JPH10251044A - Production of granulated and water granulated slag - Google Patents

Production of granulated and water granulated slag

Info

Publication number
JPH10251044A
JPH10251044A JP8193497A JP8193497A JPH10251044A JP H10251044 A JPH10251044 A JP H10251044A JP 8193497 A JP8193497 A JP 8193497A JP 8193497 A JP8193497 A JP 8193497A JP H10251044 A JPH10251044 A JP H10251044A
Authority
JP
Japan
Prior art keywords
water
slag
granulated
water tank
granulation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP8193497A
Other languages
Japanese (ja)
Other versions
JP3091161B2 (en
Inventor
Yoshito Matsuoka
義人 松岡
Koji Ariake
紘治 有明
Akira Kaga
彰 加賀
Hideto Tomura
秀人 戸村
Koji Tanaka
幸二 田中
Toru Kikuchi
亨 菊地
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JFE Steel Corp
Kawasaki Heavy Industries Ltd
Original Assignee
Kawasaki Heavy Industries Ltd
Kawasaki Steel Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kawasaki Heavy Industries Ltd, Kawasaki Steel Corp filed Critical Kawasaki Heavy Industries Ltd
Priority to JP09081934A priority Critical patent/JP3091161B2/en
Publication of JPH10251044A publication Critical patent/JPH10251044A/en
Application granted granted Critical
Publication of JP3091161B2 publication Critical patent/JP3091161B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Landscapes

  • Glanulating (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)
  • Furnace Details (AREA)

Abstract

PROBLEM TO BE SOLVED: To make it possible to granulate the shapes of water granulated slag and to increase the grain sizes of the slag by specifying the water temps. of injection water for water granulation of molten slag and a storage water tank of the water granulated slag. SOLUTION: Incineration ashes, such as waste incineration ashes, are supplied to an ash melting furnace 10 and are heated and melted by a torch 12, by which the incineration ashes are melt treated and the molten slag is obtd. While the molten slag is sent from the outlet 14 of the ash melting furnace to the storage water tank 16, the water in the storage water tank 16 is injected from a nozzle 17 by a granulation water injection pump 18 to granulate the molten slag and to cool the slag. The water granulated slag subjected to the cooling is dropped into the storage water tank 16. The water temps. of the injection water and the storage water tank 16 are controlled to 60 to 85 deg.C, more preferably 65 to 80 deg.C by controlling a circulating water flow control valve 21 via a temp. indication controller 20. The water is sent from a cooling column 22 to the storage water tank 16. The cooling water is circulated to the storage water tank 16 by the granulation water injection pump 18 and a granulation water circulating pump 24.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は、廃棄物焼却灰等の
灰溶融炉からの溶融スラグを水砕するときの水温を一定
の範囲内に制御することで、水砕スラグの形状を粒状化
する方法に関するものである。
The present invention relates to granulating the shape of granulated slag by controlling the temperature of water when granulating molten slag from an ash melting furnace for waste incineration ash or the like within a certain range. How to do it.

【0002】[0002]

【従来の技術】灰溶融炉において溶融処理された溶融ス
ラグを水砕処理して得られたスラグを水砕スラグという
が、図3に示すように、一般的な水砕スラグは針状又は
塊状である。従来、水砕処理に用いられる水の温度は、
一般的に0〜45℃の範囲であったが、水砕水の温度を
0〜45℃として得られた水砕スラグは針状又は塊状と
なり、粒径が1mm未満のスラグが、例えば45℃の場合
は46%以上を占める微細塊となっていた。
2. Description of the Related Art Slag obtained by subjecting molten slag that has been subjected to melting treatment in an ash melting furnace to granulation is called granulated slag. As shown in FIG. 3, a general granulated slag is needle-like or massive. It is. Conventionally, the temperature of water used for granulation is
Generally, the temperature was in the range of 0 to 45 ° C, but the granulated slag obtained by setting the temperature of the granulated water to 0 to 45 ° C becomes acicular or massive, and the slag having a particle size of less than 1 mm is, for example, 45 ° C. In the case of the above, it was a fine lump occupying 46% or more.

