JPS5452016A - Preparation of allyl chloride or methallyl chloride - Google Patents
Preparation of allyl chloride or methallyl chlorideInfo
- Publication number
- JPS5452016A JPS5452016A JP11757677A JP11757677A JPS5452016A JP S5452016 A JPS5452016 A JP S5452016A JP 11757677 A JP11757677 A JP 11757677A JP 11757677 A JP11757677 A JP 11757677A JP S5452016 A JPS5452016 A JP S5452016A
- Authority
- JP
- Japan
- Prior art keywords
- chloride
- olefin
- tellurium
- methallyl
- liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To prepare allyl chloride or methallyl chloride in a selectivity of above 95% at a low temperature, by the liquid-phase chlorination of an olefin using a specific chloride as a source of chlorine.
CONSTITUTION: Allyl chloride or methallyl chloride is prepared by introducing an olefin comprising propylene, isobutyline or their mixture into a solvent containing a dispersed chloride selected from tellurium and selenium chlorides or their mixture, followed by the liquid-phase chlorination at 100-300°C and at ordinary pressure to 50kg/cm2G. Chlorides of variable valence metals such as CuCl2 may coexist. Furthemore, tellurium chloride, etc. which has been converted to a lower valent chloride or a metal, is chlorinated by introducing Cl2 into the solvent together with the olefin, converted to a higher valent chloride and regenerated as a chlorinating agnet.
EFFECT: On account of a low temperature liquid-phase reaction, sublimation of tellurium chloride scarcely occurs, and therefore continuous running can be carried out stably.
USE: Raw material of epichlorohydrin
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11757677A JPS5452016A (en) | 1977-09-30 | 1977-09-30 | Preparation of allyl chloride or methallyl chloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11757677A JPS5452016A (en) | 1977-09-30 | 1977-09-30 | Preparation of allyl chloride or methallyl chloride |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5452016A true JPS5452016A (en) | 1979-04-24 |
| JPS6129937B2 JPS6129937B2 (en) | 1986-07-10 |
Family
ID=14715230
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11757677A Granted JPS5452016A (en) | 1977-09-30 | 1977-09-30 | Preparation of allyl chloride or methallyl chloride |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5452016A (en) |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4840323A (en) * | 1971-09-25 | 1973-06-13 |
-
1977
- 1977-09-30 JP JP11757677A patent/JPS5452016A/en active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4840323A (en) * | 1971-09-25 | 1973-06-13 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6129937B2 (en) | 1986-07-10 |
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