JPH09253916A - Surface coated fine grain cemented carbide end mill - Google Patents

Surface coated fine grain cemented carbide end mill

Info

Publication number
JPH09253916A
JPH09253916A JP6460796A JP6460796A JPH09253916A JP H09253916 A JPH09253916 A JP H09253916A JP 6460796 A JP6460796 A JP 6460796A JP 6460796 A JP6460796 A JP 6460796A JP H09253916 A JPH09253916 A JP H09253916A
Authority
JP
Japan
Prior art keywords
end mill
cemented carbide
coated
average
coated fine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP6460796A
Other languages
Japanese (ja)
Inventor
Hiroshi Ichikawa
洋 市川
Teruyoshi Tanase
照義 棚瀬
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Materials Corp
Original Assignee
Mitsubishi Materials Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Materials Corp filed Critical Mitsubishi Materials Corp
Priority to JP6460796A priority Critical patent/JPH09253916A/en
Publication of JPH09253916A publication Critical patent/JPH09253916A/en
Pending legal-status Critical Current

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Abstract

PROBLEM TO BE SOLVED: To provide a surface coated fine grain cemented carbide end mill excellent in wear resistance and usable in a wide cutting area from low speed to high speed by covering the surface of a tough fine particle cemented carbide base material with an inner layer formed of titanium carbide nitride having high toughness, and further applying aluminum oxide having high wear resistance and fusion resistance thereon. SOLUTION: An end mill is formed by use of a fine particle cemented carbide base material formed of a coupled phase mainly containing tungsten carbide having an average particle size of about 0.2-1.0μm and about 5-15wt.% of Co, and the surface of its cutting part is coated with titanium carbide nitride, or with titanium nitride and titanium carbide nitride. The inner layer is set to have an average thickness of 0.5-3.0μm. Further, the surface of the inner surface is coated with aluminum oxide having an average thickness of 0.1-1.0μm, and the average of total thickness is set to 0.6-4.0μm. Further, the cutting edge of the end mill is subjected to a honing of 1-50μm to form a desired surface coated fine particle cemented carbide end mill.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【発明の属する技術分野】本発明は、強靭な微粒超硬合
金母材の表面に炭窒化チタンまたは窒化チタンと炭窒化
チタンで被覆構成された内層を有し、外層に酸化アルミ
ニウム層を被覆した耐摩耗性・耐欠損性に優れた表面被
覆微粒超硬エンドミルに関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention has a tough fine grain cemented carbide base material having an inner layer coated on the surface with titanium carbonitride or titanium nitride and titanium carbonitride, and an outer layer coated with an aluminum oxide layer. The present invention relates to a surface-coated fine-grain cemented carbide end mill having excellent wear resistance and fracture resistance.

【0002】[0002]