【0003】特公昭51−15056号公報には、溶融
炉から排出される溶融鉱滓に高圧水を噴射することによ
り、急冷粒化を効果的に行い、良品の水滓スラグを製造
する方法が記載されている。特公昭59−25143号
公報には、溶融スラグを適正な水量、水圧の加圧水によ
り細分化し、急冷粒状化して、水砕スラグにする方法が
記載されている。特開昭54−155662号公報に
は、汚泥又はゴミの焼却灰を加熱溶融して溶滓とし、こ
の溶滓を水砕して水滓スラグを製造する方法が記載され
ている。特開平5−201753号公報には、廃棄物焼
却灰溶融炉の溶融スラグ排出口から流下するスラグに、
スラグ流の変化に対応して方向が変更できる水掛けノズ
ルから水を吹き掛けて、スラグを水砕する装置が記載さ
れている。なお、これまでに、水砕処理に用いる水の温
度を一定の温度以上に制御することで、水砕スラグの形
状を粒状化することを試みたという内容の文献は見当た
らない。
[0003] JP-B-51-15056 describes a method for producing high quality slag slag by injecting high-pressure water into molten slag discharged from a melting furnace to effectively perform quenching and granulation. Have been. Japanese Patent Publication No. 59-25143 describes a method in which molten slag is subdivided with pressurized water having an appropriate amount of water and a water pressure, and is granulated by rapid cooling to obtain granulated slag. Japanese Patent Application Laid-Open No. 54-155662 describes a method for producing a slag by heating and melting incinerated ash of sludge or dust to form a slag, and granulating the slag to produce a slag slag. Japanese Patent Application Laid-Open No. Hei 5-201753 discloses that slag flowing down from a molten slag discharge port of a waste incineration ash melting furnace includes:
An apparatus for spraying water from a watering nozzle whose direction can be changed in response to a change in slag flow to granulate slag is described. Heretofore, there is no document that attempts to granulate the shape of the granulated slag by controlling the temperature of the water used for the granulated treatment to a certain temperature or higher.

【0004】[0004]

【発明が解決しようとする課題】溶融スラグを水砕処理
して砂状化した場合、従来の水砕スラグでは針状又は鋭
角の塊状となるため、運搬や取り扱いの際に、スラグが
手などに突き刺さったり、裂傷などを負ったりするの
で、これらに対する十分な注意が必要であった。
When the molten slag is granulated to form a sand, the conventional granulated slag is formed into a needle-like or sharp-angled lump. It is necessary to pay close attention to such things as piercing or laceration.

【0005】また、水砕スラグが針状又は鋭角の塊状と
なれば、粒径の小さなスラグが大部分を占めるため、土
木・建築資材等として利用する際の分級化が困難になる
とともに、天然骨材の代替品として土木・建築資材等へ
の適用が困難になる。
Further, if the granulated slag is in the form of needles or sharp-angled slag, the slag having a small particle size occupies most of the granulated slag. It becomes difficult to apply it to civil engineering and construction materials as a substitute for aggregate.

【0006】本発明は上記の諸点に鑑みなされたもの
で、本発明の目的は、溶融スラグを水砕するときの水温
を一定の範囲内に制御することで、水砕スラグの形状を
粒状化し、スラグの粒径を大きくする方法を提供するこ
とにある。
SUMMARY OF THE INVENTION The present invention has been made in view of the above points, and an object of the present invention is to control the temperature of water for granulating molten slag within a certain range, thereby granulating the granulated slag. Another object of the present invention is to provide a method for increasing the particle size of slag.

【0007】[0007]

【課題を解決するための手段】上記の目的を達成するた
めに、本発明の粒状化水砕スラグの製造方法は、溶融ス
ラグを水砕処理して水砕スラグとする方法において、水
砕スラグの形状を粒状化するために、溶融スラグを水砕
するための噴射水及び落下した水砕スラグの貯留水槽の
水温を60〜85℃の範囲とすることを特徴としてい
る。
In order to achieve the above object, a method for producing granulated granulated slag of the present invention is characterized in that a granulated granulated slag is obtained by granulating molten slag into granulated slag. In order to granulate the shape of the slag, the water temperature of the injection water for granulating the molten slag and the water temperature of the storage tank of the granulated slag that falls is characterized by being in the range of 60 to 85 ° C.

