JPS5589354A - Preparation of aminothiofluoran compound - Google Patents
Preparation of aminothiofluoran compoundInfo
- Publication number
- JPS5589354A JPS5589354A JP213880A JP213880A JPS5589354A JP S5589354 A JPS5589354 A JP S5589354A JP 213880 A JP213880 A JP 213880A JP 213880 A JP213880 A JP 213880A JP S5589354 A JPS5589354 A JP S5589354A
- Authority
- JP
- Japan
- Prior art keywords
- compound
- aminothiofluoran
- substituted
- nucleus
- aminothiophenol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
PURPOSE: To prepare the title compound useful as a dye, etc. in high yield, by reacting a m-substituted aminothiophenol compound with phthalic acid anhydride (or its nucleus-substituted derivative).
CONSTITUTION: The objective aminothiofluoran compound of formula III [R is lower alkyl; Y is H or a functional group (e.g. halogen, nitro, etc.)], is prepared by reacting a m-substituted aminothiophenol of formula I with a phthalic acid anhydride (or its nucleus-substituted derivative), optionally in the presence of a Friedel- Crafts catalyst, at 140W150°C (molten state) for 1W2hr. The reaction may be carried out under reflux using a solvent. The molar ratio of the compound I to the compound II is e.g. 2:1.
USE: Raw material of aminothiofluoran-γ-lactam compound, etc.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP213880A JPS594450B2 (en) | 1980-01-14 | 1980-01-14 | Method for producing aminothiofluorane compounds |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP213880A JPS594450B2 (en) | 1980-01-14 | 1980-01-14 | Method for producing aminothiofluorane compounds |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP1800576A Division JPS52106873A (en) | 1976-02-23 | 1976-02-23 | Preparation of aminothiofluorane compound |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5589354A true JPS5589354A (en) | 1980-07-05 |
JPS594450B2 JPS594450B2 (en) | 1984-01-30 |
Family
ID=11520970
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP213880A Expired JPS594450B2 (en) | 1980-01-14 | 1980-01-14 | Method for producing aminothiofluorane compounds |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS594450B2 (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0477633A (en) * | 1990-07-19 | 1992-03-11 | Suga Shikenki Kk | Colorimeter |
-
1980
- 1980-01-14 JP JP213880A patent/JPS594450B2/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
JPS594450B2 (en) | 1984-01-30 |
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