JPH1061038A - Method for applying sealing material - Google Patents
Method for applying sealing materialInfo
- Publication number
- JPH1061038A JPH1061038A JP23992496A JP23992496A JPH1061038A JP H1061038 A JPH1061038 A JP H1061038A JP 23992496 A JP23992496 A JP 23992496A JP 23992496 A JP23992496 A JP 23992496A JP H1061038 A JPH1061038 A JP H1061038A
- Authority
- JP
- Japan
- Prior art keywords
- treatment
- sealing material
- discharge
- electric discharge
- applying
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
Description
【0001】[0001]
【発明の属する技術分野】本発明は、シーリング(シー
ル)材をプライマーなしに被施工面に高接着強度を持っ
て施工することができるシーリング材の施工方法に関
し、更に詳述すると、建築用の各種パネル、アルミサッ
シ等にシーリング材を施工する場合に好適であり、被施
工面がフッ素樹脂等の難接着面であっても、プライマー
なしに高い接着強度でシーリング材を接着できるシーリ
ング材の施工方法に関する。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for applying a sealing material to a surface to be applied with high adhesive strength without using a primer, and more particularly to a method for building a sealing material. Suitable for applying sealing materials to various panels, aluminum sashes, etc., even if the surface to be applied is a difficult-to-bond surface such as fluororesin, a sealing material that can be bonded with a high adhesive strength without a primer. About the method.
【0002】[0002]
【従来の技術及び発明が解決しようとする課題】従来よ
り、建築物などに水密性、気密性を与えるため、シーリ
ング材を施工することは広く行われているが、シーリン
グ材を被施工体の被施工面に施工する方法としては、従
来から、被施工面を洗浄脱脂後、プライマーを塗布し、
シーリング材を施工する方法が採用されている。2. Description of the Related Art Conventionally, in order to impart watertightness and airtightness to buildings and the like, sealing materials have been widely applied. As a method of applying to the work surface, conventionally, after cleaning and degreasing the work surface, apply a primer,
A method of applying a sealing material has been adopted.
【0003】特に、近年、上記シーリング材を施工する
外壁材としては、建物の外壁の汚れ防止と耐久性の改良
を目的としてフッ素樹脂塗装鋼板などのフッ素樹脂で表
面処理された外壁材が広く使用されるようになってきて
いる。In particular, in recent years, as the outer wall material for applying the above-mentioned sealing material, an outer wall material surface-treated with a fluororesin such as a fluororesin-coated steel sheet has been widely used for the purpose of preventing dirt on the outer wall of a building and improving durability. It is becoming.
【0004】しかしながら、フッ素樹脂塗装面を有する
外壁材は、表面のぬれ性が悪く、シーリング材の接着が
難しい。However, the outer wall material having a fluororesin-coated surface has poor surface wettability, and it is difficult to bond a sealing material.
【0005】そこで、このような外壁材を使用する場合
には、予め被施工面をブラスティングにより粗面化して
からプライマーを塗布し、次いでシーリング材を施工す
ることが行われている。Therefore, when such an outer wall material is used, a surface to be processed is roughened in advance by blasting, a primer is applied, and then a sealing material is applied.
【0006】ところが、上記外壁材はブラスティング処
理が施し難く、接着不良の原因となる上、ブラスティン
グ処理は非常に手間がかかり、ブラスティング処理の程
度によっては、被施工面への接着力は十分なものではな
く、やや強い力がかかるとシーリング材が剥がれてしま
うという問題がある。However, the above-mentioned outer wall material is difficult to be subjected to blasting treatment, which causes poor adhesion, and the blasting treatment is very troublesome. Depending on the degree of the blasting treatment, the adhesive strength to the surface to be processed is low. There is a problem that the sealing material is peeled off when it is not sufficient and a relatively strong force is applied.
【0007】また、ブラスティング処理後のプライマー
塗布作業は、塗工に手間がかかる上、乾燥を要するので
時間もかかり、作業能率を著しく低下せしめる。[0007] In addition, the work of applying a primer after the blasting process is time-consuming because it requires time and labor for coating, which significantly reduces the work efficiency.
