JPH06264218A - Sputtering target - Google Patents

Sputtering target

Info

Publication number
JPH06264218A
JPH06264218A JP5234893A JP5234893A JPH06264218A JP H06264218 A JPH06264218 A JP H06264218A JP 5234893 A JP5234893 A JP 5234893A JP 5234893 A JP5234893 A JP 5234893A JP H06264218 A JPH06264218 A JP H06264218A
Authority
JP
Japan
Prior art keywords
sputtering
sputtering target
target
film
magnetic field
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP5234893A
Other languages
Japanese (ja)
Inventor
Hideyuki Ishiguro
秀之 石黒
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toyo Ink Mfg Co Ltd
Original Assignee
Toyo Ink Mfg Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Toyo Ink Mfg Co Ltd filed Critical Toyo Ink Mfg Co Ltd
Priority to JP5234893A priority Critical patent/JPH06264218A/en
Publication of JPH06264218A publication Critical patent/JPH06264218A/en
Pending legal-status Critical Current

Links

Abstract

PURPOSE:To provide a sputtering target capable of sputtering by supply of high electric power even under conditions simultaneously satisfying low pressure of sputtering gas and low voltage and capable of forming a high quality coating film, a magnetic recording medium, etc., at a high speed. CONSTITUTION:A ferromagnetic body having a circularly grooved structure 4 in the surface is laminated on a backing plate 2 and a magnet 3 is disposed behind the baking plate 2 to obtain the objective sputtering target 1 disposed opposite to a substrate on which a film is formed. A magnetic field from the magnet 3 is leaked, plasma density is increased and high-speed sputtering of the ferromagnetic body is enabled.

Description

【発明の詳細な説明】Detailed Description of the Invention

【産業上の利用分野】本発明は、製膜処理をなすべき基
板に対向して配置され、Fe,Coその他の強磁性体を
高速スパッタリングにより被膜形成を行う際に使用する
スパッタリングターゲットに関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a sputtering target which is arranged so as to face a substrate to be subjected to a film-forming process and which is used when a ferromagnetic material such as Fe, Co or the like is formed by high speed sputtering. is there.

【従来の技術】基板表面に金属被膜を形成する場合の形
成技術の一つとして、スパッタリングがある。近年各種
強磁性体をスパッタリングして磁性薄膜を形成させる要
求が高まっている。従来のスパッタリング装置は図1に
示すように、ターゲット材料1を支持するバッキングプ
レート2を磁界発生装置3の上に設けたものである。こ
の装置では、ターゲット材料1がFeなどの高透磁率を
有する強磁性体の場合、磁界発生装置3の磁束が強磁性
体のターゲット材料1にシールドされてしまいプラズマ
放電しない。このため、ターゲット材料1の厚さを3m
m程度に薄く形成する必要があったが、それでもターゲ
ット材料1の表面に出る漏れ磁束が小さいために、高い
電圧が必要であった。更に、ターゲットの初期と末期に
おいて放電電圧電流特性が大きく変化し、例えば電力を
一定にしても電圧が変動して再現性のある膜形成が困難
であった。又、高速作製を行うためにスパッタガス圧を
高くして、高い電力を投入して製膜するとスパッタガス
によりシャドウイング効果が大きく作用して結晶性の劣
化が生じるという問題点があった。又、従来のプレイナ
ーマグネトロン式スパッタリングターゲットを用いたス
パッタリング製膜では、例えば軟磁性材料であるFe−
Si材を製膜した場合、製膜時に結晶性の優れた緻密な
膜を形成できる低スパッタガス圧では高電力を投入する
ことができず、又、高いスパッタガス圧においては高電
力を投入すると抗磁力が高くなってしまい軟磁性体の特
徴が失われてしまった。これらの問題を解決するために
開発されたギャップタイプターゲットはギヤップを形成
するコストが高く不経済であった。
2. Description of the Related Art Sputtering is one of the techniques for forming a metal coating on the surface of a substrate. In recent years, there is an increasing demand for forming magnetic thin films by sputtering various ferromagnetic materials. As shown in FIG. 1, the conventional sputtering apparatus has a backing plate 2 supporting a target material 1 provided on a magnetic field generator 3. In this apparatus, when the target material 1 is a ferromagnetic material having a high magnetic permeability such as Fe, the magnetic flux of the magnetic field generator 3 is shielded by the ferromagnetic target material 1 and plasma discharge does not occur. Therefore, the thickness of the target material 1 is 3 m
Although it was necessary to form it as thin as about m, a high voltage was still required because the leakage magnetic flux appearing on the surface of the target material 1 was small. Furthermore, the discharge voltage-current characteristics greatly change in the initial and final stages of the target, and for example, the voltage fluctuates even when the power is constant, and it is difficult to form a reproducible film. In addition, there is a problem that when the sputtering gas pressure is increased and high power is applied to form a film for high-speed production, the shadowing effect is largely exerted by the sputtering gas and the crystallinity is deteriorated. Further, in the sputtering film formation using the conventional planar magnetron type sputtering target, for example, Fe- which is a soft magnetic material is used.
When the Si material is formed into a film, high power cannot be applied at a low sputter gas pressure capable of forming a dense film having excellent crystallinity during film formation, and when high power is applied at a high sputter gas pressure. The coercive force increased and the characteristics of the soft magnetic material were lost. The gap type target developed to solve these problems was expensive and uneconomical to form a gap.