【従来の技術】従来の表面被覆超硬エンドミルは、切刃
部の耐摩耗性向上をはかるために、超硬合金よりなる母
材の表面に、物理蒸着法によりTiN、TiCN、(T
i、Al)N等の硬質膜を被覆処理して硬質層を生成し
たエンドミルを用いるのが一般的である。しかし、従来
の被覆処理で生成した硬質層では付着強度が弱いため耐
摩耗性が不足する。そこで、付着強度および耐摩耗性を
更に向上させる手段として、特開昭62−208803
号において,炭化タングステン基超硬合金、炭化チタン
基サ−メット、および高速度鋼のうちのいずれかからな
る硬質合金基体の表面に、平均層厚:0.1〜1μmの
金属Ti被覆層を介して、同1〜9μmの硬質被覆層を
形成してなり、かつ前記硬質被覆層が同0.2〜4μm
を有する炭化チタンの下層と、同0.2〜4μmを有す
る炭窒化チタンの中間層と、同0.2〜3μmを有する
窒化チタンの上層の3層からなる表面被覆硬質合金製切
削工具が開示されている。上記の従来表面被覆硬質合金
切削工具においては、硬質被覆層の基体に対する付着強
度が向上するため切削時の剥離現象が改善され、切削性
能の向上は得られるが、これらの被覆層では耐摩耗性が
不十分であり、近年生産性を高めるためのさらなる高速
化には応えられないのが現状である。
2. Description of the Related Art In order to improve the wear resistance of a cutting edge, a conventional surface-coated cemented carbide end mill is formed on a surface of a base material made of a cemented carbide by TiN, TiCN, (T
It is general to use an end mill in which a hard layer such as i, Al) N is coated to form a hard layer. However, the hard layer produced by the conventional coating process has a weak adhesion strength and thus lacks wear resistance. Then, as a means for further improving the adhesion strength and the wear resistance, JP-A-62-208803 has been proposed.
No. 1, a metallic Ti coating layer having an average layer thickness of 0.1 to 1 μm is formed on the surface of a hard alloy substrate made of any one of tungsten carbide based cemented carbide, titanium carbide based cermet and high speed steel. A hard coating layer having a thickness of 1 to 9 μm, and the hard coating layer having a thickness of 0.2 to 4 μm.
Disclosed is a cutting tool made of a surface-coated hard alloy, which comprises three layers of a lower layer of titanium carbide having the same, an intermediate layer of titanium carbonitride having the same 0.2 to 4 μm, and an upper layer of titanium nitride having the same 0.2 to 3 μm. Has been done. In the above conventional surface-coated hard alloy cutting tool, the peeling phenomenon at the time of cutting is improved because the adhesion strength of the hard coating layer to the substrate is improved, and the cutting performance is improved, but the wear resistance of these coating layers is improved. However, the current situation is that it cannot respond to further speeding up in recent years to improve productivity.

【0003】[0003]

【発明が解決しようとする課題】そこで、本発明は上述
のような問題点を解決するために、強靭な微粒超硬合金
母材の表面に縦長成長結晶組織を有する強度の高い炭窒
化チタンの層を被覆し、更に外層に耐溶着性に優れかつ
当該炭窒化チタンと密着性の良い酸化アルミニウムを被
覆することにより、耐摩耗性に優れ、かつ低速から高速
までの広い切削領域で使用出来る表面被覆微粒超硬エン
ドミルを提供することを目的としている。
SUMMARY OF THE INVENTION In order to solve the above problems, the present invention provides a high strength titanium carbonitride having a vertically elongated crystal structure on the surface of a tough fine grain cemented carbide base material. A surface that can be used in a wide cutting range from low speed to high speed by coating a layer, and by coating the outer layer with aluminum oxide that has excellent adhesion resistance and good adhesion with the titanium carbonitride. It is an object of the present invention to provide a coated fine cemented carbide end mill.

【0004】[0004]

【課題を解決するための手段】本発明の表面被覆微粒超
硬エンドミルは、かかる目的を達成するために、請求項
1の発明は、微粒炭化タングステン基超硬合金で構成さ
れたエンドミルの表面に、炭窒化チタンまたは窒化チタ
ンと炭窒化チタンからなる平均膜厚0.5〜3.0μm
の厚さに形成した硬質被覆層よりなる内層と、平均膜厚
0.1〜1.0μmの酸化アルミニウムからなる外層よ
り構成され、総膜厚の平均が0.6〜4.0μmであ
り、エンドミル切刃部には1〜50μmのホ−ニングが
施されていることを特徴とし、請求項2の発明は、上記
内層中の炭窒化チタン層の結晶構造を縦長成長結晶組織
または粒状結晶組織から縦長成長結晶組織へ変わる結晶
構造としたことを特徴とし、請求項3の発明は、超硬合
金母材が平均粒径0.1〜1.0μmの炭化タングステ
ンと、結合相が5〜15重量%のCo と、Cr 、V、T
a 、Nb の炭化物の1種または2種を0.3〜1.5重
量%配合した組成よりなることを特徴とする表面被覆微
粒超硬エンドミルに関するものである。
In order to achieve such an object, the surface-coated fine-grain cemented carbide end mill according to the present invention is characterized in that the surface of an end mill made of fine-grain tungsten carbide-based cemented carbide is used. , Titanium carbonitride or an average film thickness of 0.5 to 3.0 μm composed of titanium nitride and titanium carbonitride
And an outer layer composed of an aluminum oxide having an average film thickness of 0.1 to 1.0 μm, and an average total film thickness of 0.6 to 4.0 μm, The end mill cutting edge portion is subjected to honing of 1 to 50 μm, and the invention according to claim 2 is characterized in that the crystal structure of the titanium carbonitride layer in the inner layer is a vertically elongated crystal structure or a granular crystal structure. The present invention according to claim 3 is characterized in that the cemented carbide base material comprises tungsten carbide having an average grain size of 0.1 to 1.0 µm and a binder phase of 5 to 15 pieces. Wt% Co, Cr, V, T
The present invention relates to a surface-coated fine cemented carbide end mill having a composition in which one or two carbides of a and Nb are blended in an amount of 0.3 to 1.5% by weight.