【0008】本発明は、溶融スラグを水砕するための噴
射水及び落下した水砕スラグの貯留水槽の水温を一定の
温度以上に制御することで、水砕スラグの形状を粒状化
し、スラグの粒径を大きくするものであるが、上記のよ
うに、水砕するときの水温は、60〜85℃の範囲、好
ましくは、65〜80℃の範囲に保持する。これは、水
砕するときの水温が60℃未満の場合は、水砕スラグの
大部分が針状又は塊状となるという不具合があり、一
方、水砕するときの水温が85℃を超える場合は、実用
上、溶融スラグの冷却に適さないという不具合があるか
らである。
According to the present invention, the shape of the granulated slag is granulated by controlling the water temperature of the injection water for granulating the molten slag and the water temperature of the storage tank for the granulated slag that has fallen to a certain temperature or higher. Although the particle size is increased, the water temperature at the time of granulation is maintained in the range of 60 to 85C, preferably in the range of 65 to 80C, as described above. This is because when the water temperature at the time of granulation is less than 60 ° C, there is a problem that most of the granulated slag becomes needle-like or massive, while when the water temperature at the time of granulation exceeds 85 ° C, This is because there is a problem that it is not suitable for cooling the molten slag in practical use.

【0009】[0009]

【発明の実施の形態】図1は本発明の粒状化水砕スラグ
の製造方法を実施する装置の一例を示している。図1に
おいて、10は灰溶融炉であり、溶融処理に用いるトー
チ12を備えている。灰溶融炉10で溶融処理された溶
融スラグは、灰溶融炉出口14から貯留水槽16に送ら
れる間に、水砕水噴射ポンプ18によりノズル17から
貯留水槽16内の水が噴射され冷却される。そして、冷
却されたスラグは貯留水槽16に落下する。噴射水及び
貯留水槽16の水温は、温度指示制御装置20を介して
循環水流量調節弁21を調節することで60〜85℃の
範囲、望ましくは65〜80℃の範囲に制御されてお
り、冷却塔22から冷却水が貯留水槽16に送られる。
冷却水はそれぞれ、水砕水噴射ポンプ18、水砕水循環
ポンプ24により貯留水槽16に循環されている。この
ようにして得られた水砕スラグは、スラグ搬送装置25
の水砕スラグ搬出口26から搬出される。28は温度検
出器である。
FIG. 1 shows an example of an apparatus for carrying out the method for producing granulated granulated slag of the present invention. In FIG. 1, reference numeral 10 denotes an ash melting furnace, which includes a torch 12 used for a melting process. While the molten slag melt-processed in the ash melting furnace 10 is sent from the ash melting furnace outlet 14 to the storage water tank 16, water in the storage water tank 16 is injected from the nozzle 17 by the granulated water injection pump 18 to be cooled. . Then, the cooled slag falls into the storage water tank 16. The water temperature of the injection water and the storage water tank 16 is controlled in the range of 60 to 85 ° C., preferably in the range of 65 to 80 ° C. by adjusting the circulating water flow control valve 21 via the temperature instruction control device 20, Cooling water is sent from the cooling tower 22 to the storage water tank 16.
The cooling water is circulated to the storage water tank 16 by the granulated water injection pump 18 and the granulated water circulation pump 24, respectively. The granulated slag thus obtained is supplied to the slag conveying device 25.
From the granulated slag carry-out port 26. 28 is a temperature detector.

