JPH0434893Y2 - - Google Patents

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Publication number
JPH0434893Y2
JPH0434893Y2 JP1986108028U JP10802886U JPH0434893Y2 JP H0434893 Y2 JPH0434893 Y2 JP H0434893Y2 JP 1986108028 U JP1986108028 U JP 1986108028U JP 10802886 U JP10802886 U JP 10802886U JP H0434893 Y2 JPH0434893 Y2 JP H0434893Y2
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JP
Japan
Prior art keywords
gas
mixed gas
pressure
mixed
control valve
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP1986108028U
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Japanese (ja)
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JPS6316834U (en
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Priority to JP1986108028U priority Critical patent/JPH0434893Y2/ja
Publication of JPS6316834U publication Critical patent/JPS6316834U/ja
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Expired legal-status Critical Current

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Description

【考案の詳細な説明】 〔産業上の利用分野〕 本考案は、酸化性の雰囲気ガスによつて被処理
品を熱処理する酸化雰囲気炉の雰囲気ガス製造装
置に関する。
[Detailed Description of the Invention] [Industrial Application Field] The present invention relates to an atmosphere gas production device for an oxidizing atmosphere furnace that heat-treats a workpiece with an oxidizing atmosphere gas.

〔従来の技術〕[Conventional technology]

熱間熱水圧加圧装置(以下HIP装置と称する)
は、すでに超硬工具の緻密化処理に使用されて実
績を挙げているが、近年、セラミツクス、サーメ
ツトなど新素材の開発が進むにつれて、その適用
範囲が拡がりつつある。
Hot water pressure equipment (hereinafter referred to as HIP equipment)
has already been used successfully for the densification of cemented carbide tools, but in recent years, as the development of new materials such as ceramics and cermets has progressed, its scope of application has been expanding.

従来装置の一例であるHIP装置及びその加圧媒
体である例えばアルゴンガス(以下Arと称する)
のような雰囲気ガスを供給する装置を第2図によ
つて説明すると、20はHIP装置で、円筒胴20
a、上蓋20b及び下蓋20c、とこれらで構成
された加圧室20eに収納される加熱炉20d等
の主要部材からなり、開閉弁11、フイルタ1
3、逆止弁14、冷却器22及びガス配管10を
介してArボンベ1bに連結されている。
HIP equipment, which is an example of conventional equipment, and its pressurized medium, such as argon gas (hereinafter referred to as Ar)
A device for supplying atmospheric gas as shown in FIG. 2 will be explained with reference to FIG.
a, an upper lid 20b, a lower lid 20c, and a heating furnace 20d housed in a pressurizing chamber 20e composed of these, and an on-off valve 11, a filter 1, etc.
3. It is connected to the Ar cylinder 1b via a check valve 14, a cooler 22, and a gas pipe 10.

冷却器22の上流及び下流の雰囲気ガス配管1
0には増圧機21が連結され、雰囲気ガス配管1
0の各要所には、圧力計12、圧力支軸調節器1
8、放出弁11aが装設されている。圧力指示調
節器18と増圧機21とは電気的に連結されてい
る。
Atmospheric gas piping 1 upstream and downstream of the cooler 22
A pressure booster 21 is connected to the atmospheric gas pipe 1.
At each important point of 0, there is a pressure gauge 12, a pressure support shaft regulator 1
8. A discharge valve 11a is installed. The pressure indicating regulator 18 and the pressure intensifier 21 are electrically connected.

これらの逆止弁14、増圧機21、冷却器2
2、圧力計12、圧力指示調節器18、ガス配管
10によつて増圧ユニツトAが構成されている。
These check valve 14, pressure booster 21, cooler 2
2, a pressure gauge 12, a pressure indicating regulator 18, and a gas pipe 10 constitute a pressure increasing unit A.

また、HIP装置20入口の雰囲気ガス配管10
には、開閉弁11を介して真空ポンプ24が装設
されている。
In addition, the atmospheric gas pipe 10 at the inlet of the HIP device 20
A vacuum pump 24 is installed through an on-off valve 11.

