JPH0558663A - Production of parent material for optical fiber - Google Patents

Production of parent material for optical fiber

Info

Publication number
JPH0558663A
JPH0558663A JP25474291A JP25474291A JPH0558663A JP H0558663 A JPH0558663 A JP H0558663A JP 25474291 A JP25474291 A JP 25474291A JP 25474291 A JP25474291 A JP 25474291A JP H0558663 A JPH0558663 A JP H0558663A
Authority
JP
Japan
Prior art keywords
optical fiber
core
clad
parent material
production
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP25474291A
Other languages
Japanese (ja)
Other versions
JP2977966B2 (en
Inventor
Tadashi Takahashi
正 高橋
Junichi Tamura
順一 田村
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Furukawa Electric Co Ltd
Original Assignee
Furukawa Electric Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Furukawa Electric Co Ltd filed Critical Furukawa Electric Co Ltd
Priority to JP25474291A priority Critical patent/JP2977966B2/en
Publication of JPH0558663A publication Critical patent/JPH0558663A/en
Application granted granted Critical
Publication of JP2977966B2 publication Critical patent/JP2977966B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/012Manufacture of preforms for drawing fibres or filaments
    • C03B37/014Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Manufacture, Treatment Of Glass Fibers (AREA)
  • Glass Melting And Manufacturing (AREA)

Abstract

PURPOSE:To provide a method for production of a parent material for an optical fiber, capable of producing an optical fiber excellent in dispersion properties and flexural loss without injury to the intersurface of the core. CONSTITUTION:In production of a parent material of a single mode optical fiber where the core part and the clad part of a soot parent material are synthesized in the same process by VAD method, the ratio (P) of clad diameter/core diameter expressed is controlled to a value within a range of 1.0<P<1.4.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明はVAD法によりコア部と
クラッド部とを同一工程で製造する光ファイバ母材の製
造方法に関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for manufacturing an optical fiber preform in which a core part and a clad part are manufactured in the same process by the VAD method.

【0002】[0002]

【従来の技術】従来から、VAD法によりコア部とクラ
ッド部を同一工程で合成してシングルモード光ファイバ
母材を製造する方法がある。この光ファイバ母材は、次
工程で加熱して脱水透明化されている。この場合、コア
ロッド内への不純物の拡散による伝送損失の悪化防止
と、クラッド合成工程の効率アップを目的として、クラ
ッド部径/コア部径比PをP≧2.0程度の範囲で合成
していた。
2. Description of the Related Art Conventionally, there is a method of manufacturing a single mode optical fiber preform by synthesizing a core portion and a cladding portion in the same process by the VAD method. This optical fiber preform is dehydrated and transparentized by heating in the next step. In this case, in order to prevent the deterioration of the transmission loss due to the diffusion of impurities into the core rod and to improve the efficiency of the clad synthesizing process, the clad diameter / core diameter ratio P is synthesized within the range of P ≧ 2.0. It was

【0003】[0003]

【発明が解決しようとする課題】しかしながら上記VA
D法において合成した多孔質スート母材を脱水透明化す
る際、コアに含まれるGeO2 がクラッド部へ拡散し、
得られるロッドのプロファイルは図1に破線で示すよう
にコアの裾3が広がり、完成時の光ファイバの分散特
性、曲げ損失が悪化する原因となる。また、クラッド部
にクラックも入り易くなる。この裾3の広がりをなくす
にはコアのみを合成(P=1)し、それを透明ガラス化
した後、その外周にクラッドを合成することが考えられ
るが、そのようにすると透明ガラス化の工程において光
ファイバの特性を左右するコアの界面に傷が付きやすく
なり、コア近傍の欠陥が増え、1.52μmの波長にS
i−H結合に起因する吸収ピークが生ずるという問題点
があった。図2はVAD法を用いてコアのみを合成し、
それを透明ガラス化した後、その外周にクラッドを合成
して光ファイバ母材を作製したときのプロファイルを示
す図である。同光ファイバ母材を線引して得られた光フ
ァイバを1atm.、100%H2 、室温雰囲気中に8
時間保持し、48時間後にその伝送損失を測定したとこ
ろ1.52μmの波長で1.0dB/kmを越える吸収
ピークが現われた。
DISCLOSURE OF THE INVENTION Problems to be Solved by the Invention
When dehydrating and transparentizing the porous soot base material synthesized in the method D, GeO 2 contained in the core diffuses into the clad portion,
In the obtained rod profile, the skirt 3 of the core expands as shown by the broken line in FIG. 1, which causes deterioration of the dispersion characteristics and bending loss of the optical fiber at the time of completion. In addition, cracks are likely to occur in the clad portion. In order to eliminate the spread of the skirt 3, it is conceivable to synthesize only the core (P = 1), make it transparent vitrified, and then synthesize the clad on the outer periphery thereof. At the interface of the core, which influences the characteristics of the optical fiber, is easily scratched, defects near the core increase, and the S wavelength becomes 1.52 μm.
There is a problem that an absorption peak due to the i-H bond occurs. 2 shows that only the core is synthesized using the VAD method,
It is a figure which shows the profile at the time of producing an optical fiber preform by synthesize | combining a clad on the outer periphery after making it transparent glass. An optical fiber obtained by drawing the same optical fiber preform is 1 atm. , 100% H 2 , 8 at room temperature
When the transmission loss was measured after holding for 48 hours, an absorption peak exceeding 1.0 dB / km appeared at a wavelength of 1.52 μm.