【0010】表1に、溶融スラグを水砕するときの水温
を変化させた場合の水砕スラグの粒径の分布を示した。
各温度の左側は各粒径の範囲の割合(%)を示し、各温
度の右側は各上限粒径未満の割合(%)を示している。
そして、表1の結果をグラフに表したのが図2である。
なお、水砕スラグの粒径が小さければ、スラグは針状又
は鋭角の塊状ということができ、水砕スラグの粒径が大
きければ、スラグは粒状化していると言える。
[0010] Table 1 shows the particle size distribution of the granulated slag when the water temperature at the time of granulating the molten slag was changed.
The left side of each temperature shows the ratio (%) of the range of each particle size, and the right side of each temperature shows the ratio (%) less than each upper limit particle size.
FIG. 2 shows the results of Table 1 in a graph.
If the particle size of the granulated slag is small, it can be said that the slag is in the form of a needle or a sharp angle. If the particle size of the granulated slag is large, it can be said that the slag is granulated.

【0011】[0011]

【表1】 [Table 1]

【0012】表1の結果からもわかるように、溶融スラ
グを水砕するときの水温を60℃以上とした場合には、
塊状のスラグの約60%以上が粒径1mm以上の水砕スラ
グとなり、水砕スラグの約50%以上が粒状化すること
になる。このように、溶融スラグを水砕するときの水温
を60℃以上にした場合には、図4及び図5に示すよう
に、水砕スラグ中に針状又は鋭角の塊状のスラグは殆ど
無くなる。
As can be seen from the results in Table 1, when the water temperature at which the molten slag is granulated is 60 ° C. or higher,
About 60% or more of the massive slag is granulated slag having a particle size of 1 mm or more, and about 50% or more of the granulated slag is granulated. As described above, when the water temperature at the time of granulating the molten slag is 60 ° C. or higher, as shown in FIGS. 4 and 5, there is almost no needle-shaped or sharp-angled slag in the granulated slag.

【0013】そして、水砕スラグの形状を粒状化するこ
とで、土木・建築資材等として利用する際の分級化が容
易になるとともに、運搬や取り扱いにおける危険性がき
わめて少なくなる。また、スラグの粒径を大きく成長さ
せることにより、天然骨材の代替品として土木・建築資
材等への適用が容易になる。
[0013] By granulating the shape of the granulated slag, it is easy to classify the granulated slag when used as civil engineering and building materials, and the danger in transportation and handling is extremely reduced. In addition, by increasing the particle size of the slag to a large value, it becomes easy to apply it to civil engineering and construction materials as a substitute for natural aggregate.

【0014】[0014]

【発明の効果】本発明は上記のように構成されているの
で、つぎのような効果を奏する。 (1) 水砕処理に用いる水の温度を制御するだけで、
水砕スラグの形状を粒状 (2) 水砕スラグの形状を粒状化することで、運搬や
取り扱いにおける危険性がきわめて少なくなる。 (3) 水砕スラグの形状を粒状化することで、土木・
建築資材等として利用する際の分級化が容易になる。 (4) 水砕スラグの形状を粒状化し、スラグの粒径を
大きく成長させることにより、天然骨材の代替品として
土木・建築資材等への適用が容易になる。
As described above, the present invention has the following effects. (1) Just by controlling the temperature of the water used for the granulation process,
Granulated granulated slag (2) By granulating the granulated slag, the danger in transportation and handling is extremely reduced. (3) By granulating the granulated slag,
Classification when used as building materials, etc. is facilitated. (4) Granulating the shape of the granulated slag and increasing the particle size of the slag greatly facilitates application to civil engineering and construction materials as a substitute for natural aggregate.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明の粒状化水砕スラグの製造方法を実施す
る装置の一例を示す概略図である。
FIG. 1 is a schematic view showing an example of an apparatus for implementing the method for producing granulated granulated slag of the present invention.

【図2】溶融スラグを水砕するときの水温を変化させた
場合の水砕スラグの粒径の分布を示すグラフである。
FIG. 2 is a graph showing a particle size distribution of the granulated slag when the water temperature at the time of granulating the molten slag is changed.

【図3】溶融スラグを水砕するときの水温が45℃の場
合における水砕スラグの粒子構造を示す拡大写真である
(倍率10倍)。
FIG. 3 is an enlarged photograph showing a particle structure of the granulated slag when the temperature of the granulated slag is 45 ° C. (magnification: 10 ×).

【図4】溶融スラグを水砕するときの水温が60℃の場
合における水砕スラグの粒子構造を示す拡大写真である
(倍率10倍)。
FIG. 4 is an enlarged photograph showing the particle structure of the granulated slag when the temperature of the granulated slag is 60 ° C. (magnification: 10 ×).