【0008】従って、被施工面がフッ素樹脂塗装面等の
難接着面であっても、プライマー塗布を省略してシーリ
ング材を被施工面に能率よく、高い接着強度で接着し得
るシーリング材の施工方法の開発が望まれていた。Therefore, even if the surface to be applied is a surface that is difficult to adhere, such as a surface coated with a fluororesin, the application of the sealing material can be performed efficiently and the sealing material can be adhered to the surface to be applied with high adhesive strength by omitting the primer application. The development of a method was desired.
【0009】本発明は、上記事情に鑑みなされたもの
で、シーリング材を被施工体の被施工面に施工した場合
に、プライマーを使用することなく高い接着強度を発揮
でき、特に、被施工面がフッ素樹脂等の難接着面であっ
ても、手間をかけずに強固に接着することが可能なシー
リング材の施工方法を提供することを目的とする。The present invention has been made in view of the above circumstances, and when a sealing material is applied to a work surface of a work, a high adhesive strength can be exhibited without using a primer. It is an object of the present invention to provide a method of applying a sealing material capable of firmly adhering to a hard-to-adhere surface such as a fluororesin without any trouble.
【0010】[0010]
【課題を解決するための手段及び発明の実施の形態】本
発明者らは、上記目的を達成するため鋭意検討を重ねた
結果、シーリング材を被施工体の被施工面に施工するに
際し、予め被施工面に対して、所定の放電処理を施すこ
とにより、接着に最適な被施工面が得られ、高い接着強
度を発揮し得、たとえフッ素樹脂等の難接着面を有する
場合でも、プライマーを塗布することなくシーリング材
を優れた接着強度で直接かつ確実に接着できることを知
見した。Means for Solving the Problems and Embodiments of the Invention The present inventors have conducted intensive studies in order to achieve the above object, and as a result, when applying the sealing material to the work surface of the work, By performing a predetermined discharge treatment on the work surface, an optimum work surface for bonding can be obtained, and high bonding strength can be exhibited. It has been found that a sealing material can be directly and reliably bonded with excellent bonding strength without application.
【0011】即ち、シーリング材を被施工体の被施工面
に施工する場合において、予め、被施工面にコロナ処
理、プラズマ処理、コロナ放電又はアーク放電をガス流
により吹き出させる処理、プラズマトーチ処理などの放
電処理を施すことにより、被施工体の表面を最適な状態
に改質することができ、表面の濡れ性や反応性(接着
性)を著しく向上させることが可能となり、プライマー
を使用しなくても飛躍的に接着強度を向上させ得ること
を知見した。That is, when the sealing material is applied to the work surface of the work body, a corona treatment, a plasma treatment, a treatment for blowing out a corona discharge or an arc discharge by a gas flow, a plasma torch treatment, etc. By applying a discharge treatment, the surface of the object to be processed can be modified to an optimal state, and the wettability and reactivity (adhesion) of the surface can be significantly improved. However, it has been found that the bonding strength can be dramatically improved.
【0012】そして、従来から懸案であった被施工面が
フッ素樹脂等の難接着面からなる場合でも、ブラスティ
ング処理やプライマーの塗布などの手間のかかる処理を
全く必要とせず、能率よく、確実に被施工面に直接シー
リング材を接着でき、この方法で施工された建築用の各
種パネル、アルミサッシの施工面は優れた水密性、気密
性を有する高性能、高品質なものであり、上記方法が最
適なシーリング材の施工方法であることを見出し、本発
明を完成させたものである。[0012] Even when the work surface, which has conventionally been a problem, is made of a difficult-to-adhere surface such as a fluororesin, it does not require any complicated processing such as blasting treatment or application of a primer. The sealing material can be bonded directly to the work surface, and various construction panels and aluminum sash construction surfaces constructed by this method are excellent in watertightness, airtightness, high performance and high quality. The present inventors have found that the method is an optimum sealing material application method, and have completed the present invention.
