified compound as an emulsifier.
CONSTITUTION: The titled emulsion is obtained, by adding, under normal or elevated pressure, (ii) 1W30pts.wt. of an emulsifier of the formula (wherein R is aryl or alkylaryl having 2W8 benzene rings; R1 is ethylene or propylene; n is 5W40; M is H, monovalent metal or ammonium) and, if necessary (iii) 1W50wt% of a saponification value equivalent to the saporification value by using an organic or inorganic acid (e.g., NaOH), to (i) 100pts.wt. of a rosin (derivative thereof), followed by gradual addition of warm water, to form an O/N type emulsion, and applying a strong shearing force to the emulsion with heating by means of a high- pressure emulsifying vessel etc. An emulsifying agent (ii) is obtained by the addition polymerization of a corresponding arylphenol and ethylene oxide, etc., and exterification with maleic anhydride, followed by sulfonation with a sulfite.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP54115768A JPS6031330B2 (en) | 1979-09-11 | 1979-09-11 | Method for producing aqueous emulsion |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP54115768A JPS6031330B2 (en) | 1979-09-11 | 1979-09-11 | Method for producing aqueous emulsion |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5641226A true JPS5641226A (en) | 1981-04-17 |
| JPS6031330B2 JPS6031330B2 (en) | 1985-07-22 |
Family
ID=14670566
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP54115768A Expired JPS6031330B2 (en) | 1979-09-11 | 1979-09-11 | Method for producing aqueous emulsion |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6031330B2 (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1997011994A1 (en) * | 1995-09-25 | 1997-04-03 | Henkel Kommanditgesellschaft Auf Aktien | Stabilized rosin dispersions |
| CN103768991A (en) * | 2012-10-25 | 2014-05-07 | 中国石油化工股份有限公司 | Anion/nonionic sulphonate surfactant and preparation method thereof |
-
1979
- 1979-09-11 JP JP54115768A patent/JPS6031330B2/en not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1997011994A1 (en) * | 1995-09-25 | 1997-04-03 | Henkel Kommanditgesellschaft Auf Aktien | Stabilized rosin dispersions |
| CN103768991A (en) * | 2012-10-25 | 2014-05-07 | 中国石油化工股份有限公司 | Anion/nonionic sulphonate surfactant and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6031330B2 (en) | 1985-07-22 |
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