JPH0422906B2 - - Google Patents
Info
- Publication number
- JPH0422906B2 JPH0422906B2 JP11977683A JP11977683A JPH0422906B2 JP H0422906 B2 JPH0422906 B2 JP H0422906B2 JP 11977683 A JP11977683 A JP 11977683A JP 11977683 A JP11977683 A JP 11977683A JP H0422906 B2 JPH0422906 B2 JP H0422906B2
- Authority
- JP
- Japan
- Prior art keywords
- fatty acid
- acid ester
- component
- sulfonation
- ester
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- -1 fatty acid ester Chemical class 0.000 claims description 37
- 235000021122 unsaturated fatty acids Nutrition 0.000 claims description 21
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims description 16
- 239000000203 mixture Substances 0.000 claims description 9
- 125000005907 alkyl ester group Chemical group 0.000 claims description 6
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 5
- 239000000194 fatty acid Substances 0.000 claims description 5
- 229930195729 fatty acid Natural products 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 150000004671 saturated fatty acids Chemical class 0.000 claims description 3
- 150000004670 unsaturated fatty acids Chemical class 0.000 claims description 3
- 238000006277 sulfonation reaction Methods 0.000 description 25
- 238000006243 chemical reaction Methods 0.000 description 17
- 239000003921 oil Substances 0.000 description 12
- 235000019198 oils Nutrition 0.000 description 12
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 8
- 150000002148 esters Chemical class 0.000 description 8
- 125000004432 carbon atom Chemical group C* 0.000 description 7
- 238000000034 method Methods 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 125000000217 alkyl group Chemical group 0.000 description 5
- 230000007423 decrease Effects 0.000 description 4
- 239000003208 petroleum Substances 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 150000004665 fatty acids Chemical group 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000010409 thin film Substances 0.000 description 3
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000012459 cleaning agent Substances 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 239000011521 glass Substances 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 238000006386 neutralization reaction Methods 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- KEQGZUUPPQEDPF-UHFFFAOYSA-N 1,3-dichloro-5,5-dimethylimidazolidine-2,4-dione Chemical compound CC1(C)N(Cl)C(=O)N(Cl)C1=O KEQGZUUPPQEDPF-UHFFFAOYSA-N 0.000 description 1
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 235000019482 Palm oil Nutrition 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000013043 chemical agent Substances 0.000 description 1
- 239000007809 chemical reaction catalyst Substances 0.000 description 1
- 239000007810 chemical reaction solvent Substances 0.000 description 1
- XTHPWXDJESJLNJ-UHFFFAOYSA-N chlorosulfonic acid Substances OS(Cl)(=O)=O XTHPWXDJESJLNJ-UHFFFAOYSA-N 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 description 1
- 235000019387 fatty acid methyl ester Nutrition 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 150000007530 organic bases Chemical class 0.000 description 1
- 239000002540 palm oil Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 description 1
- 125000000542 sulfonic acid group Chemical group 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11977683A JPS6013751A (ja) | 1983-07-01 | 1983-07-01 | 不飽和脂肪酸エステルのスルホン酸塩の製造方法 |
| EP84304246A EP0130753B1 (en) | 1983-07-01 | 1984-06-22 | Process for producing sulfonate of unsaturated fatty acid ester |
| DE8484304246T DE3468020D1 (en) | 1983-07-01 | 1984-06-22 | Process for producing sulfonate of unsaturated fatty acid ester |
| US06/626,081 US4545939A (en) | 1983-07-01 | 1984-06-29 | Process for producing sulfonate of unsaturated fatty acid ester |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11977683A JPS6013751A (ja) | 1983-07-01 | 1983-07-01 | 不飽和脂肪酸エステルのスルホン酸塩の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6013751A JPS6013751A (ja) | 1985-01-24 |
| JPH0422906B2 true JPH0422906B2 (enExample) | 1992-04-20 |
Family
ID=14769930
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11977683A Granted JPS6013751A (ja) | 1983-07-01 | 1983-07-01 | 不飽和脂肪酸エステルのスルホン酸塩の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6013751A (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US12529738B2 (en) * | 2023-11-25 | 2026-01-20 | Inkspace Imaging, Inc. | Patient-compliant MRI coil employing patient anatomy for coil location |
-
1983
- 1983-07-01 JP JP11977683A patent/JPS6013751A/ja active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US12529738B2 (en) * | 2023-11-25 | 2026-01-20 | Inkspace Imaging, Inc. | Patient-compliant MRI coil employing patient anatomy for coil location |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6013751A (ja) | 1985-01-24 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP0130753B1 (en) | Process for producing sulfonate of unsaturated fatty acid ester | |
| JPH0430943B2 (enExample) | ||
| EP1706476B1 (en) | Novel acylalkylisethionate esters and applications in consumer products | |
| US4865774A (en) | Surface-active hydroxysulfonates | |
| US3428654A (en) | Alkene sulfonation process and products | |
| JPH0517493A (ja) | アルカリポリグリコシドの製造方法 | |
| US2687420A (en) | Process for the neutralization of sulfonated products suitable as detergents | |
| JPS6032759A (ja) | 内部オレフインスルホン酸塩の製造方法 | |
| JPH0422906B2 (enExample) | ||
| US2640070A (en) | Higher alkyl ester production | |
| JPH0142320B2 (enExample) | ||
| US5349101A (en) | Process for the preparation of secondary alkyl sulfate-containing surfactant compositions | |
| US2114042A (en) | Sulphuric derivatives of higher alcohols | |
| EP0642494B1 (en) | Process for the preparation of a surfactant composition comprising a secondary alkyl sulfate | |
| Roberts et al. | Why internal olefins are difficult to sulphonate | |
| JP3377607B2 (ja) | 不飽和アルコール硫酸エステル塩の製造法 | |
| JPH026346B2 (enExample) | ||
| US4832876A (en) | Process for the manufacture of higher fatty monoglyceride monosulfate detergents | |
| JPH09169720A (ja) | 不飽和アルコール硫酸エステル塩の製造法 | |
| US4950440A (en) | Process for the manufacture of high fatty acid monoglyceride monosulfate detergents | |
| US2042747A (en) | Sulphonated oxygenated compounds obtained by catalytic hydrogenation of oxides of carbon | |
| JPS6255A (ja) | 不飽和脂肪酸低級アルキルエステルスルホン酸塩の製造方法 | |
| JPH0421656B2 (enExample) | ||
| US2075914A (en) | Process of making sulphuric acid esters of unsaturated alcohols | |
| GB2042581A (en) | Clear aqueous olefin sulphonate solutions |