【0013】従って、本発明は、(1)被施工体の被施
工面に対して、予め放電処理を施した後、シーリング材
を直接施工することを特徴とするシーリング材の施工方
法、(2)被施工面が樹脂塗装面である(1)記載のシ
ーリング材の施工方法、(3)被施工面がフッ素樹脂を
含む樹脂塗装面である(2)記載のシーリング材の施工
方法、(4)放電処理がコロナ処理又はプラズマ処理で
ある(1)乃至(3)のいずれか1に記載のシーリング
材の施工方法、(5)放電処理がコロナ放電又はアーク
放電をガス流により吹き出させる処理である(1)乃至
(3)のいずれか1に記載のシーリング材の施工方法、
及び、(6)放電処理がプラズマ放電をガス流により吹
き出させるプラズマトーチ処理である(1)乃至(3)
のいずれか1に記載のシーリング材の施工方法を提供す
る。Accordingly, the present invention provides (1) a method for applying a sealing material, which comprises applying a discharge treatment to a surface of an object to be processed in advance and then directly applying the sealing material; ) The method of applying a sealing material according to (1), wherein the surface to be applied is a resin-coated surface; (3) the method of applying a sealing material according to (2), wherein the surface to be applied is a resin-coated surface containing a fluororesin; (1) The method for applying a sealing material according to any one of (1) to (3), wherein the discharge treatment is a corona treatment or a plasma treatment, and (5) the discharge treatment is a treatment for blowing corona discharge or arc discharge by a gas flow. The method for applying a sealing material according to any one of (1) to (3),
And (6) the discharge process is a plasma torch process for blowing a plasma discharge by a gas flow (1) to (3).
The present invention provides a method for applying a sealing material according to any one of the above.
【0014】以下、本発明につき更に詳しく説明する
と、本発明のシーリング材の施工方法は被施工体の被施
工面に対して、予め所定の放電処理を施した後、プライ
マーなしで直接シーリング材を施工するものである。Hereinafter, the present invention will be described in more detail. In the method of applying a sealing material according to the present invention, a predetermined discharge treatment is applied to a surface to be processed of a workpiece in advance, and then the sealing material is directly applied without a primer. It is to be constructed.
【0015】ここで、被施工体としては、特に制限され
ず、建築用の各種樹脂塗装パネル、塗装されたアルミサ
ッシ等、或いは表面に樹脂を塗工した建築用木材、金
属、セラミックスボード、コンクリートパネル等に好適
に使用できる。この場合、被施工面がフッ素樹脂等の難
接着面を有する樹脂塗装面であっても、手間のかかるブ
ラスティング処理やプライマー処理を施すことなく、能
率的にシーリング材を施工できるものである。The object to be processed is not particularly limited, and may be any of a variety of resin-coated panels for building, a painted aluminum sash, or the like, or wood, metal, ceramics board, concrete for building, whose surface is coated with resin. It can be suitably used for panels and the like. In this case, even if the surface to be applied is a resin-coated surface having a hardly adhered surface such as a fluororesin, the sealing material can be efficiently applied without performing a complicated blasting process or a primer process.
【0016】シーリング材は、被施工体の目地、間隙部
分に充填して水密性、気密性などの機能を発揮させる材
料であり、具体的には、ポリサルファイド系シーリング
材、変成シリコーン系シーリング材、ポリウレタン系シ
ーリング材、シリコーン系シーリング材等を用いること
ができるが、特に制限はされない。The sealing material is a material which is filled into joints and gaps of the object to be worked to exhibit functions such as water-tightness and air-tightness. Specifically, a polysulfide-based sealing material, a modified silicone-based sealing material, A polyurethane-based sealing material, a silicone-based sealing material, or the like can be used, but is not particularly limited.
【0017】本発明の放電処理としては、コロナ処理、
プラズマ処理、コロナ放電又はアーク放電をガス流によ
り吹き出させる処理、及びプラズマトーチ処理が好適で
あり、これらのいずれの放電処理を施しても本発明の優
れた作用効果を発揮させることができるものである。こ
の場合、被施工表面に上記放電処理を施すことにより、
被施工体の表面を最適な状態に改質することができ、表
面の濡れ性や反応性(接着性)が著しく向上し、シーリ
ング材と被施工面との接着強度を著しく向上させること
ができるものである。As the discharge treatment of the present invention, corona treatment,
Plasma treatment, treatment for blowing out corona discharge or arc discharge by a gas flow, and plasma torch treatment are preferable, and any of these discharge treatments can exert the excellent effects of the present invention. is there. In this case, by performing the discharge treatment on the work surface,
The surface of the workpiece can be modified to an optimal state, the wettability and reactivity (adhesion) of the surface can be significantly improved, and the adhesive strength between the sealing material and the surface to be processed can be significantly improved. Things.