【0005】[0005]

【発明の実施の形態】上記のように、強靭な微粒超硬合
金母材の表面に、靭性の高い炭窒化チタンから構成され
た内層の上にに耐摩耗性および耐溶着性の高い酸化アル
ミニウムを被覆したことにより、該表面被覆微粒超硬エ
ンドミルは、耐摩耗性に加え低速切削から高速切削まで
巾広い切削領域で使用出来、しかも大幅に寿命延長を図
れるので、生産性を大幅に向上させる利点を有するもの
である。
BEST MODE FOR CARRYING OUT THE INVENTION As described above, aluminum oxide having high wear resistance and welding resistance is formed on the surface of a tough fine-grain cemented carbide base material and on an inner layer made of titanium carbonitride having high toughness. By coating the surface-coated fine-grained carbide end mill with wear resistance, it can be used in a wide cutting range from low speed cutting to high speed cutting, and the life can be greatly extended, so productivity is greatly improved. It has advantages.

【0006】本発明は、平均粒径0.3〜1.0μmの
炭化タングステンと5〜15重量%のCoを主成分とす
る結合相からなる微粒超硬合金母材を用いてエンドミル
を形成し、切刃部表面に炭窒化チタンまたは窒化チタン
と炭窒化チタンを被覆する。内層の厚さは平均膜厚0.
5〜3.0μmとする。更に、前記内層の表面に平均膜
厚0.1〜1.0μmの酸化アルミニウムを被覆し、総
膜厚の平均は0.6〜4.0μmとする。更に、エンド
ミルの切刃には1〜50μmのホ−ニングを施して所望
の表面被覆微粒超硬エンドミルを形成したものである。
なお、内層中の炭窒化チタンの結晶構造は、基体を構成
する成分のうち少なくともWとCo を含有した縦長成長
結晶組織または粒状結晶組織から縦長成長結晶組織へ変
わる結晶構造をもったものである。なお、前記微粒炭化
タングステンの平均粒径を0.1〜1.0μmとしたの
は、0.1μmより小さいと結合相の厚みが薄くなりす
ぎて耐欠損性が低下し、また1.0μmを越えると硬度
が低下して所望の耐摩耗性が得られない。また結合相は
Co を主成分としてこれにW,Cが固溶しており、また
CrやV、Ta 、Nb の炭化物の1種または2種以上の
添加量を0.3〜1.5重量%としたのは、0.3重量
%より少ないと粒成長抑制効果に乏しく所望の耐摩耗性
が得られず、1.5重量%より多いと析出物が多くなり
耐欠損性が低下する。結合相量を5〜15重量%とした
のは、5重量%より少ないと強度が低く目的の耐チッピ
ング性が得られず、15重量%より多いと目的の耐摩耗
性が得られないうえ、高速で切削を行うと変形が生じる
ためである。チタンの窒化物や炭窒化物等からなる内層
の平均膜厚を0.5〜3.0μm好ましくは0.8〜
1.2μmとしたのは、0.5μmより薄いと目的の耐
摩耗性が得られず、3.0μmより厚いと刃先の被覆膜
が剥離またはチッピングを生じるためである。外層の酸
化アルミニウムの平均膜厚を0.1〜1.0μm好まし
くは0.1〜0.3μmとしたのは、0.1μmより薄
いと耐溶着性の効果が得られず、1.0μmより厚いと
剥離が生ずるためである。平均総膜厚を0.6〜4.0
μm好ましくは0.9〜1.5μmとしたのは、0.6
μmより薄いと目的の耐摩耗性が得られず、4.0μm
より厚いと母材と被覆膜の熱膨張係数の違いから生じる
被覆膜中の引張残留応力による被覆膜の剥離およびチッ
ピングが生じるためである。エンドミル切刃部の刃先の
ホ−ニング量を1〜50μm好ましくは10〜20μm
としたのは、ホ−ニング量が1μmより小さいとエンド
ミルの刃先先端への被覆層の局部的な厚膜化・η相の析
出が多くなり、ホ−ニング量が50μmより大きくなる
と切削抵抗が大きくなりチッピングを生じるためであ
る。
In the present invention, an end mill is formed by using a fine cemented carbide base material composed of tungsten carbide having an average particle size of 0.3 to 1.0 μm and a binder phase containing 5 to 15% by weight of Co as a main component. The surface of the cutting edge is coated with titanium carbonitride or titanium nitride and titanium carbonitride. The thickness of the inner layer is 0.
5 to 3.0 μm. Further, the surface of the inner layer is coated with aluminum oxide having an average film thickness of 0.1 to 1.0 μm, and the average of the total film thickness is set to 0.6 to 4.0 μm. Further, the cutting edge of the end mill is subjected to honing of 1 to 50 μm to form a desired surface-coated fine-grain cemented carbide end mill.
