JPS5466612A - Preparation of ketazine - Google Patents

Preparation of ketazine

Info

Publication number
JPS5466612A
JPS5466612A JP13114277A JP13114277A JPS5466612A JP S5466612 A JPS5466612 A JP S5466612A JP 13114277 A JP13114277 A JP 13114277A JP 13114277 A JP13114277 A JP 13114277A JP S5466612 A JPS5466612 A JP S5466612A
Authority
JP
Japan
Prior art keywords
alkyl
acid salt
formula
ketazine
peroxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP13114277A
Other languages
Japanese (ja)
Inventor
Tsukasa Maekawa
Hidetoshi Kume
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Otsuka Chemical Co Ltd
Otsuka Kagaku Yakuhin KK
Original Assignee
Otsuka Chemical Co Ltd
Otsuka Kagaku Yakuhin KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Otsuka Chemical Co Ltd, Otsuka Kagaku Yakuhin KK filed Critical Otsuka Chemical Co Ltd
Priority to JP13114277A priority Critical patent/JPS5466612A/en
Publication of JPS5466612A publication Critical patent/JPS5466612A/en
Pending legal-status Critical Current

Links

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PURPOSE: To prepare ketazine easily and in high yield by the reaction of ammonia, a peroxide, and a ketone at a remarkaply high raction rate using a new catalyst composed of iminoether, amidine, or their acid salt.
CONSTITUTION: Ketazine of formula IV is prepared by the reaction of ammonia, a peroxide, e.g. hydrogen peroxide, and a ketone of formula I (R1=C1-8 alkyl, phenyl; R2=C1-8 alkyl; R1 and R2 may together form C4-8 alkylene, e.g. acetone, at -20°C-100°C using a catalyst composed of an iminoether of formula II (R3=H, C1-8 alkyl, C4-10 cycloalkyl etc.; R4=C1-8 alkyl), e.g. formiminomethyl ether, acetiminomethyl ether, etc., amidine of formula III (R5, R6=H, C1-5 alkyl), e.g. formamidine, acetamidine etc., or their acid salt (e.g. hydrochloric acid salt, sulfuric acid salt, formic acid salt).
COPYRIGHT: (C)1979,JPO&Japio
JP13114277A 1977-10-31 1977-10-31 Preparation of ketazine Pending JPS5466612A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP13114277A JPS5466612A (en) 1977-10-31 1977-10-31 Preparation of ketazine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP13114277A JPS5466612A (en) 1977-10-31 1977-10-31 Preparation of ketazine

Publications (1)

Publication Number Publication Date
JPS5466612A true JPS5466612A (en) 1979-05-29

Family

ID=15050972

Family Applications (1)

Application Number Title Priority Date Filing Date
JP13114277A Pending JPS5466612A (en) 1977-10-31 1977-10-31 Preparation of ketazine

Country Status (1)

Country Link
JP (1) JPS5466612A (en)

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