JPH0616447A - Production of optical fiber base material - Google Patents
Production of optical fiber base materialInfo
- Publication number
- JPH0616447A JPH0616447A JP4191294A JP19129492A JPH0616447A JP H0616447 A JPH0616447 A JP H0616447A JP 4191294 A JP4191294 A JP 4191294A JP 19129492 A JP19129492 A JP 19129492A JP H0616447 A JPH0616447 A JP H0616447A
- Authority
- JP
- Japan
- Prior art keywords
- glass
- burner
- optical fiber
- production
- base material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/012—Manufacture of preforms for drawing fibres or filaments
- C03B37/014—Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacture, Treatment Of Glass Fibers (AREA)
- Glass Melting And Manufacturing (AREA)
Abstract
Description
【0001】[0001]
【産業上の利用分野】この発明は、光通信用ガラスファ
イバ母材の製造方法に関するもので、製造時の母材の破
損防止を図ったものである。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method of manufacturing a glass fiber preform for optical communication, and is intended to prevent damage to the preform during production.
【0002】[0002]
【従来の技術】光ファイバ母材の製造方法として、予め
用意されたコアとなる部分を有する石英系ガラスロッド
の周りに外付け法によってクラッドとなるガラス微粒子
層を形成し、その後このガラス微粒子層を脱水、透明ガ
ラス化して所定の光ファイバ母材とする方法がある。上
記外付けに際しては、1本もしくは複数本の酸水素バー
ナを前記ガラスロッドの軸方向に沿ってトラバースさせ
て火炎加水分解法によって得られるガラス微粒子をロッ
ドの周りに堆積させ所定の厚さとする。2. Description of the Related Art As a method for producing an optical fiber preform, a glass fine particle layer to be a clad is formed around a silica glass rod having a core portion prepared in advance by an external method, and then this glass fine particle layer is formed. There is a method of dehydrating and forming transparent glass into a predetermined optical fiber preform. In the external attachment, one or more oxyhydrogen burners are traversed along the axial direction of the glass rod to deposit glass fine particles obtained by the flame hydrolysis method around the rod to a predetermined thickness.
【0003】[0003]
【発明が解決しようとする課題】しかしながら、この方
法による母材の製造中に時としてガラス微粒子層が破損
するということがあった。本発明者などが破損の原因を
検討したところ、バーナの1回のトラバース毎の堆積厚
さと深い関連性が見られ、その厚さが所定以上になると
破損の頻度が急激に増大することが判明した。その理由
は、バーナのトラバース1回で厚く製造するとガラス微
粒子のかさ密度が半径方向に均一でなくなり、比較的に
軟らかい部分と硬い部分とができ、その境界に生じる歪
みのために破損してしまうということであると推測され
る。However, the glass fine particle layer sometimes breaks during the production of the base material by this method. When the inventors of the present invention examined the cause of the damage, it was found that the burner had a deep relationship with the deposition thickness of each traverse, and it was found that the frequency of the damage sharply increases when the thickness exceeds a predetermined value. did. The reason for this is that if the burner is manufactured thickly with one traverse, the bulk density of the glass fine particles becomes uneven in the radial direction, and relatively soft and hard parts are formed, which are damaged by the strain generated at the boundary. It is supposed to be that.
【0004】[0004]
【課題を解決するための手段】この発明は、以上の観点
にたってなされたもので、その特徴とする請求項1記載
の発明は、少なくともコアとなる部分を含む石英系ガラ
スロッドを、その軸の周りに回転させつつ、その軸方向
に沿って少なくとも1本のバーナをトラバースさせて前
記ガラスロッドの周りにクラッドとなるガラス微粒子を
堆積させるに際して、前記バーナの1回のトラバースに
よるガラス微粒子の堆積厚さを所定の範囲に制御しつつ
製造することにある。また、その特徴とする請求項2記
載の発明は、バーナの1回のトラバースによるガラス微
粒子の堆積厚さが1.0〜2.0mm、好ましくは1.