【0018】特に、シーリング材の施工は、通常、建築
現場で実施されることが多いが、この場合、処理の簡便
性、装置の携帯性などの点から、コロナ処理又はコロナ
放電をガス流により吹き出させる処理がより好適であ
る。In particular, the sealing material is usually applied at a construction site. In this case, the corona treatment or the corona discharge is carried out by a gas flow in terms of simplicity of treatment and portability of the apparatus. The process of blowing out is more preferable.
【0019】ここで、コロナ処理としては、高周波の高
電圧により電極と対面電極に放電を生じさせ、その放電
空間に被施工体を通過させることにより放電処理を行う
方法を採用し得る。または、被施工体が金属等の導電体
の場合には、被施工体自体を対面電極として、電極と被
施工体の間で放電を生じさせることにより被施工面を改
質させることができる。この場合、放電条件は、通常、
出力は10〜1000W、処理時間は0.1〜30se
c程度である。Here, as the corona treatment, a method in which a discharge is generated between the electrode and the facing electrode by a high-frequency high voltage and the discharge treatment is performed by passing the workpiece through the discharge space. Alternatively, when the object to be processed is a conductor such as a metal, the surface to be processed can be modified by causing a discharge between the electrode and the object to be processed by using the object to be processed as a facing electrode. In this case, the discharge condition is usually
Output is 10 to 1000 W, processing time is 0.1 to 30 sec
c.
【0020】プラズマ処理は、プラズマ中のイオン、電
子、ラジカル、光、原子、分子などを利用して被施工体
の表面改質を行うものであり、所定の圧力(低圧又は大
気圧)のガスに対し、直流又は交流電界により放電を発
生せしめ、その放電中又は放電よりガス流の下流に被施
工体を設置して放電処理を行う方法を採用し得るもので
ある。この場合、放電条件は、通常、圧力は0.001
〜1000Torr、プラズマ励起電界周波数は、直
流,50Hz等の定周波交流,1〜100kHz程度の
交流,13.56MHz等のラジオ波,2.45GHz
等のマイクロ波等が利用できる。気体としてはアルゴン
(Ar)ガス,酸素ガス,空気,窒素,ヘリウム,CF
4等が用いられる。In the plasma treatment, the surface of an object to be processed is modified by utilizing ions, electrons, radicals, light, atoms, molecules, etc. in the plasma, and a gas of a predetermined pressure (low pressure or atmospheric pressure) is applied. In contrast, a method in which a discharge is generated by a DC or AC electric field, and a discharge treatment is performed by installing a workpiece during the discharge or downstream of the gas flow from the discharge. In this case, the discharge conditions are usually such that the pressure is 0.001.
10001000 Torr, plasma excitation electric field frequency: DC, constant frequency AC such as 50 Hz, AC about 1 to 100 kHz, radio wave such as 13.56 MHz, 2.45 GHz
And other microwaves can be used. As the gas, argon (Ar) gas, oxygen gas, air, nitrogen, helium, CF
4 etc. are used.
【0021】コロナ放電又はアーク放電をガス流により
吹き出させる処理としては、電極間でコロナ放電又はア
ーク放電を生じさせ、空気等のガス流を吹き付けて、下
流側に吹き出した放電に被施工体を当てて放電処理する
方法が採用される。この場合、放電条件は、通常、放電
吹出口と被施工面とを1〜100mm離間し、処理時間
は1〜30sec程度であることが好ましい。As a treatment for blowing out a corona discharge or an arc discharge by a gas flow, a corona discharge or an arc discharge is generated between the electrodes, a gas flow such as air is blown, and the workpiece is blown to the discharge blown downstream. A method of applying a discharge treatment is adopted. In this case, it is preferable that the discharge conditions are usually such that the discharge outlet and the work surface are separated from each other by 1 to 100 mm, and the processing time is about 1 to 30 sec.
