JPS5564535A - Separation of mixture of ethylene glycol and ethylene carbonate - Google Patents
Separation of mixture of ethylene glycol and ethylene carbonateInfo
- Publication number
- JPS5564535A JPS5564535A JP13843578A JP13843578A JPS5564535A JP S5564535 A JPS5564535 A JP S5564535A JP 13843578 A JP13843578 A JP 13843578A JP 13843578 A JP13843578 A JP 13843578A JP S5564535 A JPS5564535 A JP S5564535A
- Authority
- JP
- Japan
- Prior art keywords
- ethylene glycol
- ethylene
- mixture
- ethylene carbonate
- alkylbenzene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To separate ethylene glycol and ethylene carbonate easily, with low heat consumption and with a rectifying column having a low theoretical plate number, by distilling a mixture of ethylene glycol and ethylene carbonate in the presence of an alkylbenzene.
CONSTITUTION: A mixture of ethylene glycol and ethylene carbonate is distilled in the presence of one or more compounds selected from alkylbenzenes expressed by the formula (R is 1W3C alkyl; n is 1W3; when n is 2 or 3, the substitution positions of the R are arbitrary), e.g. isopropylbenzene, etc. The azeotropic fraction of ethylene glycol and the alkylbenzene is taken out from the top of the distillation column and highly pure ethylene carbonate is obtained as the residue. The azeotropic fraction is separated to two liquid layers by condensation. The alkylbenzene is recycled to the distillation system and the ethylene glycol layer is if desired purified by distillation to give highly pure ethylene glycol.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP13843578A JPS5564535A (en) | 1978-11-10 | 1978-11-10 | Separation of mixture of ethylene glycol and ethylene carbonate |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP13843578A JPS5564535A (en) | 1978-11-10 | 1978-11-10 | Separation of mixture of ethylene glycol and ethylene carbonate |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5564535A true JPS5564535A (en) | 1980-05-15 |
JPS6215537B2 JPS6215537B2 (en) | 1987-04-08 |
Family
ID=15221903
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP13843578A Granted JPS5564535A (en) | 1978-11-10 | 1978-11-10 | Separation of mixture of ethylene glycol and ethylene carbonate |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5564535A (en) |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS4834810A (en) * | 1971-09-08 | 1973-05-22 | ||
JPS51144492A (en) * | 1975-05-27 | 1976-12-11 | Bayer Ag | Method of making apiphatic polycarbonate |
-
1978
- 1978-11-10 JP JP13843578A patent/JPS5564535A/en active Granted
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS4834810A (en) * | 1971-09-08 | 1973-05-22 | ||
JPS51144492A (en) * | 1975-05-27 | 1976-12-11 | Bayer Ag | Method of making apiphatic polycarbonate |
Also Published As
Publication number | Publication date |
---|---|
JPS6215537B2 (en) | 1987-04-08 |
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