JPH0629114A - Dust core and manufacture thereof - Google Patents

Dust core and manufacture thereof

Info

Publication number
JPH0629114A
JPH0629114A JP18144292A JP18144292A JPH0629114A JP H0629114 A JPH0629114 A JP H0629114A JP 18144292 A JP18144292 A JP 18144292A JP 18144292 A JP18144292 A JP 18144292A JP H0629114 A JPH0629114 A JP H0629114A
Authority
JP
Japan
Prior art keywords
magnetic
resin
powder
heat treatment
dust core
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP18144292A
Other languages
Japanese (ja)
Inventor
Takeshi Yagisawa
猛 八木澤
Masanobu Nakano
正允 中野
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toshiba Corp
Original Assignee
Toshiba Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Toshiba Corp filed Critical Toshiba Corp
Priority to JP18144292A priority Critical patent/JPH0629114A/en
Publication of JPH0629114A publication Critical patent/JPH0629114A/en
Pending legal-status Critical Current

Links

Landscapes

  • Soft Magnetic Materials (AREA)

Abstract

PURPOSE:To eliminate strains to a satisfactory extent by raising heat treatment temperature and provide dust cores excellent in magnetic properties. CONSTITUTION:Since dust cores are formed by compression-molding magnetic powder together with resin mainly composed of borosiloxane resin, high temperature heat treatment is available. Furthermore, there is no strain produced by differential thermal expansion during cooling time, which makes it possible to eliminate residual stress to a satis factory extent so that the plastic deformation of the magnetic powder may be allowable. It is, therefore, possible to mold with a large compression force, thereby enhancing the space factor and hence attain enhanced magnetic properties in addition to stress removal effect.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は、回転電機,変圧器,リ
アクトル等の電気機器の鉄心に用いる圧粉磁心に関す
る。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a dust core used for an iron core of electric equipment such as rotating electric machines, transformers and reactors.

【0002】[0002]

【従来の技術】通常、電気機器の鉄心には、電磁鋼板を
打抜き積み重ねて構成した積層鉄心が用いられている。
このような積層鉄心は、磁束が電磁鋼板の面内方向に流
れるときには極めて優れた磁気特性を有するが、垂直方
向の磁束成分に対してはうず電流の発生が大きく、透磁
率は低い。そのため磁束の流れを平面内に限定できない
三次元的な鉄心においては積層鉄心を使用するよりも磁
性金属粉末を樹脂で固めた圧粉磁心が使用されている。
2. Description of the Related Art Normally, a laminated iron core formed by punching and stacking electromagnetic steel sheets is used for the iron core of electric equipment.
Such a laminated iron core has extremely excellent magnetic characteristics when the magnetic flux flows in the in-plane direction of the electromagnetic steel sheet, but has a large eddy current generation with respect to the vertical magnetic flux component and has a low magnetic permeability. Therefore, in a three-dimensional iron core in which the flow of magnetic flux cannot be limited to a plane, a dust core obtained by hardening magnetic metal powder with a resin is used rather than using a laminated iron core.

【0003】[0003]

【発明が解決しようとする課題】ところで、圧粉磁心の
磁気特性を左右する主な要因は、全体積に占める磁性粉
の割合と、磁性粉の特性である。圧粉磁心は磁性粉と樹
脂とが混合されたものであり、樹脂は磁性粉の間隔を広
げて磁束の流れを妨げる。そのため、磁気特性の優れた
圧粉磁心を作るためには、樹脂の量を減らし、かつ製作
時の加圧力を大きくして空隙をも減らし、磁性粉の占積
率をできるだけ大きくすることが必要である。ところ
が、加圧力を大きくしていくと、磁性粉が塑性変形を起
こしてしまい、残留応力が生ずる。この残留応力は磁気
特性を低下させるので、除去することが必要である。
By the way, the main factors that influence the magnetic characteristics of a dust core are the proportion of magnetic powder in the total volume and the characteristics of magnetic powder. The dust core is a mixture of magnetic powder and resin, and the resin spreads the gap between the magnetic powders to obstruct the flow of magnetic flux. Therefore, in order to create a dust core with excellent magnetic properties, it is necessary to reduce the amount of resin, increase the pressure applied during manufacturing to reduce voids, and maximize the space factor of magnetic powder. Is. However, when the applied pressure is increased, the magnetic powder undergoes plastic deformation, resulting in residual stress. Since this residual stress deteriorates the magnetic properties, it needs to be removed.

