JPH0653048B2 - Manufacturing method of low-calorie sugar containing stevia sweetener - Google Patents

Manufacturing method of low-calorie sugar containing stevia sweetener

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Publication number
JPH0653048B2
JPH0653048B2 JP61062049A JP6204986A JPH0653048B2 JP H0653048 B2 JPH0653048 B2 JP H0653048B2 JP 61062049 A JP61062049 A JP 61062049A JP 6204986 A JP6204986 A JP 6204986A JP H0653048 B2 JPH0653048 B2 JP H0653048B2
Authority
JP
Japan
Prior art keywords
sugar
stevia sweetener
stevia
sweetener
aqueous solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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JP61062049A
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Japanese (ja)
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JPS62220167A (en
Inventor
孝親 増井
良一 加地
Original Assignee
新光製糖株式会社
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Priority to JP61062049A priority Critical patent/JPH0653048B2/en
Publication of JPS62220167A publication Critical patent/JPS62220167A/en
Publication of JPH0653048B2 publication Critical patent/JPH0653048B2/en
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Expired - Fee Related legal-status Critical Current

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Description

【発明の詳細な説明】 産業上の利用分野 この発明は、ステビア甘味料の添加量と顆粒化に伴う容
積の増大量とを調節することにより容積当りの甘味度を
そのまま保ってカロリーだけを低減した低カロリー砂糖
の製造法に関するものである。
TECHNICAL FIELD The present invention controls the amount of Stevia sweetener added and the amount of increase in volume associated with granulation to maintain the sweetness per volume and reduce only calories. The present invention relates to a method for producing low calorie sugar.

この明細書全体を通して「ステビア甘味料」とは、南米
産のキク科の多年性植物ステビア・レバウディアナ・バ
ルトニ(Stevia rebaudiana Bartoni)から抽出された甘
味成分であって、ステビオサイド、レバウディオサイド
−Aなどのいくつかの同族体よりなるステビオール骨格
の配糖体を意味し、ステビオサイドに少なくとも一部が
レバウディオサイド−Aに転化されたものも含まれる。
Throughout this specification, "Stevia sweetener" is a sweet component extracted from Stevia rebaudiana Bartoni, a perennial plant of the Asteraceae family from South America, which includes stevioside and rebaudioside-A. And the like, which means a glycoside having a steviol skeleton consisting of several homologues thereof, and includes those in which at least a part of stevioside is converted to rebaudioside-A.

発明の背景 砂糖は種々の飲食物、嗜好物などに添加される代表的な
甘味料であるが、近年、砂糖の多過使用によるカロリー
の摂り過ぎ、さらにこれに起因する肥満や健康阻害など
が問題視されて来ており、そのため容積当りの甘味度を
そのまま保って、カロリーだけを低減した低カロリー砂
糖が要望されている。そしてこのような要望にこたえる
ものとして、甘味度が砂糖の甘味度の100倍程度であ
るステビア甘味料をごく微量砂糖に加えてなる低カロリ
ー砂糖が脚光を浴びている。
Background of the Invention Sugar is a typical sweetener that is added to various foods and drinks, tastes and the like, but in recent years, excessive intake of calories due to excessive use of sugar, and further obesity and poor health caused by it have been observed. There is a growing concern that there is a need for low-calorie sugar that retains the sweetness per unit volume and reduces only calories. In order to meet such a demand, low-calorie sugar obtained by adding a very small amount of stevia sweetener having a sweetness of about 100 times that of sugar to the sugar is in the spotlight.

従来技術およびその問題点 従来、ステビア甘味料入りの低カロリー砂糖を得るに
は、所要濃度のステビア甘味料水溶液を顆粒状の砂糖や
グラニュー糖のようなハードシュガーに撹拌下に噴霧し
て粒子の表面にステビアのコーティング層を形成する方
法(I)や、結晶状の砂糖をステビア甘味料の水溶液と
混練して、結晶の表面にステビア甘味料のコーティング
層を形成する(II)などが提案されている。
Conventional technology and its problems Conventionally, in order to obtain low-calorie sugar containing stevia sweetener, an aqueous solution of stevia sweetener having a required concentration is sprayed on hard sugar such as granular sugar or granulated sugar under stirring to form particles of particles. A method of forming a coating layer of stevia on the surface (I) and a method of forming a coating layer of stevia sweetener on the surface of crystals by kneading crystalline sugar with an aqueous solution of stevia sweetener (II) have been proposed. ing.