【0004】本発明の目的はコアの界面を傷つけること
なく、分散特性、曲げ損失の良好な光ファイバが得られ
る光ファイバ母材の製造方法を提供することにある。
An object of the present invention is to provide a method for producing an optical fiber preform capable of obtaining an optical fiber having good dispersion characteristics and bending loss without damaging the interface of the core.

【0005】[0005]

【課題を解決するための手段】本発明の光ファイバ母材
の製造方法はVAD法によりスート母材のコア部とクラ
ッド部とを同一工程で合成するシングルモード光ファイ
バ母材の製造方法において、クラッド径/コア径比Pが
1.0<P<1.4の範囲となるようにしたものであ
る。
The method for producing an optical fiber preform according to the present invention is a method for producing a single mode optical fiber preform in which a core part and a clad part of a soot preform are synthesized by the VAD method in the same step. The clad diameter / core diameter ratio P is in the range of 1.0 <P <1.4.

【0006】[0006]

【作用】本発明の光ファイバ母材の製造方法でクラッド
部径/コア部径比Pを1.0<P<1.4の範囲とした
ので、脱水透明化時にコアに含まれるGeO2 がクラッ
ド部へ拡散することによって生じるコア部の裾3の広が
りを小さくすることができる。
Since the range of the optical fiber 1.0 cladding portion diameter / core section diameter ratio P in the manufacturing method of the base material <P <1.4 of the effects of the present invention, GeO 2 is contained in the core during dehydration transparency It is possible to reduce the spread of the skirt 3 of the core portion caused by the diffusion into the clad portion.

【0007】[0007]

【実施例】本発明において1.0<P<1.4の場合と
コア合成用バーナーの条件を変更してコア径を太くする
かクラッド合成用バーナーの条件を変更してクラッド径
を細くすることにより行なうクラッド部径/コア部径比
Pの違いによる光ファイバ母材のプロファイルの違いを
図1に示す。P=3.2の場合は、P=1.3のときに
比べて裾3の広がりが大きくなる。これらの光ファイバ
母材をこれにより作製した母材を光ファイバにし、さら
にP=1.4の光ファイバ母材も作製して、これも紡糸
して光ファイバにし、各々の分散特性及びモードフィー
ルド径(MFD)等を比較した結果を表1に示す。
EXAMPLES In the present invention, when 1.0 <P <1.4, the condition of the burner for core synthesis is changed to increase the core diameter, or the condition of the burner for clad synthesis is changed to reduce the clad diameter. FIG. 1 shows the difference in the profile of the optical fiber preform due to the difference in the clad diameter / core diameter ratio P. In the case of P = 3.2, the spread of the skirt 3 becomes larger than that in the case of P = 1.3. These optical fiber preforms are used to make the preforms that are made into optical fibers, and also the optical fiber preforms with P = 1.4, which are also spun into optical fibers. Table 1 shows the results of comparison of the diameter (MFD) and the like.

【0008】[0008]

【表1】 [Table 1]