5±0.2mmであることにある。The present invention has been made from the above viewpoint, and the invention according to claim 1 is characterized in that a silica-based glass rod including at least a core portion is provided with When at least one burner is traversed along the axial direction while rotating around the glass rod to deposit the glass fine particles to be the cladding around the glass rod, the glass fine particles are deposited by the traversing once by the burner. It is to manufacture while controlling the thickness within a predetermined range. Further, the invention according to claim 2 characterized in that the deposition thickness of the glass fine particles by one traverse of the burner is 1.0 to 2.0 mm, preferably 1.
5 ± 0.2 mm.
【0005】[0005]
【作用】酸水素バーナを用いた1回のトラバースによる
クラッド用石英ガラス微粒子層の厚さが2.0mm以下
とされているので、このガラス微粒子層の内側と外側と
の間にさほどかさ密度の差がなく歪みが生じないので製
造中に破損することがない。なお、バーナのトラバース
1回当りの石英ガラス微粒子層の堆積厚さを1.0mm
以上としたのはそれ以下では製造効率が著しく低いから
である。Since the thickness of the silica glass fine particle layer for clad by one traverse using the oxyhydrogen burner is set to 2.0 mm or less, a small bulk density is provided between the inside and the outside of the glass fine particle layer. Since there is no difference and no distortion occurs, there is no damage during manufacturing. In addition, the deposition thickness of the silica glass fine particle layer per traverse of the burner was 1.0 mm.
The reason for the above is that the manufacturing efficiency is remarkably low below that.
【0006】[0006]
【実施例1】図1は、この発明方法を示す概略説明図で
ある。図において、1はGeO2 −SiO2 や純粋石英
などの石英系ガラスからなるコア用ロッドで、その軸の
周りに回転される。2はコア用ロッド1上に堆積され
た、クラッドとなるSiO2 やフッ素ドープSiO2 か
らなるガラス微粒子層、3はこのガラス微粒子を生成さ
せる同心多重管バーナもしくはマルチバーナで、説明の
便宜上1本だけ示してあるが、通常はガラス微粒子の堆
積効率を高めるために複数本用意され、上記コア用ロッ
ド1の軸に沿ってトラバースされる。なお、バーナが同
心4重管バーナの場合、例えば、その中心部にクラッド
用原料ガスであるSiCl4 やSiF4 +SiCl4 が
供給され、2層目にArなどのシールガス、3層目に水
素、4層目に酸素ガスが順次供給される。4は堆積され
るガラス微粒子の厚さを測定するカメラで、各バーナの
通過前と通過後の厚さを測定して、それが1.0〜2.
0mmの範囲になるようにする。具体的には、この厚さ
の測定結果を原料ガスの供給量にフィードバックして上
記厚さの範囲に収まるようにする。なお、各バーナの1
回のトラバースによる堆積厚さを1.5±0.2mmを
許容範囲として製造したところ、ガラス微粒子層を全く
破損させることなく製造することができた。Embodiment 1 FIG. 1 is a schematic explanatory view showing the method of the present invention. In the figure, reference numeral 1 is a core rod made of silica glass such as GeO 2 —SiO 2 or pure quartz, which is rotated around its axis. Reference numeral 2 is a glass fine particle layer made of SiO 2 or fluorine-doped SiO 2 which becomes a clad deposited on the core rod 1, and 3 is a concentric multi-tube burner or a multi-burner for producing the glass fine particles. Although only shown, a plurality of glass rods are usually prepared to increase the deposition efficiency of the glass particles and traversed along the axis of the core rod 1. When the burner is a concentric quadruple burner, for example, SiCl 4 or SiF 4 + SiCl 4 as a cladding material gas is supplied to the center of the burner, a seal gas such as Ar is supplied to the second layer, and hydrogen is supplied to the third layer. Oxygen gas is sequentially supplied to the fourth layer. Reference numeral 4 is a camera for measuring the thickness of the deposited glass particles, which measures the thickness of each burner before and after passing, and it is 1.0 to 2.