【発明が解決しようとする課題】本発明は、上記の問題
点を解決するためになされたものであり、低いスパッタ
ガス圧及び低い電圧を同時に満たす条件においても大電
力投入のスパッタリングが可能であり、高品質の被膜や
磁気記録媒体などを高速で作製でき、従来のプレイナー
スパッタリング装置を単に改良するだけで使用すること
ができるスパッタリングターゲットを提供するものであ
る。
The present invention has been made in order to solve the above problems, and it is possible to perform sputtering with a large power input even under the condition that a low sputtering gas pressure and a low voltage are simultaneously satisfied. The present invention provides a sputtering target capable of producing a high-quality coating film or a magnetic recording medium at a high speed and used by simply improving a conventional planar sputtering apparatus.

【課題を解決するための手段】すなわち、本発明は、バ
ッキングプレート上に表面に環状の溝構造を有する強磁
性体材料を積層してなるスパッタリングターゲットに関
する。本発明を図3に基づき説明すると、強磁性体材料
1は板形状であって表面に環状の溝構造4が形成されて
いる。この構造により磁界発生装置3の磁界が強磁性体
のスパッタリングターゲット表面に漏れるようにする。
環状の溝構造4は、円形でもよく角形あるいはその他の
形状であってもよい。窪みの深さは強磁性材料の厚さの
30〜90%であることが好ましい。強磁性材料は比透
磁率が100〜1000万のものが使用でき、例えば、
Ni、Co、Fe及びこれらを主成分とする化合物が使
用できる。バッキングプレート2は強磁性体材料1を支
持するためのものである。バッキングプレート2は、C
u等からなり強磁性体材料1とボンディングされてい
る。永久磁石3はバッキングプレート2の背面に設けら
れ、磁界を強磁性体材料1の窪み構造に透過させる。本
発明のスパッタリングターゲットは、対向して配置され
た基材(図示せず)の表面にスパッタリングされた強磁
性体が薄膜形成させるために使用される。スパッタリン
グの条件は、スパッタリングガス圧0.1〜100mT
orr、電圧200〜1KVが好ましい。
That is, the present invention relates to a sputtering target formed by laminating a ferromagnetic material having an annular groove structure on its surface on a backing plate. The present invention will be described with reference to FIG. 3. The ferromagnetic material 1 is plate-shaped and has an annular groove structure 4 formed on the surface. With this structure, the magnetic field of the magnetic field generator 3 leaks to the surface of the ferromagnetic sputtering target.
The annular groove structure 4 may have a circular shape, a rectangular shape, or another shape. The depth of the depression is preferably 30 to 90% of the thickness of the ferromagnetic material. As the ferromagnetic material, one having a relative magnetic permeability of 1 to 10,000,000 can be used.
Ni, Co, Fe and compounds containing these as the main components can be used. The backing plate 2 is for supporting the ferromagnetic material 1. The backing plate 2 is C
It is made of u or the like and is bonded to the ferromagnetic material 1. The permanent magnet 3 is provided on the back surface of the backing plate 2 and transmits a magnetic field to the hollow structure of the ferromagnetic material 1. The sputtering target of the present invention is used for forming a thin film of a ferromagnetic material sputtered on the surface of a base material (not shown) arranged to face each other. The sputtering conditions are sputtering gas pressure of 0.1 to 100 mT.
Orr and voltage of 200 to 1 KV are preferable.