しかしながら、これらの方法では、ステビア甘味料は砂
糖の顆粒ないし結晶の表面にはコーティングされるが、
結晶の内部には収蔵されなかった。そのため、このよう
なステビア甘味料入り砂糖をたとえばコーヒー砂糖とし
て使用すると、コーティング層をなすステビア甘味料が
最初に溶解し、砂糖甘味とは異質のステビア特有の甘味
が強く現われた。そのため、このステビア甘味料入り砂
糖がほぼ全体溶解するまでは、ステビア甘味料に起因す
る甘味の違和感があった。
However, in these methods, stevia sweetener is coated on the surface of sugar granules or crystals,
It was not stored inside the crystal. Therefore, when such stevia sweetener-containing sugar is used as, for example, coffee sugar, the stevia sweetener forming the coating layer is first dissolved, and a sweet taste peculiar to stevia, which is different from sugar sweetness, appears strongly. Therefore, until the sugar containing the Stevia sweetener was almost entirely dissolved, there was a feeling of strangeness in sweetness due to the Stevia sweetener.

またこれらの製造法では砂糖は終始固相で処理されるの
で、均質なステビア甘味料入り製品を得るのがはなはだ
困難であった。
In addition, since sugar is always processed in a solid phase in these production methods, it is extremely difficult to obtain a homogeneous stevia-sweetened product.

この発明は、以上の如き諸問題を解決して、使用時にス
テビア甘味料に起因する甘味の違和感を生じるおそれが
ない均質なステビア甘味料入り低カロリー砂糖の製造法
を提供することを目的とする。
It is an object of the present invention to solve the above problems and provide a method for producing a homogeneous low calorie sugar containing stevia sweetener, which does not cause a feeling of strangeness in sweetness caused by stevia sweetener during use. .

問題点の解決手段 この発明によるステビア甘味料入りの低カロリー砂糖の
製造法は、純糖率85%以上の蔗糖の水溶液を沸点が大
気圧下に124〜134℃に達するまで濃縮する工程
と、得られた濃縮糖液にステビア甘味料の水溶液を加え
る工程と、濃縮糖液を撹拌して水分の蒸発により冷却し
結晶を析出せしめる工程と、得られた結晶の粉粒物を解
砕し、解砕物を乾燥しついで分級して顆粒を得る工程と
よりなる。
Solution to Problem A method for producing low-calorie sugar containing stevia sweetener according to the present invention comprises a step of concentrating an aqueous solution of sucrose having a pure sugar rate of 85% or more until the boiling point thereof reaches 124 to 134 ° C. under atmospheric pressure, A step of adding an aqueous solution of stevia sweetener to the obtained concentrated sugar solution, a step of stirring the concentrated sugar solution and cooling by evaporating water to precipitate crystals, and crushing the obtained crystal powder and granules, The crushed product is dried and then classified to obtain granules.

この発明の方法によって製造された砂糖は、表面にステ
ビア甘味料をコーティングしかつ内部にステビア甘味料
を収蔵した蔗糖の微細結晶よりなる顆粒状のものであ
る。こうして得られた低カロリー砂糖において、ステビ
ア甘味料の割合は、好ましくは砂糖の0.2〜1.0重
量%である。その理由は、0.2重量%未満では、充分
なカロリリー低減効果が得られず、また逆に1.0重量
%を越えると、砂糖の容積を通常の容積の2倍以上に増
大させなければならず、実用的でないからである。特に
好ましい割合は0.3〜0.5重量%である。
The sugar produced by the method of the present invention is in the form of granules composed of fine crystals of sucrose having a stevia sweetener coated on the surface and containing the stevia sweetener inside. In the low calorie sugar thus obtained, the proportion of stevia sweetener is preferably 0.2 to 1.0% by weight of sugar. The reason is that if it is less than 0.2% by weight, a sufficient calorie reducing effect cannot be obtained, and conversely, if it exceeds 1.0% by weight, the volume of sugar must be increased to more than twice the normal volume. Because it is not practical. A particularly desirable ratio is 0.3 to 0.5% by weight.

