JPS5625129A - Separation of polymeric ketone from plant - Google Patents
Separation of polymeric ketone from plantInfo
- Publication number
- JPS5625129A JPS5625129A JP9911979A JP9911979A JPS5625129A JP S5625129 A JPS5625129 A JP S5625129A JP 9911979 A JP9911979 A JP 9911979A JP 9911979 A JP9911979 A JP 9911979A JP S5625129 A JPS5625129 A JP S5625129A
- Authority
- JP
- Japan
- Prior art keywords
- bombiprenone
- esp
- saponified
- solvent
- extracted
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To separate a polymeric ketone, esp. bombiprenone useful as a raw material of pharmaceutical, easily and conveniently from plants containg a long chain polyisoprenoid compound, using n-hexane as a solvent which is selective to bombiprenone.
CONSTITUTION: Esp. leaves of a plant containing a long chain polyisoprenoid compound, e.g. tabacco, mulberry etc., are extracted with an ordinary lipophilic solvent, e.g. acetone. The extracted lipophilic component of the leaf is then saponified with an alkali. By this treatment most of the non-sisprenoid compounds are saponified and transferred to the aqueous layer. After the separation of the aqueous layer, the substances which are not saponified are treated with n-hexane to extract bonbiprenone selectively into the above layer. The impurities extracted together are separaed by crystallization and then the solvent is removed by conventional method, to give a polymeric ketone, esp. bombiprenone, easily and conveniently.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP9911979A JPS5625129A (en) | 1979-08-04 | 1979-08-04 | Separation of polymeric ketone from plant |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP9911979A JPS5625129A (en) | 1979-08-04 | 1979-08-04 | Separation of polymeric ketone from plant |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5625129A true JPS5625129A (en) | 1981-03-10 |
JPS6227051B2 JPS6227051B2 (en) | 1987-06-12 |
Family
ID=14238893
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP9911979A Granted JPS5625129A (en) | 1979-08-04 | 1979-08-04 | Separation of polymeric ketone from plant |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5625129A (en) |
-
1979
- 1979-08-04 JP JP9911979A patent/JPS5625129A/en active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS6227051B2 (en) | 1987-06-12 |
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