【0004】しかしながら、磁性粉中の残留応力を除去
するために熱処理を施すことは、樹脂の劣化を招くため
に、必要な温度にまで高くすることができず、そのため
従来の圧粉磁心の特性は、電磁鋼板などの積層鉄心に比
較して低く、したがって広い範囲には使用されず、用途
が限定されてしまうという問題があった。
However, the heat treatment for removing the residual stress in the magnetic powder causes deterioration of the resin, so that the temperature cannot be raised to the required temperature, and therefore the characteristics of the conventional dust core are not obtained. Is lower than that of a laminated iron core such as an electromagnetic steel plate, and thus is not used in a wide range, and there is a problem that the application is limited.

【0005】本発明は上記問題を解消するためになされ
たもので、その目的は熱処理温度を高くして十分なひず
み取りを行い、磁気特性の優れた圧粉磁心を提供するこ
とにある。
The present invention has been made to solve the above problems, and an object of the present invention is to provide a dust core having excellent magnetic characteristics by increasing the heat treatment temperature to sufficiently remove strain.

【0006】[0006]

【課題を解決するための手段】上記目的を達成するため
に、本発明の請求項1は磁性金属粉をボロシロキサン樹
脂を主成分とする樹脂とともに圧縮成形した圧粉磁心で
あり、また、請求項2はその表面に絶縁性のコーティン
グを施した磁性金属粉をボロシロキサン樹脂を主成分と
する樹脂とともに圧縮成形した圧粉磁心であり、さら
に、請求項3は絶縁性のコーティングの有るまたは無い
磁性金属粉を、ボロシロキサン樹脂を主成分とする樹脂
とともに圧縮成形した後、550℃以上の温度で歪み取
り熱処理を行うこと圧粉磁心の製造方法を特徴とするも
のである。
In order to achieve the above object, claim 1 of the present invention is a powder magnetic core obtained by compression molding magnetic metal powder together with a resin containing a borosiloxane resin as a main component. Item 2 is a powder magnetic core in which magnetic metal powder having an insulating coating on its surface is compression-molded together with a resin containing a borosiloxane resin as a main component, and Claim 3 is further provided with or without an insulating coating. The method is characterized in that the magnetic metal powder is compression-molded together with a resin containing a borosiloxane resin as a main component, and then strain relief heat treatment is performed at a temperature of 550 ° C. or higher.

【0007】[0007]

【作用】圧粉磁心の磁気特性を熱処理によって向上させ
るためには、耐熱性の優れた樹脂を用いるだけでは不十
分である。なぜなら、冷却時の熱膨脹係数の違いによっ
て磁性粉に応力が生じ、それが磁気特性を低下させてし
まうからである。すなわち、耐熱性が優れ、かつ冷却時
に磁性粉に応力を生じさせない樹脂を選ぶことが必要で
ある。
In order to improve the magnetic characteristics of the dust core by heat treatment, it is not enough to use a resin having excellent heat resistance. This is because the difference in the coefficient of thermal expansion during cooling causes stress in the magnetic powder, which reduces the magnetic properties. That is, it is necessary to select a resin that has excellent heat resistance and does not cause stress in the magnetic powder during cooling.

【0008】本発明は耐熱性樹脂としてボロシロキサン
樹脂を選ぶことにより、磁気特性の優れた圧粉磁心を得
ることができる。すなわち、ボロシロキサン樹脂を用い
た圧粉磁心は、高い温度で熱処理を行うことができ、さ
らに冷却時に熱膨脹差によるひずみを生じないことか
ら、十分な残留応力除去が可能である。さらに応力除去
が可能であれば、磁性粉の塑性変形が許容されるので、
従来より大きな圧縮力を加えて成形することも可能とな
り、その結果占積率も向上し、応力除去効果に加えて磁
気特性の向上にも有効である。
According to the present invention, by selecting a borosiloxane resin as the heat resistant resin, it is possible to obtain a dust core having excellent magnetic characteristics. That is, the dust core using the borosiloxane resin can be heat-treated at a high temperature, and does not cause strain due to the difference in thermal expansion during cooling, so that sufficient residual stress can be removed. If the stress can be further removed, plastic deformation of the magnetic powder is allowed.
It is also possible to apply a larger compressive force than before, and as a result, the space factor is improved, which is effective for improving the magnetic properties in addition to the stress relief effect.

