JPH0711438A - Method and device for forming film while controlling temperature of substrate - Google Patents
Method and device for forming film while controlling temperature of substrateInfo
- Publication number
- JPH0711438A JPH0711438A JP15833793A JP15833793A JPH0711438A JP H0711438 A JPH0711438 A JP H0711438A JP 15833793 A JP15833793 A JP 15833793A JP 15833793 A JP15833793 A JP 15833793A JP H0711438 A JPH0711438 A JP H0711438A
- Authority
- JP
- Japan
- Prior art keywords
- substrate
- shutter
- film formation
- temp
- gaseous
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
Description
【0001】[0001]
【産業上の利用分野】本発明はシャッター開閉前後及び
成膜中の基板温度を一定に保つ成膜方法及びその装置に
関するものである。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a film forming method and apparatus for keeping the substrate temperature constant before and after opening and closing a shutter and during film formation.
【0002】[0002]
【従来の技術】プラズマを利用した従来の成膜装置では
基板温度の制御を以下のように行っている。 1.温度を制御した基板ホルダーに基板を接触させる。 2.基板裏面よりヒーターで加熱する。2. Description of the Related Art In a conventional film forming apparatus using plasma, the substrate temperature is controlled as follows. 1. The substrate is brought into contact with the substrate holder whose temperature is controlled. 2. Heat from the back of the substrate with a heater.
【0003】[0003]
【発明が解決しようとする課題】ところがこれらの成膜
装置では、基板がプラズマ及び蒸着粒子に曝されるため
成膜中に基板の温度が上昇する。この温度上昇によって
所望の膜質が得られなかったり、基板と薄膜の間に熱応
力が発生したりする。成膜前に成膜防止用シャッターを
閉じて基板を長時間プラズマに曝すと基板は熱平衡状態
に達するが、シャッターを開けることによってプラズマ
の密度変化や蒸着粒子のエネルギーによって基板温度が
変化する。この基板温度の変化によって熱応力が発生し
たり、膜の性質が変わったりする。However, in these film forming apparatuses, the temperature of the substrate rises during film formation because the substrate is exposed to plasma and vapor deposition particles. Due to this temperature rise, desired film quality cannot be obtained, or thermal stress is generated between the substrate and the thin film. If the shutter for film formation prevention is closed and the substrate is exposed to plasma for a long time before film formation, the substrate reaches a thermal equilibrium state, but when the shutter is opened, the substrate temperature changes due to the density change of plasma and the energy of vapor deposition particles. Due to the change in the substrate temperature, thermal stress is generated or the property of the film is changed.
【0004】本発明は、これらの問題点を解決するため
シャッター開閉前後、及び成膜中の基板温度を一定に保
つ装置を提供することを目的とする。An object of the present invention is to provide an apparatus for solving these problems, which keeps the substrate temperature constant before and after opening / closing the shutter and during film formation.
【0005】[0005]
【課題を解決するための手段】本発明では基板裏面にス
パッタリングガス又は不活性なガスを流すことによって
基板温度を一定に保つと同時にシャッターにヒーターを
設けることによってシャッター開閉に伴う基板表面に与
えられる熱量の変化を防いでいる。According to the present invention, a sputtering gas or an inert gas is caused to flow on the back surface of a substrate to keep the substrate temperature constant, and at the same time, a heater is provided on the shutter to provide the substrate surface with opening and closing of the shutter. Prevents changes in the amount of heat.
【0006】[0006]
【作用】基板温度制御にガスを用いると温度平衡に達す
る時間が短く、様々な温度が設定できる。またシャッタ
ーにヒーターがついているとシャッター開閉前後に基板
に与えられる熱量が変化しないので基板温度が変化しな
い。実際の成膜をする前に、ヒーターを何℃に加熱すれ
ばシャッター開閉前後及び成膜中の基板温度を一定に保
つことができるかを条件にしておく。When a gas is used for controlling the substrate temperature, it takes a short time to reach temperature equilibrium and various temperatures can be set. If the shutter is equipped with a heater, the amount of heat applied to the substrate does not change before and after the shutter is opened and closed, so the substrate temperature does not change. Before the actual film formation, a condition is set at what temperature the heater can be heated to keep the substrate temperature before and after opening and closing the shutter and during the film formation constant.
【0007】[0007]
【実施例】以下、図1に示す実施例によりスパッタリン
グ法によるTaの成膜方法を説明する。EXAMPLE A Ta film forming method by the sputtering method will be described below with reference to the example shown in FIG.
【0008】低応力なTa膜を得るために、RFパワー
を1.0kW、スパッタガス1であるXeのガス圧を
0.5Pa、基板温度は200℃に設定する。基板温度
を200℃に保つために180℃のXeガスを基板裏面
に流す。成膜中はプラズマ及び蒸着粒子から与えられる
エネルギーと180℃のガスから与えられる熱によって
基板温度は平衡状態に達し200℃に制御される。成膜
前の防着シャッター4が閉じられた状態では、内蔵され
たヒーター3によって300℃に加熱されたシャッター
4と180℃のガス1によって基板温度は200℃に保
たれる。この様に、スパッタリング中にプラズマ及び蒸
着粒子から与えられるエネルギーとヒーター内蔵のシャ
ッターから与えられるエネルギーが等しくなる様にする
と、プリスパッタリング時から成膜終了まで基板温度を
一定に保つことができる。そのことによって薄膜中の熱
応力や膜質を安定にコントロールすることが可能にな
る。In order to obtain a Ta film with low stress, the RF power is set to 1.0 kW, the gas pressure of Xe which is the sputtering gas 1 is set to 0.5 Pa, and the substrate temperature is set to 200 ° C. In order to keep the substrate temperature at 200 ° C., 180 ° C. Xe gas is flown to the back surface of the substrate. During film formation, the substrate temperature reaches an equilibrium state and is controlled to 200 ° C. by the energy given by the plasma and vapor deposition particles and the heat given by the gas at 180 ° C. When the deposition-preventing shutter 4 before film formation is closed, the substrate temperature is kept at 200 ° C. by the shutter 4 heated to 300 ° C. by the built-in heater 3 and the gas 1 at 180 ° C. In this way, if the energy given by plasma and vapor deposition particles during sputtering is made equal to the energy given by the shutter built into the heater, the substrate temperature can be kept constant from the time of pre-sputtering to the end of film formation. This makes it possible to stably control the thermal stress and film quality in the thin film.