【0022】プラズマトーチ処理としては、大気圧等で
プラズマ放電を生じさせ、ガスを吹き付け、下流側に吹
き出した放電に被施工体を当てて放電処理を行う方法が
採用できる。この場合、放電条件は、通常、ガスとして
はヘリウム(He)ガス、アルゴン等を用い、圧力は5
00〜2000Torr、周波数は50Hz〜 100
MHz、処理時間は1〜30sec程度である。As the plasma torch treatment, a method in which a plasma discharge is generated at atmospheric pressure or the like, a gas is blown, and an object to be processed is applied to the discharge blown to the downstream side to perform a discharge treatment. In this case, the discharge conditions are usually helium (He) gas, argon or the like as the gas, and the pressure is 5
00 to 2000 Torr, frequency is 50 Hz to 100
MHz and the processing time are about 1 to 30 sec.
【0023】本発明のシーリング材の施工方法は、被施
工面に対して上記放電処理を施した後、プライマーを塗
布することなく直接シーリング材を施工するものであ
る。これにより、難接着面を有しない通常の樹脂の場合
には、従来に比べて更に接着強度が向上し、難接着面を
有するフッ素樹脂等の場合には、ブラスティング処理を
することなく、しかもブラスティング処理を施した場合
よりも高い接着強度でプライマーなしにシーリング材を
直接被施工面に接着できるものである。また、このよう
にプライマー塗布作業を省略し得るので、施工作業を大
幅に効率化することができる。In the method for applying a sealing material according to the present invention, the above-mentioned discharge treatment is applied to the surface to be applied, and then the sealing material is applied directly without applying a primer. As a result, in the case of a normal resin having no hard-to-bond surface, the bonding strength is further improved compared to the conventional case, and in the case of a fluororesin or the like having a hard-to-bond surface, without blasting treatment, The sealing material can be directly bonded to the surface to be processed without a primer with a higher bonding strength than in the case of performing the blasting treatment. In addition, since the primer application operation can be omitted as described above, the efficiency of the operation can be greatly improved.
【0024】なお、本発明の対象となる被施工体として
は建築用の各種パネル、プレハブ部材の窓周りのアルミ
サッシに好適なものであり、本発明のシーリング材の施
工方法により、シーリング材がその性能を有効に発揮
し、水密性、気密性に優れた特性を発揮し得るものであ
る。The object to be processed according to the present invention is suitable for various types of building panels and aluminum sashes around windows of prefabricated members. It can exhibit its performance effectively and exhibit excellent watertightness and airtightness.
【0025】[0025]
【発明の効果】本発明のシーリング材の施工方法は、シ
ーリング材を被施工体の被施工面に施工した場合に、プ
ライマーを使用することなく高い接着強度を発揮し得る
ものであり、特に、被施工面がフッ素樹脂等の難接着面
を有する場合でも、手間をかけずにシーリング材を強固
に接着できるものである。According to the method for applying a sealing material of the present invention, when a sealing material is applied to a work surface of a work, a high adhesive strength can be exhibited without using a primer. Even when the surface to be processed has a difficult-to-bond surface such as a fluororesin, the sealing material can be firmly bonded without any trouble.
【0026】[0026]
【実施例】以下、実施例と比較例を示し、本発明を具体
的に説明するが、本発明は下記実施例に制限されるもの
ではない。EXAMPLES The present invention will be described below in detail with reference to examples and comparative examples, but the present invention is not limited to the following examples.