【実施例】図2に示す構造の強磁性体としてバッキング
プレートとボンデングされたFeスパッタリングターゲ
ット材(大きさ100mm×200mm、最大厚さ5m
m、窪みの底部分の厚さ2mm)を用いてターゲット上
に漏洩した磁界を測定したところ8000Oeを示した
(図4参照)。次に、このスパッタリングターゲットを
用いてスパッタガス圧2mTorrでの放電電圧電流特
性を測定し図5に示した。300〜400V付近でマグ
ネトロン放電が起きており高い電流を投入できることが
確認された。一方、従来のプレーナー式マグネトロンス
パッタリングのFe製スパッタリングターゲット(大き
さ100mm×200mm)の表面の漏れ磁界を測定し
たところ20Oeであった(図6参照)。又、このスパ
ッタリングターゲットの放電電圧電流特性図を図5に示
した。このスパッタリングターゲットは、使用初期では
低いスパッタリングガス圧(2mTorr)では750
Vとかなり高い印加電圧を加えても200W程度しか電
力を投入することができないので高堆積速度の製膜がで
きないことが判明した。
EXAMPLE A backing plate and a Fe sputtering target material bonded as a ferromagnetic material having a structure shown in FIG. 2 (size 100 mm × 200 mm, maximum thickness 5 m).
When the magnetic field leaked onto the target was measured using m, the thickness of the bottom of the depression was 2 mm), it was 8000 Oe (see FIG. 4). Next, using this sputtering target, discharge voltage-current characteristics at a sputtering gas pressure of 2 mTorr were measured and shown in FIG. It was confirmed that magnetron discharge occurred near 300 to 400 V and a high current could be applied. On the other hand, the leakage magnetic field on the surface of a conventional sputtering target made of Fe (size 100 mm × 200 mm) for planar magnetron sputtering was measured and found to be 20 Oe (see FIG. 6). The discharge voltage-current characteristic diagram of this sputtering target is shown in FIG. This sputtering target has a low sputtering gas pressure (2 mTorr) of 750 at the beginning of use.
It has been found that a film having a high deposition rate cannot be formed because the electric power can be applied only to about 200 W even when an applied voltage as high as V is applied.

【発明の効果】本発明によって、次の効果が確認され
た。 (1)ターゲット表面にかなり強い磁場を形成すること
が可能となり、その結果、放電インピーダンスを小さく
する事ができ、スパッタリングターゲットの発熱が少な
く電力(スパッタリングに寄与する)効率が向上した。 (2)磁気回路の工夫により放電プラズマはスパッタリ
ングターゲットの空隙でのみ強く発生するために、基板
への電子衝撃が極めて少なく基板がスパッタリング中に
加熱することがない。 (3)高速の膜堆積を目的として高電力を投入してもそ
の電圧は低いのでスパッタリングターゲットも高温にな
ず、高電力の低温スパッタが促進され、かつ電力の損失
が少ない。 (4)低スパッタガス圧でも高電力が投入できるように
なったので高速で堆積させても緻密で結晶性のよい膜が
できる。
The following effects have been confirmed by the present invention. (1) It becomes possible to form a fairly strong magnetic field on the target surface, and as a result, the discharge impedance can be reduced, and the sputtering target generates less heat and improves the power (contribution to sputtering) efficiency. (2) Since the discharge plasma is strongly generated only in the voids of the sputtering target due to the devise of the magnetic circuit, the electron impact on the substrate is extremely small and the substrate is not heated during sputtering. (3) Even if high power is applied for the purpose of high-speed film deposition, the voltage is low, so that the sputtering target does not reach high temperature, high-temperature low-temperature sputtering is promoted, and power loss is small. (4) Since high power can be applied even with a low sputtering gas pressure, a dense and crystallized film can be formed even when deposited at a high speed.