【0009】[0009]
【発明の効果】以上述べてきたように、本発明によれ
ば、成膜中の基板温度を極めて安定に制御することが可
能なので、薄膜中の熱応力や熱による膜質の変化の影響
を著しく低減することができる。なお、実施例では基板
温度制御のガスとしてスパッタガスと同じXeを用いた
が、He,Ar、等ターゲット材料に対して不活性な他
のガスを用いてもよい。As described above, according to the present invention, since the substrate temperature during film formation can be controlled extremely stably, the influence of the thermal stress in the thin film and the change of the film quality due to the heat is remarkable. It can be reduced. Although Xe, which is the same as the sputtering gas, is used as the substrate temperature control gas in the embodiments, other gases such as He and Ar that are inert to the target material may be used.
【図1】本発明の基板温度制御装置の概略図である。FIG. 1 is a schematic diagram of a substrate temperature control device of the present invention.
1 スパッタガス 2 ウエハ 3 ヒーター 4 シャッター 5 ターゲット 1 Sputtering gas 2 Wafer 3 Heater 4 Shutter 5 Target
Claims (2)
ーにヒーターを設けて成膜前に基板を加熱しておくこと
によってシャッター開閉直後及び成膜中の基板温度を一
定に保つことを特徴とする成膜方法。1. A substrate temperature is kept constant immediately after opening and closing of the shutter and during film formation by flowing gas to the back surface of the substrate and further providing a heater on the shutter to heat the substrate before film formation. Deposition method.
徴とする成膜装置。2. A film forming apparatus comprising a shutter provided with a heater.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP15833793A JPH0711438A (en) | 1993-06-29 | 1993-06-29 | Method and device for forming film while controlling temperature of substrate |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP15833793A JPH0711438A (en) | 1993-06-29 | 1993-06-29 | Method and device for forming film while controlling temperature of substrate |
Publications (1)
Publication Number | Publication Date |
---|---|
JPH0711438A true JPH0711438A (en) | 1995-01-13 |
Family
ID=15669435
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP15833793A Pending JPH0711438A (en) | 1993-06-29 | 1993-06-29 | Method and device for forming film while controlling temperature of substrate |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPH0711438A (en) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2011084768A (en) * | 2009-10-14 | 2011-04-28 | Stanley Electric Co Ltd | Film deposition apparatus, and method for manufacturing ferroelectric film |
JP2022525635A (en) * | 2019-03-22 | 2022-05-18 | アプライド マテリアルズ インコーポレイテッド | Methods and equipment for depositing metal nitrides |
US11437559B2 (en) | 2019-03-22 | 2022-09-06 | Applied Materials, Inc. | Method and apparatus for deposition of multilayer device with superconductive film |
US11653576B2 (en) | 2020-02-03 | 2023-05-16 | Applied Materials, Inc. | SNSPD with integrated aluminum nitride seed or waveguide layer |
US11788883B2 (en) | 2020-02-03 | 2023-10-17 | Applied Materials, Inc. | SNSPD with integrated aluminum nitride seed or waveguide layer |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6354790A (en) * | 1986-08-26 | 1988-03-09 | Toshiba Corp | Laser oscillator |
JP4088034B2 (en) * | 2000-12-22 | 2008-05-21 | 用 西村 | Nuisance call monitoring system, nuisance call monitoring method, and computer-readable recording medium recording program for causing computer to execute the method |
-
1993
- 1993-06-29 JP JP15833793A patent/JPH0711438A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6354790A (en) * | 1986-08-26 | 1988-03-09 | Toshiba Corp | Laser oscillator |
JP4088034B2 (en) * | 2000-12-22 | 2008-05-21 | 用 西村 | Nuisance call monitoring system, nuisance call monitoring method, and computer-readable recording medium recording program for causing computer to execute the method |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2011084768A (en) * | 2009-10-14 | 2011-04-28 | Stanley Electric Co Ltd | Film deposition apparatus, and method for manufacturing ferroelectric film |
JP2022525635A (en) * | 2019-03-22 | 2022-05-18 | アプライド マテリアルズ インコーポレイテッド | Methods and equipment for depositing metal nitrides |
US11437559B2 (en) | 2019-03-22 | 2022-09-06 | Applied Materials, Inc. | Method and apparatus for deposition of multilayer device with superconductive film |
US11739418B2 (en) * | 2019-03-22 | 2023-08-29 | Applied Materials, Inc. | Method and apparatus for deposition of metal nitrides |
US11778926B2 (en) | 2019-03-22 | 2023-10-03 | Applied Materials, Inc. | Method and apparatus for deposition of multilayer device with superconductive film |
US11653576B2 (en) | 2020-02-03 | 2023-05-16 | Applied Materials, Inc. | SNSPD with integrated aluminum nitride seed or waveguide layer |
US11788883B2 (en) | 2020-02-03 | 2023-10-17 | Applied Materials, Inc. | SNSPD with integrated aluminum nitride seed or waveguide layer |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
A02 | Decision of refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A02 Effective date: 19961119 |