ステビア甘味料は安全性の高い天然物であり、砂糖の甘
味になじみやすい甘味を有し、調理、製菓、飲料などへ
の添加における加熱条件や広いpH範囲に対して極めて安
定な物質である。
Stevia sweetener is a highly safe natural product, has a sweetness that easily blends in with the sweetness of sugar, and is an extremely stable substance under heating conditions and a wide pH range when added to cooking, confectionery, beverages and the like.

発明の作用・効果 この発明による製造法は、純糖率85%以上の蔗糖の水
溶液を沸点が大気圧下に124〜134℃に達するまで
濃縮する工程と、得られた濃縮糖液にステビア甘味料の
水溶液を加える工程と、濃縮糖液を撹拌して水分の蒸発
により冷却し結晶を析出せしめる工程を具備しているの
で、ステビア甘味料の一部は結晶の析出過程において内
部に残留し、結晶内に収蔵される。そのためこの発明に
よるステビア甘味料入り砂糖では、上述した従来技術に
よるステビア甘味料コーティング砂糖に比べて、砂糖の
溶解過程における蔗糖の溶出割合が大きくなり、ステビ
ア甘味料特有の甘味が大幅に弱められる。
Action and effect of the invention The production method according to the present invention comprises a step of concentrating an aqueous solution of sucrose having a pure sugar rate of 85% or more until the boiling point thereof reaches 124 to 134 ° C under atmospheric pressure, and stevia sweetness in the obtained concentrated sugar solution. Since it has a step of adding an aqueous solution of an ingredient and a step of stirring the concentrated sugar solution and cooling it by evaporating water to precipitate crystals, part of the stevia sweetener remains inside during the crystal precipitation process, It is stored in the crystal. Therefore, in the stevia sweetener-containing sugar according to the present invention, the elution ratio of sucrose in the dissolution process of sugar is higher than that of the above-described conventional stevia sweetener-coated sugar, and the sweetness peculiar to stevia sweetener is significantly weakened.

またこの発明による製造法は、結晶析出後、結晶の粉粒
物を解砕し、解砕物を乾燥しついで分級して顆粒を得る
工程を具備するので、得られた顆粒製品は極めて速い溶
解速度を示す。
Further, since the production method according to the present invention comprises the steps of crushing the crystal powder after crystal precipitation, drying the crushed material, and then classifying to obtain granules, the obtained granular product has an extremely high dissolution rate. Indicates.

したがって、この発明によれば、上述のようにステビア
甘味料特有の甘味が弱い点と顆粒状に起因する優れた溶
解性とが相俟って、先に述べた問題点、すなわち、ステ
ビア特有の甘味に起因する甘味の違和感を可及的になく
することができる。
Therefore, according to the present invention, as described above, the weak sweetness peculiar to Stevia sweetener and the excellent solubility due to the granular form are combined, and the above-mentioned problem, namely, Stevia peculiar to It is possible to eliminate the unpleasant sensation of sweetness due to the sweetness.

またこの発明の製造法では、上述の如く、濃縮糖液とス
テビア甘味料の水溶液を液相どうしで撹拌混合するの
で、全体に均質なステビア甘味料入り製品を得ることが
できる。
Further, in the production method of the present invention, as described above, the concentrated sugar solution and the aqueous solution of stevia sweetener are stirred and mixed in the liquid phase, so that a product containing stevia sweetener which is homogeneous throughout can be obtained.

さらに、この発明の製造法によって得られた製品は顆粒
状をなすので、上述の如く優れた溶解性を有し、かつ
「だま」と呼ばれる塊状部を生じにくいうえに、顆粒化
に伴う容積の増大量を調節することにより、従来の砂糖
と同じ目分量で取って使用することができて、極めて使
い勝手がよい。
Furthermore, since the product obtained by the production method of the present invention is in the form of granules, it has excellent solubility as described above, and it is difficult to form a lump called "dama", and the volume accompanying granulation is reduced. By adjusting the amount of increase, it can be taken in the same amount as conventional sugar and used, which is extremely convenient.

実施例 つぎに、上記効果を実証するために、この発明の実施例
および従来技術を示す比較例を挙げ、さらにこれらを比
較する官能試験の結果を示す。
Example Next, in order to demonstrate the above-mentioned effect, an example of the present invention and a comparative example showing a conventional technique will be given, and the results of a sensory test comparing these will be shown.