【0009】[0009]

【実施例】以下、本発明を実施例について説明する。EXAMPLES The present invention will be described below with reference to examples.

【0010】粒径150メッシュパスの純鉄粉を98.
0質量%、ボロシロキサン樹脂を1.5質量%、無機質
充填材を0.5質量%を溶剤を加えて混練し、金型に充
填して900MPaの圧力で圧縮成形を行い、300℃
1時間の加熱により硬化させた。さらにこの圧粉磁心を
500℃〜650℃の間で温度を変え、N2 中でひずみ
取り焼鈍を行った。
Pure iron powder having a particle size of 150 mesh pass is 98.
0% by mass, 1.5% by mass of borosiloxane resin, and 0.5% by mass of inorganic filler were kneaded by adding a solvent, filled in a mold, and compression-molded at a pressure of 900 MPa at 300 ° C.
It was cured by heating for 1 hour. Further, this powder magnetic core was subjected to strain relief annealing in N 2 while changing the temperature between 500 ° C and 650 ° C.

【0011】本実施例においては、成形時の圧縮力を約
50%高くしたことで占積率が向上するとともに、高温
度による熱処理で残留応力を除去することにより、磁気
特性の優れた圧粉磁心が可能となる。
In the present embodiment, the space factor is improved by increasing the compression force at the time of molding by about 50%, and the residual stress is removed by the heat treatment at a high temperature, so that the powder compact having excellent magnetic properties is obtained. Magnetic core becomes possible.

【0012】表1に最大磁化力Hm=800A/mにお
いて測定した本実施例の圧粉磁心の磁気特性を示す。ま
た比較例として従来のエポキシ樹脂を用いた圧粉磁心の
特性を併せて示している。
Table 1 shows the magnetic characteristics of the powder magnetic core of this example measured at the maximum magnetizing force Hm = 800 A / m. Further, as a comparative example, the characteristics of the dust core using the conventional epoxy resin are also shown.

【0013】[0013]

【表1】 [Table 1]

【0014】熱処理温度が低い場合には、磁気特性は従
来材よりかえって特性が低いが、550℃以上では磁束
密度は高くまた保磁力は低くなって、優れた磁気特性を
示している。
When the heat treatment temperature is low, the magnetic properties are lower than those of the conventional materials, but at 550 ° C. or higher, the magnetic flux density is high and the coercive force is low, showing excellent magnetic properties.

【0015】また、圧粉磁心を高周波用に使用する場合
は、磁性粉の粒子間の電気的絶縁をより完全にしておく
必要がある。そのためには磁性粉の粒子の表面をあらか
じめリン酸塩被膜でコーティングしておき、この表面処
理後の磁性粉をボロシロキサン樹脂とともに圧縮成形す
ることにより、高周波特性の優れた圧粉磁心を得ること
ができる。なお、リン酸塩の代りに、クロム酸塩あるい
は他の耐熱性絶縁コーティングでもよいことはもちろん
である。
When the powder magnetic core is used for high frequencies, it is necessary to make the electrical insulation between the particles of the magnetic powder more complete. For that purpose, the surface of the particles of the magnetic powder is coated with a phosphate coating in advance, and the magnetic powder after the surface treatment is compression-molded with a borosiloxane resin to obtain a dust core having excellent high frequency characteristics. You can Of course, instead of phosphate, chromate or another heat resistant insulating coating may be used.

【0016】[0016]

【発明の効果】以上説明したように、本発明によれば、
耐熱性で、占積率も高く、かつ磁気特性の優れた圧粉磁
心及び低鉄損の高周波用圧粉鉄心を提供することが可能
となる。
As described above, according to the present invention,
It is possible to provide a dust core having heat resistance, a high space factor, and excellent magnetic characteristics, and a high-frequency dust core having a low iron loss.

Claims (3)

