JPS5528963A - Purification of estrone - Google Patents
Purification of estroneInfo
- Publication number
- JPS5528963A JPS5528963A JP10313878A JP10313878A JPS5528963A JP S5528963 A JPS5528963 A JP S5528963A JP 10313878 A JP10313878 A JP 10313878A JP 10313878 A JP10313878 A JP 10313878A JP S5528963 A JPS5528963 A JP S5528963A
- Authority
- JP
- Japan
- Prior art keywords
- estrone
- solvent
- crude
- brought
- solid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- DNXHEGUUPJUMQT-UHFFFAOYSA-N (+)-estrone Natural products OC1=CC=C2C3CCC(C)(C(CC4)=O)C4C3CCC2=C1 DNXHEGUUPJUMQT-UHFFFAOYSA-N 0.000 title abstract 8
- DNXHEGUUPJUMQT-CBZIJGRNSA-N Estrone Chemical compound OC1=CC=C2[C@H]3CC[C@](C)(C(CC4)=O)[C@@H]4[C@@H]3CCC2=C1 DNXHEGUUPJUMQT-CBZIJGRNSA-N 0.000 title abstract 8
- 229960003399 estrone Drugs 0.000 title abstract 8
- 238000000746 purification Methods 0.000 title 1
- 239000002904 solvent Substances 0.000 abstract 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- 239000012535 impurity Substances 0.000 abstract 3
- 239000007787 solid Substances 0.000 abstract 2
- KPQGJISRWLEDFQ-QAGGRKNESA-N (8r,9s,10r,13s,14s)-10,13-dimethyl-3,6,7,8,9,11,12,14,15,16-decahydrocyclopenta[a]phenanthren-17-one Chemical compound C1C=C[C@]2(C)[C@H]3CC[C@](C)(C(CC4)=O)[C@@H]4[C@@H]3CCC2=C1 KPQGJISRWLEDFQ-QAGGRKNESA-N 0.000 abstract 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 230000017858 demethylation Effects 0.000 abstract 1
- 238000010520 demethylation reaction Methods 0.000 abstract 1
- -1 polycyclic aromatic compound Chemical class 0.000 abstract 1
- 239000008096 xylene Substances 0.000 abstract 1
Landscapes
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Steroid Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10313878A JPS5528963A (en) | 1978-08-24 | 1978-08-24 | Purification of estrone |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP10313878A JPS5528963A (en) | 1978-08-24 | 1978-08-24 | Purification of estrone |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5528963A true JPS5528963A (en) | 1980-02-29 |
| JPS6136520B2 JPS6136520B2 (enrdf_load_stackoverflow) | 1986-08-19 |
Family
ID=14346158
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP10313878A Granted JPS5528963A (en) | 1978-08-24 | 1978-08-24 | Purification of estrone |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5528963A (enrdf_load_stackoverflow) |
-
1978
- 1978-08-24 JP JP10313878A patent/JPS5528963A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6136520B2 (enrdf_load_stackoverflow) | 1986-08-19 |
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