実施例 上白糖500gを蒸発皿にとり、これに水235mを
加えて上白糖を加温溶解させた。得られた糖水溶液を室
温に冷却した後、アルカリの添加により液のpHを7.0
に調整した。
Example 500 g of white sucrose was placed in an evaporating dish, and 235 m of water was added thereto to dissolve the white sucrose by heating. The obtained sugar aqueous solution was cooled to room temperature, and then the pH of the solution was adjusted to 7.0 by adding an alkali.
Adjusted to.

糖水溶液を大匙で撹拌しながら、蒸発皿を強火で加熱し
て、糖水溶性液の濃縮を行なった。8分後糖水溶液が沸
騰し始め、16分後沸点が127℃に達したので、この
時点で濃縮を終え、水分含量約9%の濃縮糖液を得た。
While stirring the sugar aqueous solution in a large spoon, the evaporation dish was heated on high heat to concentrate the sugar aqueous solution. After 8 minutes, the aqueous sugar solution started to boil, and after 16 minutes, the boiling point reached 127 ° C., so the concentration was completed at this point, and a concentrated sugar solution having a water content of about 9% was obtained.

他方、市販のステビア甘味料(商品名「SKスイート」
山陽国策パルプ社製)20gを水100mに溶かし
て、ステビア甘味料の水溶液を調製し、この水溶液10
mを上記濃縮糖液にゆっくり加えた。
On the other hand, commercially available Stevia sweetener (trade name "SK Suite")
Sanyo Kokusaku Pulp Co., Ltd.) (20 g) was dissolved in 100 m of water to prepare an aqueous solution of stevia sweetener.
m was slowly added to the above concentrated sugar solution.

ついで濃縮糖液を強く撹拌して、水分を蒸発させた。そ
の結果、水分の蒸発によって濃縮糖液から蒸発潜熱が奪
われて同液が冷却され、撹拌開始後約1分で蒸発皿の壁
面に蔗糖の微細結晶が現われ、以後2分間の撹拌で濃縮
糖液全体がスラリー化した。さらに約4分間撹拌を続け
たところ、スラリーは約50℃まで冷却され、粉状物か
ら直径2〜3cmの塊までの種々の大きさの脆い粉粒物が
生成した。
Then, the concentrated sugar solution was vigorously stirred to evaporate the water. As a result, the latent heat of vaporization was removed from the concentrated sugar liquid by the evaporation of water, and the liquid was cooled. Fine crystals of sucrose appeared on the wall of the evaporation dish about 1 minute after the start of stirring, and then the concentrated sugar was stirred for 2 minutes. The entire liquid turned into a slurry. When stirring was continued for about 4 more minutes, the slurry was cooled to about 50 ° C., and brittle powder particles of various sizes from powder to lumps having a diameter of 2 to 3 cm were formed.

得られた粉粒物を蒸発皿から平らな底を有する金属製の
大皿に移して、金属製のローラで十分に解砕した。得ら
れた解砕物を温度40℃で30分間時々掻き混ぜながら
風乾した。ついで乾燥した解砕物を室温まで放冷した
後、28メッシュ(開き目590μ)の篩で分級し、篩
上残をローラで解砕して分級を繰り返し、全部篩を通過
させた。
The obtained granules were transferred from the evaporating dish to a metal plate having a flat bottom and sufficiently crushed with a metal roller. The obtained crushed product was air-dried at a temperature of 40 ° C. for 30 minutes with occasional stirring. Then, the dried crushed product was allowed to cool to room temperature, then classified with a 28-mesh (opening 590μ) sieve, and the residue on the sieve was crushed with a roller to repeat the classification, and all were passed through the sieve.

こうして顆粒状のステビア甘味料入り砂糖(A)494
gを得た。
In this way, granulated Stevia sweetener-containing sugar (A) 494
g was obtained.

比較例1 この製造法は本書冒頭で述べた従来技術の製造法(I)
に相当する。
Comparative Example 1 This manufacturing method is the conventional manufacturing method (I) described at the beginning of this document.
Equivalent to.

上記実施例の製造法において、ステビア甘味料の添加を
行なわないで、その他の点を実施例と同様に操作し、顆
粒状の砂糖500gを得た。
In the production method of the above-mentioned example, the addition of stevia sweetener was not carried out, and the other points were the same as in the example to obtain 500 g of granular sugar.

