JPH04188720A - Etching of vapor growth susceptor - Google Patents
Etching of vapor growth susceptorInfo
- Publication number
- JPH04188720A JPH04188720A JP31906690A JP31906690A JPH04188720A JP H04188720 A JPH04188720 A JP H04188720A JP 31906690 A JP31906690 A JP 31906690A JP 31906690 A JP31906690 A JP 31906690A JP H04188720 A JPH04188720 A JP H04188720A
- Authority
- JP
- Japan
- Prior art keywords
- susceptor
- polysilicon film
- thin plate
- wafer
- wafer pocket
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 230000012010 growth Effects 0.000 title claims abstract description 11
- 238000005530 etching Methods 0.000 title claims description 13
- 229910021420 polycrystalline silicon Inorganic materials 0.000 claims abstract description 15
- 229920005591 polysilicon Polymers 0.000 claims abstract description 15
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims description 11
- 238000001947 vapour-phase growth Methods 0.000 claims description 7
- 239000004065 semiconductor Substances 0.000 claims description 5
- 239000012808 vapor phase Substances 0.000 claims 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract description 9
- 229910052710 silicon Inorganic materials 0.000 abstract description 9
- 239000010703 silicon Substances 0.000 abstract description 9
- 235000012431 wafers Nutrition 0.000 description 23
- 230000000694 effects Effects 0.000 description 4
- 238000011109 contamination Methods 0.000 description 3
- 239000013078 crystal Substances 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
Abstract
Description
【発明の詳細な説明】
産業上の利用分野
本発明は半導体ウェハのエピタキシャル成長に用いるサ
セプタのエツチング方法に関するものである。DETAILED DESCRIPTION OF THE INVENTION Field of the Invention The present invention relates to a method for etching a susceptor used for epitaxial growth of semiconductor wafers.
従来の技術
半導体装置の製造において、エピタキシャル成長技術は
広く用いられている。エピタキシャル成長用のサセプタ
は一般に5iC(シリコンカーフs+イト)膜でコート
されたグラファイトでできており、また半導体ウェハ、
例えばンリコンウエノ1はウェハポケットと呼ばれる凹
状に座ぐりされた部分に入れられる。そしてエピタキシ
ャル成長を行なうとシリコンウェハ上にはエピタキシャ
ル層が成長し、一方サセプタ上にはポリシリコン膜が成
長する。複数回のエピタキシャル成長を行なうとポリシ
リコン膜が積重なって厚くなりエピタキシャル層にパー
ティクル、結晶欠陥発生等の悪影響が生ずるため、−旦
すセブタ上のポリシリコン膜を高濃度の塩酸ガスでガス
エツチングして除去する。第2図に従来のサセプタエツ
チング時の断面を示す。2はサセプタ、3はウェハポケ
ット、5はサセプタ上に成長したポリシリコン膜である
。BACKGROUND OF THE INVENTION Epitaxial growth techniques are widely used in the manufacture of semiconductor devices. Susceptors for epitaxial growth are generally made of graphite coated with a 5iC (silicon kerf s+ite) film, and are also made of semiconductor wafers,
For example, the processed wafer 1 is placed in a recessed counterbore called a wafer pocket. When epitaxial growth is performed, an epitaxial layer grows on the silicon wafer, while a polysilicon film grows on the susceptor. If epitaxial growth is performed multiple times, the polysilicon film will accumulate and become thicker, causing adverse effects such as particles and crystal defects on the epitaxial layer. and remove it. FIG. 2 shows a cross section during conventional susceptor etching. 2 is a susceptor, 3 is a wafer pocket, and 5 is a polysilicon film grown on the susceptor.
発明が解決しようとする課題
しかしながら上記の従来の方法ではポリシリコン膜のな
いウェハポケット部3は直接高濃度の壇酸ガスに曝され
るため、S】C膜でコートされてはいるもののエツチン
グが進行して形状が変化するとともにピンホール等も発
生し、その後のエピタキシャル成長においてシリコンウ
ェハに熱歪による結晶欠陥の発生、汚染による比抵抗バ
ラツキの発生等の問題点があった。Problems to be Solved by the Invention However, in the above-mentioned conventional method, the wafer pocket 3 without the polysilicon film is directly exposed to the highly concentrated carbonic acid gas, so that although it is coated with the S]C film, etching is not possible. As the process progresses, pinholes and the like occur as the shape changes, and during subsequent epitaxial growth, there are problems such as crystal defects in the silicon wafer due to thermal strain and resistivity variations due to contamination.