被処理品が装填された加熱炉20dを加圧室2
0eへ収納し、真空ポンプ24によつて加圧室2
0eを略真空に吸引する。次に、Arボンベ1b
から例えば100〜150Kgf/cm2のような高圧の雰囲
気ガスを雰囲気ガス配管10へ供給し、フイルタ
13で不純物を除去して増圧機21によつて一次
増圧する。一次増圧によつて昇温した雰囲気ガス
を冷却器22によつて冷却し、更に増圧機21に
よつて例えば2000Kgf/cm2のような超高圧に二次
増圧してHIP装置へ供給する。圧力指示調節器1
8は、超高圧雰囲気ガスの圧力値を常に検出し、
予め設定された例えば2000Kgf/cm2のような圧力
値を保持するよう、増圧機21の作動を調節す
る。被処理品の加熱加圧処理が完了すると、放出
弁11aによつて加圧室20eの雰囲気ガスを大
気中に放出し、大気圧に減圧して上蓋20bを外
し、加熱炉20dを取り出す。
The heating furnace 20d loaded with the products to be processed is transferred to the pressurizing chamber 2.
0e and pressurized chamber 2 by vacuum pump 24.
Aspirate 0e to a near vacuum. Next, Ar cylinder 1b
A high-pressure atmospheric gas of, for example, 100 to 150 Kgf/cm 2 is supplied from the atmosphere to the atmospheric gas pipe 10 , impurities are removed by a filter 13 , and the pressure is primarily increased by a pressure intensifier 21 . The atmospheric gas whose temperature has been raised by the primary pressure increase is cooled by the cooler 22, and further pressure increased to an ultra-high pressure such as 2000 Kgf/cm 2 by the pressure intensifier 21, and then supplied to the HIP device. Pressure indicator regulator 1
8 constantly detects the pressure value of ultra-high pressure atmospheric gas,
The operation of the pressure booster 21 is adjusted so as to maintain a preset pressure value of, for example, 2000 Kgf/cm 2 . When the heating and pressurizing treatment of the workpiece is completed, the atmospheric gas in the pressurizing chamber 20e is released into the atmosphere by the release valve 11a, the pressure is reduced to atmospheric pressure, the upper cover 20b is removed, and the heating furnace 20d is taken out.

〔考案が解決しようとする問題点〕[Problem that the invention attempts to solve]

ところが、前記したようなAr等の不活性ガス
を雰囲気ガスとして、ZrO2、Al2O2、BaTiO3
ZnO、MgO、Y2O3等の酸化物系セラミツクスの
被処理品を、例えば1600℃、2000Kgf/cm2のよう
な高温超高圧で処理すると、同被処理品がO2
解を生じてその特性が劣化し、変質、変色、機械
的性質の低下等が生ずる。そこで、このような不
具合を防止するために、Ar等の不活性ガスに酸
素ガス(以下O2と称する)を、その被処理品の
種類によつて最適な体積比で混合した雰囲気ガス
を使用するO2HIP法が開発され、その雰囲気ガ
スを製造してHIP装置へ供給する装置の開発が急
がれていた。
However, when using an inert gas such as Ar as described above as an atmospheric gas, ZrO 2 , Al 2 O 2 , BaTiO 3 ,
When a treated product made of oxide ceramics such as ZnO, MgO, Y2O3 , etc. is treated at a high temperature and ultra - high pressure such as 1600℃ and 2000Kgf/ cm2 , the treated product causes O2 decomposition and its Properties deteriorate, resulting in deterioration, discoloration, deterioration of mechanical properties, etc. Therefore, in order to prevent such problems, we use an atmosphere gas that is a mixture of inert gas such as Ar and oxygen gas (hereinafter referred to as O 2 ) in the optimal volume ratio depending on the type of product to be processed. The O 2 HIP method was developed, and there was an urgent need to develop equipment to produce the atmospheric gas and supply it to the HIP equipment.