【図5】溶融スラグを水砕するときの水温が75℃の場
合における水砕スラグの粒子構造を示す拡大写真である
(倍率10倍)。
FIG. 5 is an enlarged photograph showing a particle structure of the granulated slag when the water temperature at the time of granulating the molten slag is 75 ° C. (magnification: 10 ×).

【符号の説明】[Explanation of symbols]

10 灰溶融炉 12 トーチ 14 灰溶融炉出口 16 貯留水槽 17 ノズル 18 水砕水噴射ポンプ 20 温度指示制御装置 21 循環水流量調節弁 22 冷却塔 24 水砕水循環ポンプ 25 スラグ搬送装置 26 水砕スラグ搬出口 28 温度検出器 DESCRIPTION OF SYMBOLS 10 Ash melting furnace 12 Torch 14 Ash melting furnace outlet 16 Reservoir tank 17 Nozzle 18 Granulated water injection pump 20 Temperature indication control device 21 Circulating water flow control valve 22 Cooling tower 24 Granulated water circulation pump 25 Slag conveyance device 26 Granulated slag conveyance Outlet 28 Temperature detector

───────────────────────────────────────────────────── フロントページの続き (72)発明者 有明 紘治 神戸市中央区東川崎町1丁目1番3号 川 崎重工業株式会社神戸本社内 (72)発明者 加賀 彰 神戸市中央区東川崎町1丁目1番3号 川 崎重工業株式会社神戸本社内 (72)発明者 戸村 秀人 神戸市中央区東川崎町1丁目1番3号 川 崎重工業株式会社神戸本社内 (72)発明者 田中 幸二 神戸市中央区東川崎町1丁目1番3号 川 崎重工業株式会社神戸本社内 (72)発明者 菊地 亨 東京都千代田区内幸町2丁目2番3号 川 崎製鉄株式会社東京本社内 ──────────────────────────────────────────────────続 き Continuing on the front page (72) Inventor Koji Ariake 1-3-1 Higashikawasakicho, Chuo-ku, Kobe Kawasaki Heavy Industries, Ltd. Kobe Head Office (72) Inventor Akira Kaga 1-1-1, Higashikawasakicho, Chuo-ku, Kobe No. 3 Kawasaki Heavy Industries, Ltd.Kobe Head Office (72) Inventor Hideto Tomura 1-3-1, Higashi Kawasaki-cho, Chuo-ku, Kobe City Kawasaki Heavy Industries, Ltd.Kobe Head Office (72) Inventor Koji Tanaka Chuo-ku, Kobe City Kawasaki Heavy Industries, Ltd. Kobe Head Office (72) Inventor Toru Kikuchi 2-3-2 Uchisaiwai-cho, Chiyoda-ku, Tokyo Kawasaki Steel Corporation Tokyo Head Office

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】 溶融スラグを水砕処理して水砕スラグと
する方法において、 水砕スラグの形状を粒状化するために、溶融スラグを水
砕するための噴射水及び落下した水砕スラグの貯留水槽
の水温を60〜85℃の範囲とすることを特徴とする粒
状化水砕スラグの製造方法。
1. A method for granulating a molten slag by granulating the molten slag, wherein the granulated slag is granulated. A method for producing granulated granulated slag, wherein the water temperature of the storage water tank is in the range of 60 to 85 ° C.
JP09081934A 1997-03-13 1997-03-13 Method for producing granulated granulated slag Expired - Fee Related JP3091161B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP09081934A JP3091161B2 (en) 1997-03-13 1997-03-13 Method for producing granulated granulated slag

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP09081934A JP3091161B2 (en) 1997-03-13 1997-03-13 Method for producing granulated granulated slag

Publications (2)

Publication Number Publication Date
JPH10251044A true JPH10251044A (en) 1998-09-22
JP3091161B2 JP3091161B2 (en) 2000-09-25

Family

ID=13760322

Family Applications (1)

