JPS55154326A - Manufacture of iron-pentacarbonyl - Google Patents
Manufacture of iron-pentacarbonylInfo
- Publication number
- JPS55154326A JPS55154326A JP5988579A JP5988579A JPS55154326A JP S55154326 A JPS55154326 A JP S55154326A JP 5988579 A JP5988579 A JP 5988579A JP 5988579 A JP5988579 A JP 5988579A JP S55154326 A JPS55154326 A JP S55154326A
- Authority
- JP
- Japan
- Prior art keywords
- iron
- pentacarbonyl
- manufacture
- atom
- alkyl group
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
PURPOSE: To manufacture the iron-pentacarbonyl in high yield and with a high selectively by the reaction of a divalent iron compound and CO in an aqueous ammonia or amine solution containing an iron-pentacarbonyl extraction solvent.
CONSTITUTION: The divalent iron compound, e.g., ferrous sulfate, ferrous lactate, etc., is mixed with 2mol or more, particularly 6W15mol (based on 1g atom of iron) an ammonia or amine aqueous solution, represented as the formulas IWIII (where R1 and R2 are, respectively, H or 1W5C alkyl group, R3 and R4 are, respectively, H or 1W2C alkyl group, and n is 1 or 2), and 200W5,000g, particularly 300W3,000g (based on 1g atom of iron) of an iron-pentacarbonyl extraction solvent, e.g., pentane, benzene, etc. Then, the mixture is treated with CO gas of a pressure of 20W250kg/cm2G, particularly 50W200kg/cm2G, at 60W200°C, particularly 80W150°C, so as to cause the reaction of the divalent iron compound with CO to take place.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5988579A JPS586693B2 (en) | 1979-05-16 | 1979-05-16 | Production method of iron pentacarbonyl |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5988579A JPS586693B2 (en) | 1979-05-16 | 1979-05-16 | Production method of iron pentacarbonyl |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS55154326A true JPS55154326A (en) | 1980-12-01 |
| JPS586693B2 JPS586693B2 (en) | 1983-02-05 |
Family
ID=13126023
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP5988579A Expired JPS586693B2 (en) | 1979-05-16 | 1979-05-16 | Production method of iron pentacarbonyl |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS586693B2 (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113196537B (en) * | 2018-12-19 | 2024-03-22 | Lg电子株式会社 | Apparatus for manufacturing cell stack of secondary battery |
| JP6588181B1 (en) | 2019-04-25 | 2019-10-09 | 株式会社日立パワーソリューションズ | Strip workpiece supply device |
-
1979
- 1979-05-16 JP JP5988579A patent/JPS586693B2/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| JPS586693B2 (en) | 1983-02-05 |
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