Incidentally, the crystal structure of titanium carbonitride in the inner layer has a crystal structure which changes from a vertically grown crystal structure or a granular crystal structure containing at least W and Co among the constituents of the substrate to a vertically grown crystal structure. . The average grain size of the fine-grained tungsten carbide is set to 0.1 to 1.0 μm, because when the average grain size is smaller than 0.1 μm, the thickness of the binder phase becomes too thin and the fracture resistance decreases. If it exceeds, the hardness is lowered and desired wear resistance cannot be obtained. In addition, the binder phase contains Co as a main component and W and C as a solid solution, and the addition amount of one or more carbides of Cr, V, Ta and Nb is 0.3 to 1.5 wt. If the amount is less than 0.3% by weight, the desired wear resistance cannot be obtained because the grain growth suppressing effect is poor, and if it is more than 1.5% by weight, the amount of precipitates increases and the fracture resistance decreases. The amount of the binder phase is set to 5 to 15% by weight because when the amount is less than 5% by weight, the strength is low and the desired chipping resistance cannot be obtained, and when the amount is more than 15% by weight, the desired abrasion resistance cannot be obtained. This is because deformation occurs when cutting at high speed. The average thickness of the inner layer made of titanium nitride or carbonitride is 0.5 to 3.0 μm, preferably 0.8 to 3.0 μm.
The reason for setting the thickness to 1.2 μm is that if it is thinner than 0.5 μm, the intended wear resistance cannot be obtained, and if it is thicker than 3.0 μm, the coating film at the cutting edge peels or chips. The average thickness of the outer layer of aluminum oxide is set to 0.1 to 1.0 μm, preferably 0.1 to 0.3 μm, because the effect of welding resistance cannot be obtained when the thickness is less than 0.1 μm, This is because if it is thick, peeling occurs. Average total film thickness of 0.6 to 4.0
μm, preferably 0.9 to 1.5 μm is 0.6
If it is thinner than μm, the desired wear resistance cannot be obtained, and it is 4.0 μm.
This is because if the thickness is thicker, peeling and chipping of the coating film due to the tensile residual stress in the coating film caused by the difference in thermal expansion coefficient between the base material and the coating film occur. The honing amount of the cutting edge of the end mill is 1 to 50 μm, preferably 10 to 20 μm.
The reason is that if the honing amount is less than 1 μm, the coating layer locally thickens at the tip of the end mill and the η phase precipitates more, and if the honing amount exceeds 50 μm, the cutting resistance increases. This is because it becomes large and chipping occurs.

