JPS54148740A - Production of 3-methyl-2-cyclopentene-1-one - Google Patents
Production of 3-methyl-2-cyclopentene-1-oneInfo
- Publication number
- JPS54148740A JPS54148740A JP5531778A JP5531778A JPS54148740A JP S54148740 A JPS54148740 A JP S54148740A JP 5531778 A JP5531778 A JP 5531778A JP 5531778 A JP5531778 A JP 5531778A JP S54148740 A JPS54148740 A JP S54148740A
- Authority
- JP
- Japan
- Prior art keywords
- acid
- solid
- methylpentenoic
- cyclopentene
- methyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: Only heating of 4-methylpentenoic acid in the presence of a solid acid catalyst economically and advantageously gives title compound usefuel as a starting material for various medicines, perfumes, agricultural chemicals in high yield.
CONSTITUTION: 4-Methylpentenoic acid is heated in the presence of a solid acid catalyst at 250W450°C and converted to 3-methyl-2-cyclopentene-1-one. The solid catalyst used is, e.g., silica-alumina, solid phosphoric acid, boron phosphate, zeolite. The starting compound, 4-methylpentenoic acid, is readily prepared by reaction between methallyl chloride and an acetoacetate ester in the presence of an alkali metal alkoxide followed by hydrolysis using an alkali.
EFFECT: The operations are simple.
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP5531778A JPS54148740A (en) | 1978-05-10 | 1978-05-10 | Production of 3-methyl-2-cyclopentene-1-one |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP5531778A JPS54148740A (en) | 1978-05-10 | 1978-05-10 | Production of 3-methyl-2-cyclopentene-1-one |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS54148740A true JPS54148740A (en) | 1979-11-21 |
JPS6157293B2 JPS6157293B2 (en) | 1986-12-06 |
Family
ID=12995167
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP5531778A Granted JPS54148740A (en) | 1978-05-10 | 1978-05-10 | Production of 3-methyl-2-cyclopentene-1-one |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS54148740A (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS55108648A (en) * | 1978-11-17 | 1980-08-21 | Energy Conversion Devices Inc | Flash printing device |
EP0266687A2 (en) * | 1986-11-07 | 1988-05-11 | BASF Aktiengesellschaft | Process for the manufacture of cyclopentanone |
EP0297447A2 (en) * | 1987-06-30 | 1989-01-04 | BASF Aktiengesellschaft | Method for the preparation of 2-cyclopentenones |
US5118864A (en) * | 1990-03-13 | 1992-06-02 | Basf Aktiengesellschaft | Preparation of cyclopentenones |
-
1978
- 1978-05-10 JP JP5531778A patent/JPS54148740A/en active Granted
Non-Patent Citations (1)
Title |
---|
CHEMICAL ABSTRACTS=1967 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS55108648A (en) * | 1978-11-17 | 1980-08-21 | Energy Conversion Devices Inc | Flash printing device |
EP0266687A2 (en) * | 1986-11-07 | 1988-05-11 | BASF Aktiengesellschaft | Process for the manufacture of cyclopentanone |
EP0266687A3 (en) * | 1986-11-07 | 1989-04-19 | Basf Aktiengesellschaft | Process for the manufacture of cyclopentanone |
EP0297447A2 (en) * | 1987-06-30 | 1989-01-04 | BASF Aktiengesellschaft | Method for the preparation of 2-cyclopentenones |
US5118864A (en) * | 1990-03-13 | 1992-06-02 | Basf Aktiengesellschaft | Preparation of cyclopentenones |
Also Published As
Publication number | Publication date |
---|---|
JPS6157293B2 (en) | 1986-12-06 |
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