【特許請求の範囲】[Claims] 【請求項1】 磁性金属粉をボロシロキサン樹脂を主成
分とする樹脂とともに圧縮成形したことを特徴とする圧
粉磁心。
1. A powder magnetic core, characterized in that magnetic metal powder is compression molded together with a resin containing a borosiloxane resin as a main component.
【請求項2】 その表面にあらかじめ絶縁性のコーティ
ングを施した磁性金属粉を設けたことを特徴とする請求
項1記載の圧粉磁心。
2. The dust core according to claim 1, wherein magnetic metal powder having an insulative coating applied on its surface is provided.
【請求項3】 絶縁性のコーティングの有るまたは無い
磁性金属粉を、ボロシロキサン樹脂を主成分とする樹脂
とともに圧縮成形した後、550℃以上の温度で歪み取
り熱処理を行うことを特徴とする圧粉磁心の製造方法。
3. A pressure characterized by performing heat treatment for strain relief at a temperature of 550 ° C. or higher after compression-molding a magnetic metal powder with or without an insulating coating together with a resin containing a borosiloxane resin as a main component. A method for manufacturing a powder magnetic core.
JP18144292A 1992-07-09 1992-07-09 Dust core and manufacture thereof Pending JPH0629114A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP18144292A JPH0629114A (en) 1992-07-09 1992-07-09 Dust core and manufacture thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP18144292A JPH0629114A (en) 1992-07-09 1992-07-09 Dust core and manufacture thereof

Publications (1)

Publication Number Publication Date
JPH0629114A true JPH0629114A (en) 1994-02-04

Family

ID=16100846

Family Applications (1)

Application Number Title Priority Date Filing Date
JP18144292A Pending JPH0629114A (en) 1992-07-09 1992-07-09 Dust core and manufacture thereof

Country Status (1)

Country Link
JP (1) JPH0629114A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010038441A1 (en) 2008-10-01 2010-04-08 パナソニック株式会社 Composite magnetic material and process for producing the composite magnetic material
WO2013140762A1 (en) 2012-03-22 2013-09-26 パナソニック株式会社 Composite magnetic material and method for manufacturing same
JP2014082382A (en) * 2012-10-17 2014-05-08 Tdk Corp Magnetic powder, inductor element, and method for manufacturing inductor element
US8808566B2 (en) 2009-03-25 2014-08-19 Panasonic Corporation Composite magnetic material

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010038441A1 (en) 2008-10-01 2010-04-08 パナソニック株式会社 Composite magnetic material and process for producing the composite magnetic material
US8808566B2 (en) 2009-03-25 2014-08-19 Panasonic Corporation Composite magnetic material
WO2013140762A1 (en) 2012-03-22 2013-09-26 パナソニック株式会社 Composite magnetic material and method for manufacturing same
US9691529B2 (en) 2012-03-22 2017-06-27 Panasonic Intellectual Property Management Co., Ltd. Composite magnetic material and method for manufacturing same
JP2014082382A (en) * 2012-10-17 2014-05-08 Tdk Corp Magnetic powder, inductor element, and method for manufacturing inductor element

Similar Documents

Publication Publication Date Title
US7544417B2 (en) Soft magnetic material and dust core comprising insulating coating and heat-resistant composite coating
US4543208A (en) Magnetic core and method of producing the same
JP6277426B2 (en) Composite magnetic body and method for producing the same
JP5218567B2 (en) Manufacturing method of dust core
EP2518740A1 (en) Reactor and method for producing same
JP3964213B2 (en) Manufacturing method of dust core and high frequency reactor
JP5522173B2 (en) Composite magnetic body and method for producing the same
US1669644A (en) Magnetic material
JP2010027871A (en) Dust core and manufacturing method thereof
US20090220372A1 (en) Low Magnetostrictive Body and Dust Core Using the Same
JPH0629114A (en) Dust core and manufacture thereof
JP4909312B2 (en) Soft magnetic material for dust core and dust core
JP4315436B2 (en) Dust core manufacturing method and dust core
KR101882444B1 (en) SOFT MAGNETIC CORE FOR alternating current MOTOR, METHOD FOR MAKING THE SAME AND alternating current MOTOR WITH IT
JP4650450B2 (en) Dust core, method for manufacturing dust core, and motor using the same
JP2018142642A (en) Powder magnetic core
JPH11238614A (en) Soft magnetic material and manufacture thereof and electrical equipment using the same
KR20140076282A (en) Soft magnetic core and manufacturing method of the same
JP2008141012A (en) Reactor
JP6581270B2 (en) Manufacturing method of magnetic core
JPH10189323A (en) Dust core and its manufacture
KR102468304B1 (en) Magnetic dust core and manufacturing method thereof
KR102244550B1 (en) Manufacturing method of amorphous soft magnetic core and amorphous soft magnetic core
JP7405659B2 (en) A powder compact, a method for producing a powder compact, and a method for producing a powder magnetic core;
JP7138736B2 (en) CORE, REACTOR, CORE MANUFACTURING METHOD AND REACTOR MANUFACTURING METHOD