〔目的〕〔the purpose〕

本考案は、上記要望にそう雰囲気ガス製造装置
を提供することを目的とし、酸化性の雰囲気ガス
によつて被処理品を熱処理する酸化雰囲気炉の雰
囲気ガス製造装置を提供することを目的とする。
The purpose of the present invention is to provide an atmosphere gas production device that satisfies the above-mentioned needs, and the purpose of the present invention is to provide an atmosphere gas production device for an oxidizing atmosphere furnace that heat-treats a workpiece with an oxidizing atmosphere gas. .

〔問題点を解決するための手段〕[Means for solving problems]

すなわち、本考案は、不活性ガスと、酸素と不
活性ガスとの混合ガスを所定比率に混合する雰囲
気ガス製造装置において、前記混合ガスが不活性
ガスと上限混合比率の酸素ガスとからなる混合ガ
スであつて、同混合ガスが充填された混合ガス供
給源と、該混合ガスの供給路に配設された混合ガ
ス流量制御弁と、不活性ガス供給源と、該不活性
ガスの供給路に配設された不活性ガス流量制御弁
と、前記混合ガスの供給路と前記不活性ガスの供
給路とに連結されたガス混合装置と、該ガス混合
装置に装設された圧力調節手段と、前記ガス混合
装置の下流の雰囲気ガス供給路に配設されて前記
混合ガス流量制御弁と前記不活性ガス流量制御弁
とに連結されたガス混合比率制御装置とを具えて
なることを特徴とする雰囲気ガス製造装置であ
る。
That is, the present invention provides an atmospheric gas production device that mixes an inert gas and a mixed gas of oxygen and an inert gas at a predetermined ratio. A mixed gas supply source filled with the mixed gas, a mixed gas flow control valve disposed in the mixed gas supply path, an inert gas supply source, and the inert gas supply path. an inert gas flow control valve disposed in the inert gas flow rate control valve, a gas mixing device connected to the mixed gas supply path and the inert gas supply path, and a pressure regulating means installed in the gas mixing device; , comprising a gas mixture ratio control device disposed in an atmospheric gas supply path downstream of the gas mixing device and connected to the mixed gas flow rate control valve and the inert gas flow rate control valve. This is an atmospheric gas production device.

本考案において、上限酸素濃度の雰囲気ガスを
用いる場合は混合ガス供給源から焼成炉へ混合ガ
スを供給し、圧力調節手段によつて所定の圧力に
保持する。一方、上限よりも酸素濃度の低い雰囲
気ガスを用いる場合は、混合ガス供給源と不活性
ガス供給源とからガス混合装置へ各々のガスを供
給し、混合ガス比率制御装置によつて、酸素濃度
を検出し、予め指定された所定の酸素濃度になる
ように、混合ガス流量制御弁と不活性ガス流量制
御弁とを制御して所定の混合比率を保持し、圧力
調節手段によつて所定の圧力に保持する。
In the present invention, when an atmospheric gas having an upper limit oxygen concentration is used, the mixed gas is supplied from the mixed gas supply source to the firing furnace and maintained at a predetermined pressure by the pressure regulating means. On the other hand, when using an atmospheric gas with an oxygen concentration lower than the upper limit, each gas is supplied from the mixed gas supply source and the inert gas supply source to the gas mixing device, and the oxygen concentration is adjusted by the mixed gas ratio control device. is detected, the mixed gas flow control valve and the inert gas flow control valve are controlled to maintain a predetermined mixing ratio so that a predetermined oxygen concentration is achieved, and the pressure adjustment means is used to maintain a predetermined mixing ratio. Hold in pressure.

〔実施例〕〔Example〕

以下、本考案の実施例を第1図の配置図によつ
て説明するが従来装置と同一の部材には同一の符
号を付し、構成及び作用の重複説明を省略する。
Hereinafter, an embodiment of the present invention will be described with reference to the layout diagram of FIG. 1. The same members as those of the conventional device will be denoted by the same reference numerals, and redundant explanation of the structure and operation will be omitted.