Application Number Title Priority Date Filing Date
JP09081934A Expired - Fee Related JP3091161B2 (en) 1997-03-13 1997-03-13 Method for producing granulated granulated slag

Country Status (1)

Country Link
JP (1) JP3091161B2 (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20010017293A (en) * 1999-08-10 2001-03-05 이구택 A Method for Preparing Water-Granulated Slag Having Low Density
JP2004050136A (en) * 2002-07-23 2004-02-19 Nippon Steel Corp Slag granulation plant in waste melting treatment
JP2007055855A (en) * 2005-08-25 2007-03-08 Nippon Steel Engineering Co Ltd Method and apparatus for cooling granulation water
JP2016204759A (en) * 2016-08-31 2016-12-08 住友金属鉱山株式会社 Method for production of water-granulated slag
CN109696055A (en) * 2018-12-26 2019-04-30 青海铜业有限责任公司 A kind of melting furnace slag-discharging device and method

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20010017293A (en) * 1999-08-10 2001-03-05 이구택 A Method for Preparing Water-Granulated Slag Having Low Density
JP2004050136A (en) * 2002-07-23 2004-02-19 Nippon Steel Corp Slag granulation plant in waste melting treatment
JP2007055855A (en) * 2005-08-25 2007-03-08 Nippon Steel Engineering Co Ltd Method and apparatus for cooling granulation water
JP4644068B2 (en) * 2005-08-25 2011-03-02 新日鉄エンジニアリング株式会社 Cooled water cooling method and cooling device
JP2016204759A (en) * 2016-08-31 2016-12-08 住友金属鉱山株式会社 Method for production of water-granulated slag
CN109696055A (en) * 2018-12-26 2019-04-30 青海铜业有限责任公司 A kind of melting furnace slag-discharging device and method

Also Published As

Publication number Publication date
JP3091161B2 (en) 2000-09-25

Similar Documents

Publication Publication Date Title
US11273491B2 (en) Process for producing spheroidized powder from feedstock materials
US11590568B2 (en) Process for producing spheroidized powder from feedstock materials
DE60116009T2 (en) METHOD FOR PRODUCING REDUCED IRON
DE102016105162A1 (en) Process and plant for the additive production of metallic moldings
CN102605115B (en) Process method for producing steel shots by ladle-casting slag pelletization
JPH10251044A (en) Production of granulated and water granulated slag
CN108296490A (en) A kind of manufacturing method of spherical shape tungsten tantalum alloy powder
Su et al. In-situ thermal control-assisted laser directed energy deposition of curved-surface thin-walled parts
AU2018400808B2 (en) Methods of forming spherical metallic particles
JP5380264B2 (en) Method for melting metal ingots
JP2008184341A (en) Method and apparatus for regulating particle size of water-granulated slag
JPH1095644A (en) Prevention of solidification of blast furnace granulated slug and solidification preventing system
JP2005226939A (en) Slag treating method and treating apparatus
SU872509A1 (en) Method of producing chrome-magnesial refractory materials
CN115058631B (en) Manufacturing method suitable for coaxial powder feeding composite friction stir treatment of oxide dispersion strengthening steel
KR101844158B1 (en) Metal Oxide Powder by Plasma Treatment and Method of using the same
JPH10169951A (en) Spheroidizing treatment method of sewerage sludge incineration ash
JP5706189B2 (en) Metal melting method using electron beam melting furnace
JPS62125843A (en) Production of spherical particle
KR20140005032A (en) Method for controlling particle size of reduction slag ball for control of blast pressure
JPS62171949A (en) Water granulation equipment for waste molten slag
EP3913070A1 (en) Method and device for dry granulation
JP2000219545A (en) Process and equipment for producing water granulated slag
Narayanan et al. Laser Powder Bed Fusion of Ti6Al4V Alloy for Biomedical Applications: Prospects and Challenges—Process Details, Powder Characteristics and Laser Irradiation
JPH046772B2 (en)

Legal Events

Date Code Title Description
R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

S111 Request for change of ownership or part of ownership

Free format text: JAPANESE INTERMEDIATE CODE: R313117

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

LAPS Cancellation because of no payment of annual fees