It should be in the range of 0 mm. Specifically, the measurement result of the thickness is fed back to the supply amount of the raw material gas so that the thickness falls within the above range. One of each burner
When the deposition thickness by the single traverse was set within the allowable range of 1.5 ± 0.2 mm, the glass fine particle layer could be produced without any damage.
【0007】[0007]
【発明の効果】この発明による光ファイバ母材の製造方
法は、外付け法によってクラッド用ガラス微粒子を堆積
させる際に、バーナの1回のトラバースによる堆積厚さ
を1.0〜2.0mm、好ましくは1.5±0.2mm
としたので、製造中にガラス微粒子層を破損させること
なく製造できる。According to the method of manufacturing an optical fiber preform according to the present invention, when the glass particles for cladding are deposited by the external attachment method, the deposition thickness by one traverse of the burner is 1.0 to 2.0 mm, Preferably 1.5 ± 0.2 mm
Therefore, it can be manufactured without damaging the glass fine particle layer during manufacturing.
【図1】この発明方法による光ファイバ母材の説明図で
ある。FIG. 1 is an explanatory diagram of an optical fiber preform according to the method of the present invention.
1 コア用石英系ガラスロッド 2 クラッド用石英系ガラス微粒子層 3 酸水素バーナ 4 カメラ 1 Quartz glass rod for core 2 Quartz glass particle layer for clad 3 Hydrogen oxyburner 4 Camera
Claims (2)
ガラスロッドを、その軸の周りに回転させつつ、その軸
方向に沿って少なくとも1本のバーナをトラバースさせ
て前記ガラスロッドの周りにクラッドとなるガラス微粒
子を堆積させるに際して、前記バーナの1回のトラバー
スによるガラス微粒子の堆積厚さを所定の範囲に制御し
つつ製造することを特徴とする光ファイバ母材の製造方
法。1. A quartz glass rod including at least a core portion is rotated around its axis, and at least one burner is traversed along its axial direction to form a cladding around the glass rod. The method for producing an optical fiber preform, characterized in that, when depositing the glass particles, the glass fiber is produced while controlling the deposition thickness of the glass particles by one traverse of the burner within a predetermined range.
微粒子の堆積厚さが1.0〜2.0mm、好ましくは
1.5±0.2mmであることを特徴とする請求項1記
載の光ファイバ母材の製造方法。2. The optical fiber according to claim 1, wherein the deposition thickness of the glass particles by one traverse of the burner is 1.0 to 2.0 mm, preferably 1.5 ± 0.2 mm. Base material manufacturing method.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP4191294A JPH0616447A (en) | 1992-06-26 | 1992-06-26 | Production of optical fiber base material |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP4191294A JPH0616447A (en) | 1992-06-26 | 1992-06-26 | Production of optical fiber base material |
Publications (1)
Publication Number | Publication Date |
---|---|
JPH0616447A true JPH0616447A (en) | 1994-01-25 |
Family
ID=16272176
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP4191294A Pending JPH0616447A (en) | 1992-06-26 | 1992-06-26 | Production of optical fiber base material |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPH0616447A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2006080294A1 (en) * | 2005-01-26 | 2006-08-03 | Shin-Etsu Chemical Co., Ltd. | Quartz glass preform for optical fiber and process for producing the same |
-
1992
- 1992-06-26 JP JP4191294A patent/JPH0616447A/en active Pending
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2006080294A1 (en) * | 2005-01-26 | 2006-08-03 | Shin-Etsu Chemical Co., Ltd. | Quartz glass preform for optical fiber and process for producing the same |
JP2006206356A (en) * | 2005-01-26 | 2006-08-10 | Shin Etsu Chem Co Ltd | Quartz glass preform for optical fiber and its manufacturing method |
JP4614782B2 (en) * | 2005-01-26 | 2011-01-19 | 信越化学工業株式会社 | Method for producing quartz glass preform for optical fiber |
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