図において、1aはArに20%のO2が混入され
た混合ガス(以下20%O2混合ガスと称する)が
充填された混合ガスボンベで、開閉弁11、フイ
ルタ13、混合ガス流量制御弁15a、逆止弁1
4、自動開閉弁16及び混合ガス配管10aを介
してミキシングタンク4に連結されている。
In the figure, 1a is a mixed gas cylinder filled with a mixed gas of Ar mixed with 20% O2 (hereinafter referred to as 20% O2 mixed gas), which includes an on-off valve 11, a filter 13, and a mixed gas flow rate control valve 15a. , check valve 1
4. Connected to the mixing tank 4 via an automatic on-off valve 16 and a mixed gas pipe 10a.

1bはArボンベで、開閉弁11、フイルタ1
3、Ar流量制御弁15b、逆止弁14及びAr配
管10bを介して、自動開閉弁16入側の混合ガ
ス配管10aに連結されている。混合ガス配管1
0a、Ar配管10b及びミキシングタンク4に
は圧力計12が装設されている。また、ミキシン
グタンク4には圧力指示調節器18が装設され、
自動開閉弁16に電気的に連結されている。
1b is an Ar cylinder, on-off valve 11, filter 1
3. It is connected to the mixed gas pipe 10a on the inlet side of the automatic on-off valve 16 via the Ar flow rate control valve 15b, the check valve 14, and the Ar pipe 10b. Mixed gas piping 1
0a, the Ar pipe 10b, and the mixing tank 4 are equipped with a pressure gauge 12. Further, the mixing tank 4 is equipped with a pressure indicating regulator 18,
It is electrically connected to the automatic on-off valve 16.

このミキシングタンク4はO2濃度検出器8、
開閉弁11及び雰囲気ガス配管10を介して増圧
ユニツトAへ連結されている。17はO2濃度指
示調節器で、混合ガス流量制御弁15a、Ar流
量制御弁15b及びO2濃度検出器8に電気的に
連結されている。雰囲気ガス配管10の酸素濃度
検出器8の下流には開放弁11bが装設されてい
る。(図中※印は雰囲気ガス配管の連結を示す。) HIP装置20において例えばAr=80%、O2
20%の雰囲気ガスを使用する場合は、混合ガスボ
ンベ1aから100〜150Kgf/cm2の20%O2混合ガ
スを、フイルタ13、開放された混合ガス流量制
御弁15a、自動開閉弁16、混合ガス配管10
a、ミキシングタンク4、雰囲気ガス配管10、
酸素濃度検出器8、開閉弁11を経て増圧ユニツ
トAへ供給する。このとき、圧力指示調節器18
はミキシングタンク4内の圧力を検出し、その圧
力が100Kgf/cm2を超えていれば自動開閉弁16
を開閉させて調節し、その圧力をほぼ100Kgf/
cm2に保持する。
This mixing tank 4 has an O 2 concentration detector 8,
It is connected to the pressure increasing unit A via an on-off valve 11 and an atmospheric gas pipe 10. Reference numeral 17 denotes an O 2 concentration indicating regulator, which is electrically connected to the mixed gas flow rate control valve 15a, the Ar flow rate control valve 15b, and the O 2 concentration detector 8. A release valve 11b is installed downstream of the oxygen concentration detector 8 in the atmospheric gas pipe 10. (The * mark in the figure indicates the connection of atmospheric gas piping.) In the HIP device 20, for example, Ar = 80%, O 2 =
When using 20% atmospheric gas, apply 20% O 2 mixed gas of 100 to 150 kgf/cm 2 from the mixed gas cylinder 1a to the filter 13, the opened mixed gas flow control valve 15a, the automatic on-off valve 16, and the mixed gas. Piping 10
a, mixing tank 4, atmospheric gas piping 10,
It is supplied to the pressure boosting unit A via the oxygen concentration detector 8 and the on-off valve 11. At this time, the pressure indication regulator 18
detects the pressure inside the mixing tank 4, and if the pressure exceeds 100Kgf/ cm2 , the automatic on-off valve 16 is activated.
Adjust the pressure by opening and closing and adjust the pressure to approximately 100Kgf/
Hold in cm 2 .