ついで実施例で用いたステビア甘味料の水溶液(水10
0m中に20g)10mを撹拌下に上記顆粒砂糖に
散布し、顆粒砂糖の表面にステビア甘味料をコーティン
グした。得られたコーティング顆粒を40℃で60分間
時々掻き混ぜながら風乾し、ついで室温まで放冷した。
Then, an aqueous solution of stevia sweetener (water 10
20 g in 10 m) and 10 m were sprinkled onto the above-mentioned granular sugar with stirring, and the surface of the granular sugar was coated with a stevia sweetener. The resulting coated granules were air dried at 40 ° C. for 60 minutes with occasional agitation and then allowed to cool to room temperature.

こうしてステビア甘味料コーティング顆粒砂糖(B)5
01gを得た。
In this way Stevia sweetener coated granule sugar (B) 5
01 g was obtained.

比較例2 この比較例は本書冒頭で述べた従来技術の製造法(II)
に相当する。
Comparative Example 2 This comparative example is based on the conventional manufacturing method (II) described at the beginning of this document.
Equivalent to.

実施例で用いた上白糖500gに、やはり実施例で用い
たステビア甘味料の水溶液(水100m中に20g)
10mを混練下にゆっくり散布して混練を20分続
け、ステビア甘味料を上白糖の結晶表面にコーティング
した。得られたコーティング上白糖を40℃で60分間
時々掻き混ぜながら風乾し、ついで室温まで放冷した。
こうしてステビア甘味料コーティング上白糖(C)50
0gを得た。
An aqueous solution of the stevia sweetener also used in the examples (20 g in 100 m of water) was added to 500 g of the white sucrose used in the examples.
10 m was slowly sprinkled under kneading and the kneading was continued for 20 minutes to coat Stevia sweetener on the surface of the crystals of upper sucrose. The resulting coated sucrose was air dried at 40 ° C. for 60 minutes with occasional agitation, and then allowed to cool to room temperature.
In this way, white sugar (C) 50 on Stevia sweetener coating
0 g was obtained.

官能試験 つぎに上記実施例および比較例1、2の製造法によって
それぞれ得られた顆粒状ステビア甘味料入り砂糖
(A)、ステビア甘味料コーティング顆粒砂糖(B)お
よびステビア甘味料コーティング上白糖(C)につい
て、官能試験を行なった。また実施例で用いた上白糖
(D)も試験対象とした。
Sensory test Next, the granular stevia sweetener-containing sugar (A), the stevia sweetener-coated granule sugar (B), and the stevia sweetener-coated white sugar (C) obtained by the production methods of the above Examples and Comparative Examples 1 and 2, respectively. ) Was subjected to a sensory test. The white sucrose (D) used in the examples was also tested.

試験方法は、ステビア甘味料特有の甘味に対して鋭敏な
感受性を持つパネルメンバー12名が、薬包紙に包み込
んだ上記砂糖(A)(B)(C)(D)の各試料5gを
ランダムに抽出して直接試食し、ステビア甘味料特有の
甘味を強く感じた試料から順に1、2、3、および4の
番号を付すことによって行なった。
The test method was as follows. Twelve panel members having a sensitive sensitivity to the sweetness peculiar to Stevia sweetener randomly selected 5 g of each sample of the sugar (A) (B) (C) (D) wrapped in a medicine packing paper. The samples were directly tasted and were numbered 1, 2 and 3 in order from the sample in which the sweetness peculiar to Stevia sweetener was strongly felt.

試験結果はつぎの表1に示すとおりである。The test results are shown in Table 1 below.

上記表1から明らかなように、実施例で得られた顆粒状
ステビア甘味料入り砂糖(A)は、比較例で得られたス
テビア甘味料コーティング顆粒砂糖(B)およびステビ
ア甘味料コーティング上白糖(C)に比べて、ステビア
甘味料特有の甘味が弱いものであることがわかる。
As is clear from Table 1 above, the sugar (A) containing the granular stevia sweetener obtained in the Examples was the stevia sweetener-coated granule sugar (B) and the stevia sweetener-coated white sugar ( It can be seen that the sweetness peculiar to Stevia sweetener is weaker than that of C).