【図面の簡単な説明】[Brief description of drawings]

【図1】従来のスパッタリングターゲットの断面図FIG. 1 is a sectional view of a conventional sputtering target.

【図2】本発明のスパッタリングターゲットの斜視図FIG. 2 is a perspective view of a sputtering target of the present invention.

【図3】図1のA−A´断面図3 is a sectional view taken along the line AA ′ in FIG.

【図4】漏れ磁界強さを示すグラフFIG. 4 is a graph showing leakage magnetic field strength.

【図5】放電特性図FIG. 5: Discharge characteristic diagram

【図6】漏れ磁界強さを示すグラフFIG. 6 is a graph showing leakage magnetic field strength.

【符号の説明】[Explanation of symbols]

1 ターゲット材 2 バッキングプレート 3 永久磁石 4 溝構造 1 target material 2 backing plate 3 permanent magnet 4 groove structure

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】 バッキングプレート上に表面に環状の溝
構造を有する強磁性体材料を積層してなるスパッタリン
グターゲット。
1. A sputtering target obtained by laminating a ferromagnetic material having an annular groove structure on the surface of a backing plate.
JP5234893A 1993-03-12 1993-03-12 Sputtering target Pending JPH06264218A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP5234893A JPH06264218A (en) 1993-03-12 1993-03-12 Sputtering target

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP5234893A JPH06264218A (en) 1993-03-12 1993-03-12 Sputtering target

Publications (1)

Publication Number Publication Date
JPH06264218A true JPH06264218A (en) 1994-09-20

Family

ID=12912312

Family Applications (1)

Application Number Title Priority Date Filing Date
JP5234893A Pending JPH06264218A (en) 1993-03-12 1993-03-12 Sputtering target

Country Status (1)

Country Link
JP (1) JPH06264218A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007239099A (en) * 2006-02-10 2007-09-20 Ricoh Co Ltd Sputtering target and manufacturing method therefor, and optical recording medium and manufacturing method therefor
CN107151784A (en) * 2017-05-26 2017-09-12 中国电子科技集团公司第四十八研究所 A kind of negative electrode magnetron sputtering target assembly

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007239099A (en) * 2006-02-10 2007-09-20 Ricoh Co Ltd Sputtering target and manufacturing method therefor, and optical recording medium and manufacturing method therefor
CN107151784A (en) * 2017-05-26 2017-09-12 中国电子科技集团公司第四十八研究所 A kind of negative electrode magnetron sputtering target assembly
CN107151784B (en) * 2017-05-26 2019-08-16 中国电子科技集团公司第四十八研究所 A kind of cathode magnetron sputtering target assembly

Similar Documents

Publication Publication Date Title
US5147734A (en) Magnetic recording media manufactured by a process in which a negative bias voltage is applied to the substrate during sputtering
US4399013A (en) Method of producing a magnetic recording medium
JPS6134723A (en) Magnetic recording medium and its manufacture
JPH06264218A (en) Sputtering target
JPS5836413B2 (en) Magnetic recording medium manufacturing method and its manufacturing device
JPH06136533A (en) Sputtering target
US4410406A (en) Process for preparing magnetic recording medium
JPH031810B2 (en)
JPH059849B2 (en)
JP2980266B2 (en) Sputtering apparatus for forming a laminated film of a magnetic thin film and a non-magnetic thin film
JPS5813622B2 (en) Magnetron type sputtering equipment
JPS59129944A (en) Method and device for manufacturing magnetic recording medium
JPS62285253A (en) Manufacture of photomagnetic recording medium
JPS63140509A (en) Manufacture of magnetically soft film
JPS6249974B2 (en)
JPS61227231A (en) Production of magnetic recording body
JPH04356728A (en) Production of magnetic recording medium
JPH05128515A (en) Manufacture of sputtered thin film
JPH05335169A (en) Forming method of magnetic thin film
JPS63244728A (en) Target for sputtering
JPS6188511A (en) Manufacture of magnetic thin film
JPS6334226B2 (en)
JPS581832A (en) Vertical magnetized recording medium
JPS60111348A (en) Production of magnetic recording medium
JPH0680530B2 (en) Method of manufacturing magnetic recording medium