次に、被処理品が異なり、例えばO2濃度が15
%の雰囲気ガスを使用する場合は、Arボンベ1
bからArをフイルタ13、Ar流量制御弁15
b、逆止弁14、Ar配管10bを経て混合ガス
配管10aへ供給し、混合ガスボンベ1aから供
給される20%O2混合ガスと合流して自動開閉弁
16を経てミキシングタンク4へ供給する。この
とき、20%O2混合ガスが75%、Arが25%となる
よう、双方の流量制御弁15a,15bを調節
し、ミキシングタンク4によつて両者を混合し、
O2混合比が15%の雰囲気ガスを製造する。そし
て、この雰囲気ガスを雰囲気ガス配管10へ供給
し、開閉弁11を閉じて開放弁11bを開き、雰
囲気ガスを大気中に放出しながらO2濃度検出器
8でO2濃度を検出し、予め15%のO2濃度が設定
されたO2濃度指示調節器17を介して混合ガス
流量制御弁15a及びAr流量制御弁15bを自
動制御してO2濃度を微調節し、O2濃度が安定す
ると開閉弁11を開いて開放弁11bを閉じ、増
圧ユニツトAへこの雰囲気ガスを供給する。圧力
指示調節器18はミキシングタンク4内の圧力を
検出し、その圧力が100Kgf/cm2を超えると自動
開閉弁16を開閉させて調節し、その圧力をほぼ
100Kgf/cm2に保持する。
Next, the products to be treated are different, for example, the O 2 concentration is 15
% atmosphere gas, use Ar cylinder 1
Ar from b to filter 13, Ar flow rate control valve 15
b. It is supplied to the mixed gas pipe 10a via the check valve 14 and the Ar pipe 10b, where it joins with the 20% O 2 mixed gas supplied from the mixed gas cylinder 1a, and is supplied to the mixing tank 4 via the automatic opening/closing valve 16. At this time, both flow control valves 15a and 15b are adjusted so that the 20% O 2 mixed gas is 75% and the Ar is 25%, and both are mixed by the mixing tank 4.
Produce an atmosphere gas with an O 2 mixing ratio of 15%. Then, this atmospheric gas is supplied to the atmospheric gas piping 10, the on-off valve 11 is closed and the release valve 11b is opened, and while the atmospheric gas is released into the atmosphere, the O 2 concentration is detected by the O 2 concentration detector 8, and the O 2 concentration is detected in advance. The O 2 concentration is finely adjusted by automatically controlling the mixed gas flow control valve 15a and the Ar flow control valve 15b via the O 2 concentration indicating regulator 17, which is set to an O 2 concentration of 15%, and the O 2 concentration is stabilized. Then, the on-off valve 11 is opened, the release valve 11b is closed, and the atmospheric gas is supplied to the pressure increase unit A. The pressure indicator regulator 18 detects the pressure inside the mixing tank 4, and when the pressure exceeds 100Kgf/cm 2 , it opens and closes the automatic on-off valve 16 to adjust the pressure to approximately the same level.
Maintain at 100Kgf/ cm2 .

〔考案の効果〕[Effect of idea]