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】純糖率85%以上の蔗糖の水溶液を沸点が
大気圧下に124〜134℃に達するまで濃縮する工程
と、得られた濃縮糖液にステビア甘味料の水溶液を加え
る工程と、濃縮糖液を撹拌して水分の蒸発により冷却し
結晶を析出せしめる工程と、得られた結晶の粉粒物を解
砕し、解砕物を乾燥しついで分級して顆粒を得る工程と
よりなるステビア甘味料入り低カロリー砂糖の製造法。
1. A step of concentrating an aqueous solution of sucrose having a pure sugar rate of 85% or more until the boiling point reaches 124 to 134 ° C. under atmospheric pressure, and a step of adding an aqueous solution of stevia sweetener to the obtained concentrated sugar solution. , A step of stirring the concentrated sugar solution and cooling by evaporation of water to precipitate crystals, and a step of crushing the obtained crystal powder and granules, drying the crushed material, and then classifying to obtain granules A method for producing low-calorie sugar containing stevia sweetener.
JP61062049A 1986-03-20 1986-03-20 Manufacturing method of low-calorie sugar containing stevia sweetener Expired - Fee Related JPH0653048B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP61062049A JPH0653048B2 (en) 1986-03-20 1986-03-20 Manufacturing method of low-calorie sugar containing stevia sweetener

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP61062049A JPH0653048B2 (en) 1986-03-20 1986-03-20 Manufacturing method of low-calorie sugar containing stevia sweetener

Publications (2)

Publication Number Publication Date
JPS62220167A JPS62220167A (en) 1987-09-28
JPH0653048B2 true JPH0653048B2 (en) 1994-07-20

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US9001486B2 (en) 2005-03-01 2015-04-07 X2Y Attenuators, Llc Internally overlapped conditioners
US9019679B2 (en) 1997-04-08 2015-04-28 X2Y Attenuators, Llc Arrangement for energy conditioning
US9036319B2 (en) 1997-04-08 2015-05-19 X2Y Attenuators, Llc Arrangement for energy conditioning
US9054094B2 (en) 1997-04-08 2015-06-09 X2Y Attenuators, Llc Energy conditioning circuit arrangement for integrated circuit
KR101599975B1 (en) * 2015-03-30 2016-03-15 주식회사 샘넷식품 농업회사법인 Method for preparing of low-calorie sweetener composition

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US8404297B2 (en) 2006-06-13 2013-03-26 Ingenio del Cauca S.A.—Incauca S.A. Process for co-crystallizing sucrose and a natural sweetener and the product thereof
MX354449B (en) * 2010-03-16 2018-03-05 Imp Sugar Company Process for the manufacture of cocrystallized sucrose - polyol natural sweeteners and products thereof.
AU2014271347B2 (en) * 2010-03-16 2016-07-28 United States Sugar Savannah Refinery, Llc Process for the manufacture of cocrystallized sucrose - polyol natural sweeteners and products thereof
JP6099870B2 (en) * 2012-01-06 2017-03-22 松谷化学工業株式会社 Novel sweetener containing sucrose and D-psicose

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS56131400A (en) * 1980-03-17 1981-10-14 Nissin Sugar Mfg Production of stevioside containing sugar
JPS5716782A (en) * 1980-07-04 1982-01-28 Tsurumi Goseirozai Co Ltd Exothermic irregular-shaped refractory and lining construction using thereof
JPS5820170A (en) * 1981-07-24 1983-02-05 Toshizo Fukushima Preparation of sweetener
JPS5840066A (en) * 1981-09-04 1983-03-08 Fuji Food:Kk Low-caloric composite natural sweetening agent

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9019679B2 (en) 1997-04-08 2015-04-28 X2Y Attenuators, Llc Arrangement for energy conditioning
US9036319B2 (en) 1997-04-08 2015-05-19 X2Y Attenuators, Llc Arrangement for energy conditioning
US9054094B2 (en) 1997-04-08 2015-06-09 X2Y Attenuators, Llc Energy conditioning circuit arrangement for integrated circuit
US9001486B2 (en) 2005-03-01 2015-04-07 X2Y Attenuators, Llc Internally overlapped conditioners
KR101599975B1 (en) * 2015-03-30 2016-03-15 주식회사 샘넷식품 농업회사법인 Method for preparing of low-calorie sweetener composition

Also Published As

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