【0007】[0007]

【実施例】表1、2、3、にそれぞれ示した基体、コ−
ティング、およびホ−ニングを施した刃先径10mm、ね
じれ角45°、2枚刃のスクエア−型エンドミルを作製
した。また比較として表1に示した基材に、イオンプレ
−ティング法により表4に示したコ−ティングを施し
た。この時ホ−ニング量は全て10μmとした。これら
のエンドミルを下記条件により切削試験を行い、その結
果を表3、表4に示す。欠損本数は10本中の欠損を生
じた本数で、2枚刃のうちの1枚でも欠損が生じた場合
1本とした。また外周刃摩耗量は、チッピングを生じた
部分も含め、最大摩耗量とした。 切削速度 :120m/min. 1刃当たりの送り:0.04mm/刃 切込み深さ:15mm 切込み幅 :1mm 被削材 :S50C ク−ラント:水溶性 ダウンカット 切削長 :30m
EXAMPLES The substrates and cores shown in Tables 1, 2, and 3, respectively.
A square-type end mill having a blade edge diameter of 10 mm, a helix angle of 45 °, and a two-blade blade was manufactured by subjecting to cutting and honing. For comparison, the base material shown in Table 1 was coated with the coating material shown in Table 4 by the ion plating method. At this time, the amount of honing was 10 μm. A cutting test was performed on these end mills under the following conditions, and the results are shown in Tables 3 and 4. The number of defects was 10 out of 10 and was defined as 1 when one of the two blades was damaged. The amount of wear of the outer peripheral blade was set to the maximum amount of wear, including the portion where chipping occurred. Cutting speed: 120m / min. Feed per blade: 0.04mm / blade Cutting depth: 15mm Cutting width: 1mm Work material: S50C coolant: Water-soluble downcut Cutting length: 30m

【0008】[0008]

【表1】 [Table 1]

【0009】[0009]

【表2】 [Table 2]

【0010】[0010]

【表3】 [Table 3]

【0011】[0011]

【表4】 [Table 4]

【0012】[0012]

【発明の効果】本発明は強靭な微粒超硬合金母材の表面
に、靭性の高い炭窒化チタン、または窒化チタンと該高
靭性炭窒化チタンで被覆された内層で構成され、かつ内
層の被覆層の結晶構造を縦長成長結晶組織または粒状結
晶組織から縦長成長結晶組織へ変わる結晶構造とし、外
層に耐酸化性に優れた酸化アルミニウムを被覆する組み
合わせにより、表1〜4に示されるとおり耐欠損性およ
び耐摩耗性を向上させた表面被覆微粒超硬エンドミルを
得ることができた。
INDUSTRIAL APPLICABILITY The present invention comprises, on the surface of a tough fine-grain cemented carbide base material, titanium carbonitride having high toughness, or an inner layer coated with titanium nitride and the high-toughness titanium carbonitride, and coating the inner layer. The layer has a crystal structure that changes from a vertically grown crystal structure or a granular crystal structure to a vertically grown crystal structure, and the outer layer is coated with aluminum oxide having excellent oxidation resistance. It was possible to obtain a surface-coated fine-grain cemented carbide end mill with improved wear resistance and wear resistance.