本考案は、以上詳記した構成からなる雰囲気ガ
ス製造装置であり、そして、雰囲気ガスへの酸素
供給手段に、不活性ガスと上限混合比率の酸素ガ
スとから成る混合ガスを用いることにより、雰囲
気ガスの酸素濃度管理が容易になり、上限濃度を
超える酸素供給過剰が無くなるので安全であり、
被処理品の良好な焼成が可能である効果が生ず
る。
The present invention is an atmospheric gas production device having the configuration described in detail above, and by using a mixed gas consisting of an inert gas and an oxygen gas at an upper limit mixing ratio as a means for supplying oxygen to the atmospheric gas. It is safe because it makes it easier to manage the oxygen concentration of the gas and eliminates excess oxygen supply exceeding the upper limit concentration.
The effect is that the article to be processed can be fired in a good manner.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図は本考案の一実施例である雰囲気ガス製
造装置の概略配置図であり、第2図は従来装置の
一例を示す概略配置図である。 1a……混合ガスボンベ、1b……Arボンベ、
4……ミキシングタンク、8……O2濃度検出器、
10……ガス配管、10a……混合ガス配管、1
0b……Ar配管、11……開閉弁、11a……
放出弁、11b……開放弁、12……圧力計、1
3……フイルタ、14……逆止弁、15a……混
合ガス流量制御弁、15b……Ar流量制御弁、
16……自動開閉弁、17……O2濃度指示調節
器、18……圧力指示調節器、20……HIP装
置、20a……円筒胴、20b……上蓋、20c
……下蓋、20d……加熱炉、20e……加圧
室、21……増圧機、22……冷却器、24……
真空ポンプ、A……増圧ユニツト。
FIG. 1 is a schematic layout diagram of an atmospheric gas production device which is an embodiment of the present invention, and FIG. 2 is a schematic layout diagram showing an example of a conventional device. 1a...Mixed gas cylinder, 1b...Ar cylinder,
4...Mixing tank, 8... O2 concentration detector,
10...Gas piping, 10a...Mixed gas piping, 1
0b...Ar piping, 11...Opening/closing valve, 11a...
Release valve, 11b...Release valve, 12...Pressure gauge, 1
3...Filter, 14...Check valve, 15a...Mixed gas flow rate control valve, 15b...Ar flow rate control valve,
16...Automatic opening/closing valve, 17... O2 concentration indicating regulator, 18...Pressure indicating regulator, 20...HIP device, 20a...Cylindrical body, 20b...Top lid, 20c
... Lower lid, 20d ... Heating furnace, 20e ... Pressure chamber, 21 ... Pressure booster, 22 ... Cooler, 24 ...
Vacuum pump, A...pressure booster unit.

Claims (1)

【実用新案登録請求の範囲】[Scope of utility model registration request] 不活性ガスと、酸素ガスと不活性ガスとの混合
ガスを所定比率に混合する雰囲気ガス製造装置に
おいて、前記混合ガスが不活性ガスと上限混合比
率の酸素ガスとからなる混合ガスであつて、同混
合ガスが充填された混合ガス供給源と、該混合ガ
スの供給路に配設された混合ガス流量制御弁と、
不活性ガス供給源と、該不活性ガスの供給路に配
設された不活性ガス流量制御弁と、前記混合ガス
の供給路と前記不活性ガスの供給路とに連結され
たガス混合装置と、該ガス混合装置に装設された
圧力調節手段と、前記ガス混合装置の下流の雰囲
気ガス供給路に配設されて前記混合ガス流量制御
弁と前記不活性ガス流量制御弁とに連結されたガ
ス混合比率制御装置とを具えてなることを特徴と
する雰囲気ガス製造装置。
In an atmospheric gas production device that mixes an inert gas and a mixed gas of oxygen gas and inert gas at a predetermined ratio, the mixed gas is a mixed gas consisting of an inert gas and an upper limit mixing ratio of oxygen gas, a mixed gas supply source filled with the mixed gas; a mixed gas flow rate control valve disposed in the mixed gas supply path;
an inert gas supply source, an inert gas flow control valve disposed in the inert gas supply path, and a gas mixing device connected to the mixed gas supply path and the inert gas supply path; , a pressure regulating means installed in the gas mixing device, and a pressure regulating means provided in an atmospheric gas supply path downstream of the gas mixing device and connected to the mixed gas flow rate control valve and the inert gas flow rate control valve. An atmospheric gas production device characterized by comprising a gas mixture ratio control device.
JP1986108028U 1986-07-16 1986-07-16 Expired JPH0434893Y2 (en)

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JP1986108028U JPH0434893Y2 (en) 1986-07-16 1986-07-16

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JP1986108028U JPH0434893Y2 (en) 1986-07-16 1986-07-16

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JPS6316834U JPS6316834U (en) 1988-02-04
JPH0434893Y2 true JPH0434893Y2 (en) 1992-08-19

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JP1986108028U Expired JPH0434893Y2 (en) 1986-07-16 1986-07-16

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Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5743828B2 (en) * 1975-10-29 1982-09-17

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6344099Y2 (en) * 1980-08-26 1988-11-16

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5743828B2 (en) * 1975-10-29 1982-09-17

Also Published As

Publication number Publication date
JPS6316834U (en) 1988-02-04

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