【0009】表1より、同一のΔTOP (最大比屈折率
差)およびλc(カットオフ波長)の場合、P=3.2
の場合とP=1.3及びP=1.4の場合とを比較する
と、P=1.3及びP=1.4のほうが分散特性も、M
FDも共に小さくなっている。また、P=1.4の場合
はP=1.3の場合よりP=3.2の場合との分散特性
及びMFDの変化が大きくないことから、脱水透明化時
のGeO2 の拡散による分散特性への影響はP≧1.4
の領域では鈍くなることが分かる。尚、P<1.4のと
きGeO2 の拡散による裾の広がりが小さくなる理由は
以下のように考えられる。多孔質スート母材の最外層部
の焼結時間は、スートの密度や径が同じであれば同一と
考えられる。従ってPが小さい程、コアに近い部分の焼
結が速く完了し、それ故GeO2 の拡散がよりコア近傍
で止まる。即ち裾の広がりが小さく抑えられる。従って
P<1.4で合成を行うことで分散特性を良好な値に保
つことができる。尚、コア部の界面の保護のために1.
0<Pが必要であるので、良好な分散特性及びMFDを
保つためのPの適性値は1.0<P<1.4と考えられ
る。
From Table 1, P = 3.2 for the same Δ TOP (maximum relative refractive index difference) and λ c (cutoff wavelength).
Comparing the case of P = 1.3 and the case of P = 1.4, the dispersion characteristics of P = 1.3 and P = 1.4 are
Both FDs are getting smaller. In addition, when P = 1.4, the dispersion characteristics and MFD of P = 3.2 are not so different from the case of P = 1.3, so dispersion due to diffusion of GeO 2 during dehydration and transparency Influence on characteristics is P ≧ 1.4
It can be seen that the area becomes dull. Incidentally, the reason why the skirt expansion due to the diffusion of GeO 2 becomes smaller when P <1.4 is considered as follows. The sintering time of the outermost layer of the porous soot base material is considered to be the same if the soot has the same density and diameter. Therefore, the smaller P is, the faster the sintering near the core is completed, and therefore the diffusion of GeO 2 stops closer to the core. That is, the spread of the hem can be suppressed small. Therefore, the dispersion characteristic can be maintained at a good value by performing the composition with P <1.4. In order to protect the interface of the core part, 1.
Since 0 <P is required, the suitability value of P for maintaining good dispersion characteristics and MFD is considered to be 1.0 <P <1.4.

【0010】[0010]

【発明の効果】本発明の光ファイバ母材の製造方法は次
のような効果がある。 .光ファイバ内を伝搬する光の分散特性が向上し、Δ
を従来より大きくしても分散規格を満足できるので曲げ
損失特性の優れた光ファイバが得られる。 .クラッド部の量が減ることで脱水透明化時に発生す
るクラックが減少する。
The method of manufacturing the optical fiber preform of the present invention has the following effects. . The dispersion characteristics of the light propagating in the optical fiber are improved, and Δ
Since the dispersion standard can be satisfied even when the value is larger than the conventional value, an optical fiber with excellent bending loss characteristics can be obtained. . By reducing the amount of the clad portion, the cracks that occur during dehydration and transparency are reduced.

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明の光ファイバ母材の製造方法においてP
=1.3の場合とP=3.2の場合のコア周辺部の裾の
拡がりを示す説明図。
FIG. 1 is a diagram illustrating a method of manufacturing an optical fiber preform according to the present invention, wherein P
Explanatory drawing which shows the skirt expansion of a core peripheral part in the case of = 1.3 and in the case of P = 3.2.

【図2】従来の光ファイバ母材の製造方法において作製
された光ファイバのプロファイルの一例を示す説明図。
FIG. 2 is an explanatory diagram showing an example of a profile of an optical fiber manufactured by a conventional method of manufacturing an optical fiber preform.

【符号の説明】[Explanation of symbols]

3 裾 3 hem

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】 VAD法によりスート母材のコア部とク
ラッド部とを同一工程で合成するシングルモード光ファ
イバ母材の製造方法において、クラッド部径/コア部径
比Pを1.0<P<1.4の範囲とすることを特徴とす
る光ファイバ母材の製造方法。
1. A method of manufacturing a single mode optical fiber preform in which a core part and a clad part of a soot base material are synthesized in the same step by the VAD method, and a clad part diameter / core part diameter ratio P is 1.0 <P. <1.4 range, optical fiber preform manufacturing method characterized by the above.
JP25474291A 1991-09-05 1991-09-05 Method for manufacturing single mode optical fiber preform Expired - Lifetime JP2977966B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP25474291A JP2977966B2 (en) 1991-09-05 1991-09-05 Method for manufacturing single mode optical fiber preform

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP25474291A JP2977966B2 (en) 1991-09-05 1991-09-05 Method for manufacturing single mode optical fiber preform

Publications (2)

Publication Number Publication Date
JPH0558663A true JPH0558663A (en) 1993-03-09
JP2977966B2 JP2977966B2 (en) 1999-11-15

Family

ID=17269240

Family Applications (1)

Application Number Title Priority Date Filing Date
JP25474291A Expired - Lifetime JP2977966B2 (en) 1991-09-05 1991-09-05 Method for manufacturing single mode optical fiber preform

Country Status (1)

Country Link
JP (1) JP2977966B2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000026709A1 (en) * 1998-11-02 2000-05-11 Sumitomo Electric Industries, Ltd. Single-mode optical fiber and its production method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000026709A1 (en) * 1998-11-02 2000-05-11 Sumitomo Electric Industries, Ltd. Single-mode optical fiber and its production method
US6625360B2 (en) 1998-11-02 2003-09-23 Sumitomo Electric Industries, Ltd. Single-mode optical fibers and fabrication methods thereof

Also Published As

Publication number Publication date
JP2977966B2 (en) 1999-11-15

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