Claims (3)

【特許請求の範囲】[Claims] 【請求項1】 微粒炭化タングステン基超硬合金で構成
されたエンドミルの表面に、炭窒化チタンまたは窒化チ
タンと炭窒化チタンからなる平均膜厚0.5〜3.0μ
mの厚さに形成した硬質被覆層よりなる内層と、平均膜
厚0.1〜1.0μmの酸化アルミニウムからなる外層
より構成され、総膜厚の平均が0.6〜4.0μmであ
り、エンドミル切刃部には1〜50μmのホ−ニングが
施されていることを特徴とする表面被覆微粒超硬合金製
エンドミル。
1. An average film thickness of 0.5 to 3.0 μm made of titanium carbonitride or titanium nitride and titanium carbonitride on the surface of an end mill composed of fine-grained tungsten carbide based cemented carbide.
and an outer layer made of aluminum oxide having an average film thickness of 0.1 to 1.0 μm and having an average total film thickness of 0.6 to 4.0 μm. A surface-coated fine-grain cemented carbide end mill, characterized in that the end mill cutting edge portion is subjected to honing of 1 to 50 μm.
【請求項2】 請求項1に記載の表面被覆微粒超硬合金
製エンドミルにおいて、上記内層中の炭窒化チタン層の
結晶構造を、縦長成長結晶組織または粒状結晶組織から
縦長成長結晶組織へ変わる結晶構造としたことを特徴と
する表面被覆微粒超硬エンドミル。
2. The surface-coated fine grain cemented carbide end mill according to claim 1, wherein the crystal structure of the titanium carbonitride layer in the inner layer is changed from a vertically elongated crystal structure or a granular crystal structure to a vertically grown crystal structure. Surface-coated fine-grain carbide end mill characterized by having a structure.
【請求項3】 請求項1に記載の表面被覆微粒超硬合金
製エンドミルにおいて、超硬合金母材が平均粒径0.1
〜1.0μmの炭化タングステンと、結合相が5〜15
重量%のCoと、Cr 、V、Ta 、Nb の炭化物の1種
または2種を0.3〜1.5重量%配合した組成よりな
ることを特徴とする表面被覆微粒超硬合金製エンドミ
ル。
3. The surface-coated fine grain cemented carbide end mill according to claim 1, wherein the cemented carbide base material has an average grain size of 0.1.
.About.1.0 .mu.m tungsten carbide and 5 to 15 binder phases
A surface-coated fine-grain cemented carbide end mill having a composition in which 0.3% to 1.5% by weight of Co and 1 or 2 types of carbides of Cr, V, Ta, and Nb are blended.
JP6460796A 1996-03-21 1996-03-21 Surface coated fine grain cemented carbide end mill Pending JPH09253916A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP6460796A JPH09253916A (en) 1996-03-21 1996-03-21 Surface coated fine grain cemented carbide end mill

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP6460796A JPH09253916A (en) 1996-03-21 1996-03-21 Surface coated fine grain cemented carbide end mill

Publications (1)

Publication Number Publication Date
JPH09253916A true JPH09253916A (en) 1997-09-30

Family

ID=13263127

Family Applications (1)

Application Number Title Priority Date Filing Date
JP6460796A Pending JPH09253916A (en) 1996-03-21 1996-03-21 Surface coated fine grain cemented carbide end mill

Country Status (1)

Country Link
JP (1) JPH09253916A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20040068476A (en) * 2003-01-24 2004-07-31 산드빅 악티에볼라그 Coated cemented carbide insert
JP2014104545A (en) * 2012-11-28 2014-06-09 Kyocera Corp Coated tool

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20040068476A (en) * 2003-01-24 2004-07-31 산드빅 악티에볼라그 Coated cemented carbide insert
JP2004223711A (en) * 2003-01-24 2004-08-12 Sandvik Ab Cutting tool insert
JP2014104545A (en) * 2012-11-28 2014-06-09 Kyocera Corp Coated tool

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