JPS5452031A - Preparation of alcohol sulfuric acid ester salt - Google Patents

Preparation of alcohol sulfuric acid ester salt

Info

Publication number
JPS5452031A
JPS5452031A JP11518277A JP11518277A JPS5452031A JP S5452031 A JPS5452031 A JP S5452031A JP 11518277 A JP11518277 A JP 11518277A JP 11518277 A JP11518277 A JP 11518277A JP S5452031 A JPS5452031 A JP S5452031A
Authority
JP
Japan
Prior art keywords
sulfuric acid
acid ester
sulfating
sulfur trioxide
boric anhydride
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP11518277A
Other languages
Japanese (ja)
Other versions
JPS5715113B2 (en
Inventor
Hachiro Yamaguchi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nitto Chemical Industry Co Ltd
Original Assignee
Nitto Chemical Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nitto Chemical Industry Co Ltd filed Critical Nitto Chemical Industry Co Ltd
Priority to JP11518277A priority Critical patent/JPS5452031A/en
Publication of JPS5452031A publication Critical patent/JPS5452031A/en
Publication of JPS5715113B2 publication Critical patent/JPS5715113B2/ja
Granted legal-status Critical Current

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

PURPOSE: To prepare an almost colorless title compound in high yield with little side ractions under mild conditions, by sulfating a primary or secondary alcohol having 6-18 C atoms using a complex of boric anhydride and sulfur trioxide as novel sulfating agent.
CONSTITUTION: An alcohol sulfuric acid ester salt (e.g. cyclohexanol sulfuric acid ester ammonium salt) is prepared by sulfating a 6-18C primary or secondary alcohol (e.g. cyclohexanol) in a solvent pref. comprising dimethylformamide containing a chlorinated alkane such as 1,2-dichloroethane, at a low temperature (e.g. -20- -10°C) using a complex of boric anhydride and sulfur trioxide obtained by the reaction of boric anhydride with sulfur trioxide in a solvent, as sulfating agent
COPYRIGHT: (C)1979,JPO&Japio
JP11518277A 1977-09-27 1977-09-27 Preparation of alcohol sulfuric acid ester salt Granted JPS5452031A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP11518277A JPS5452031A (en) 1977-09-27 1977-09-27 Preparation of alcohol sulfuric acid ester salt

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP11518277A JPS5452031A (en) 1977-09-27 1977-09-27 Preparation of alcohol sulfuric acid ester salt

Publications (2)

Publication Number Publication Date
JPS5452031A true JPS5452031A (en) 1979-04-24
JPS5715113B2 JPS5715113B2 (en) 1982-03-29

Family

ID=14656376

Family Applications (1)

Application Number Title Priority Date Filing Date
JP11518277A Granted JPS5452031A (en) 1977-09-27 1977-09-27 Preparation of alcohol sulfuric acid ester salt

Country Status (1)

Country Link
JP (1) JPS5452031A (en)

Also Published As

Publication number Publication date
JPS5715113B2 (en) 1982-03-29

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