【0027】[実施例、比較例]フッ素樹脂を表面に塗
工した50mm×50mmのサンプルパネル(カイナー
高温焼付けパネル)に対して、下記条件に従って放電処
理を施した(実施例(A)〜(D))。なお、(E)は
放電処理を施さない比較例である(プライマー未処
理)。 (A)コロナ処理(出力:300W、処理時間:5se
c);TANTEC社製HV05−2 (B)プラズマ処理(圧力:1Torr、使用気体:ア
ルゴン(Ar)ガス、出力:100W、処理時間:30
sec);ヤマト科学社製灰化装置PC101A (C)吹き出しコロナ処理(40mmの距離、処理時
間:4sec;アールブラント社製プラズマトリーター (D)プラズマトーチ処理(圧力:760Torr、使
用気体:Heガス、周波数:13.56MHz、出力:
100W、処理時間:5sec) (E)未処理 その後、シーリング材((株)ブリヂストン製、1液型
変成シリコーン系シーリング材、ペタムMS1000)
を施工して、JIS A5758に準拠したH型試験体
(サンプル)を作成した。サンプルは20℃,55%R
Hにて1週間前養生した後、50℃にて1週間後養生し
た。[Examples and Comparative Examples] A 50 mm × 50 mm sample panel (Kyner high-temperature baked panel) coated with a fluororesin on its surface was subjected to a discharge treatment under the following conditions (Examples (A) to (C)). D)). (E) is a comparative example in which no discharge treatment was performed (primer untreated). (A) Corona treatment (output: 300 W, processing time: 5 sec)
c); HV05-2 manufactured by TANTEC (B) Plasma treatment (pressure: 1 Torr, working gas: argon (Ar) gas, output: 100 W, treatment time: 30)
sec); Ashing device PC101A manufactured by Yamato Scientific Co., Ltd. (C) Blow-off corona treatment (distance of 40 mm, treatment time: 4 sec; Plasma treater manufactured by R-Brand Co., Ltd. (D) Plasma torch treatment (pressure: 760 Torr, gas used: He gas, Frequency: 13.56 MHz, output:
100 W, processing time: 5 sec) (E) Untreated, then sealing material (Bridgestone Corp., one-component modified silicone-based sealing material, Petam MS1000)
To prepare an H-type specimen (sample) in accordance with JIS A5758. Sample is 20 ℃, 55% R
After curing for one week at H, curing was performed at 50 ° C. for one week.
【0028】得られたサンプルをJIS A5758に
準拠して接着試験を行った。結果を表1に示す。The obtained sample was subjected to an adhesion test according to JIS A5758. Table 1 shows the results.
【0029】[0029]
【表1】 [Table 1]
【0030】表1の結果から、被施工面に対して、予め
放電処理を行うことにより、被施工面がフッ素樹脂等の
難接着面を有する場合であっても、破断強度が大きく、
凝集破壊剥離となり、シーリング材をプライマーなしに
直接強固に接着し得ることが確認できた。From the results in Table 1, it can be seen that by subjecting the work surface to a discharge treatment in advance, even if the work surface has a hardly adherent surface such as a fluororesin, the breaking strength is high.
Cohesive failure peeling was observed, and it was confirmed that the sealing material could be directly and firmly bonded without a primer.
Claims (6)
処理を施した後、シーリング材を直接施工することを特
徴とするシーリング材の施工方法。1. A method for applying a sealing material, wherein a surface to be processed of an object to be processed is subjected to a discharge treatment in advance, and then a sealing material is directly applied.
載のシーリング材の施工方法。2. The method according to claim 1, wherein the surface to be applied is a resin-coated surface.
である請求項2記載のシーリング材の施工方法。3. The method according to claim 2, wherein the surface to be applied is a resin-coated surface containing a fluororesin.
である請求項1乃至3のいずれか1項に記載のシーリン
グ材の施工方法。4. The method according to claim 1, wherein the discharge treatment is a corona treatment or a plasma treatment.
ガス流により吹き出させる処理である請求項1乃至3の
いずれか1項に記載のシーリング材の施工方法。5. The method for applying a sealing material according to claim 1, wherein the discharge treatment is a treatment for blowing corona discharge or arc discharge by a gas flow.
吹き出させるプラズマトーチ処理である請求項1乃至3
のいずれか1項に記載のシーリング材の施工方法。6. A plasma torch process for discharging a plasma discharge by a gas flow.
The method for applying a sealing material according to any one of the above.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP23992496A JPH1061038A (en) | 1996-08-22 | 1996-08-22 | Method for applying sealing material |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP23992496A JPH1061038A (en) | 1996-08-22 | 1996-08-22 | Method for applying sealing material |
Publications (1)
Publication Number | Publication Date |
---|---|
JPH1061038A true JPH1061038A (en) | 1998-03-03 |
Family
ID=17051876
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP23992496A Pending JPH1061038A (en) | 1996-08-22 | 1996-08-22 | Method for applying sealing material |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPH1061038A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6299714B1 (en) | 1997-06-30 | 2001-10-09 | Bridgestone Corporation | Sealant application method |
-
1996
- 1996-08-22 JP JP23992496A patent/JPH1061038A/en active Pending
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6299714B1 (en) | 1997-06-30 | 2001-10-09 | Bridgestone Corporation | Sealant application method |
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