本発明は上記従来の問題点を解決するものでウェハポケ
ットの形状を変化させない気相成長用サセプタのエツチ
ング方法を提供することを目的とするものである。SUMMARY OF THE INVENTION The present invention solves the above-mentioned conventional problems and aims to provide a method for etching a susceptor for vapor phase growth without changing the shape of a wafer pocket.
課題を解決するための手段
この目的を達成するために本発明の気相成長用サセプタ
のエツチング方法は、塩酸ガスでポリシリコン膜を除去
する際に、サセプタのウェハポケット部に薄板を載置す
る。Means for Solving the Problems To achieve this object, the method of etching a susceptor for vapor phase growth of the present invention includes placing a thin plate in the wafer pocket of the susceptor when removing a polysilicon film with hydrochloric acid gas. .
作用
サセプタのウェハポケット部は、薄板が入ることにより
直接塩酸ガスとは接触せずエツチングされない。The wafer pocket portion of the working susceptor does not come into direct contact with the hydrochloric acid gas and is not etched because the thin plate is inserted therein.
実施例 以下本発明の実施例を、図面を参照しながら説明する。Example Embodiments of the present invention will be described below with reference to the drawings.
第1図に本発明の一実施例における気相成長用サセプタ
のエツチング方法を示す。まず第1図fatに示すよう
に、ンリコンウエ/%lをサセプタ2のウェハポケット
部3に入れてエピタキシャル層4を成長させる。この場
合サセプタ2の上にはポリシリコン膜5が成長する。こ
のエピタキシャル成長を数回繰り返すと第1図fblに
示すようにポリシリコン膜5は積重なって厚くなる。次
にこの不要なポリシリコン膜5を高濃度の塩酸、ガスで
エツチングし除去する。この際、ウェハポケット部にシ
リコンウェハと同一形状のSiC製の薄板6を入れてお
く。このため、ウェハポケット部3は薄板6によって保
護され直接塩酸ガスとは接触せずエツチングされない。FIG. 1 shows a method of etching a susceptor for vapor phase growth in one embodiment of the present invention. First, as shown in FIG. 1, a silicon wafer/%l is placed in the wafer pocket 3 of the susceptor 2 and an epitaxial layer 4 is grown. In this case, a polysilicon film 5 is grown on the susceptor 2. When this epitaxial growth is repeated several times, the polysilicon film 5 is stacked and becomes thicker, as shown in FIG. 1fbl. Next, this unnecessary polysilicon film 5 is removed by etching with highly concentrated hydrochloric acid and gas. At this time, a thin SiC plate 6 having the same shape as the silicon wafer is placed in the wafer pocket. Therefore, the wafer pocket portion 3 is protected by the thin plate 6 and does not come into direct contact with the hydrochloric acid gas and is not etched.
したがってウエノ1ポケット部3は設計通りの形状がそ
のまま保たれ変化しないので安定した品質のエピタキシ
ャル層か再現性良く得られる。またピンホールの発生も
防止されるので汚染等の心配もなくサセプタ自体の寿命
も飛躍的に増大する。薄板6の材質はSiCが好ましく
、塩酸ガスに対する耐性も比較的あり、またSiC自体
が高純度のためSiCからの汚染の心配がない。Therefore, the Ueno 1 pocket portion 3 maintains its designed shape and does not change, so that an epitaxial layer of stable quality can be obtained with good reproducibility. Furthermore, since the generation of pinholes is prevented, there is no fear of contamination, and the life of the susceptor itself is dramatically increased. The material of the thin plate 6 is preferably SiC, which is relatively resistant to hydrochloric acid gas, and since SiC itself is highly pure, there is no fear of contamination from SiC.
なお、薄板として実施例ではSiCにより説明したが石
英板、高純度ンリコンウエハダミーを用いても本発明の
効果は維持し得る。Although SiC is used as the thin plate in the embodiment, the effects of the present invention can be maintained even if a quartz plate or a high-purity silicon wafer dummy is used.
また、実施例ではウェハポケットを有するサセプタにつ
いて説明したが、ウェハポケットのない平板型サセプタ
にも適用し得る。Further, in the embodiment, a susceptor having a wafer pocket has been described, but the present invention can also be applied to a flat plate type susceptor without a wafer pocket.
発明の効果
本発明の気相成長用サセプタのエツチング方法は、塩酸
ガスでポリシリコン膜を除去する際に、サセプタのウェ
ハポケット部に薄板を載置することによりウェハポケッ
ト部がエツチングされないため、品質の安定したエピタ
キシャル層か得られるとともに、サセプタの寿命をも増
大させると言う優れた効果が得られる。Effects of the Invention The method of etching a susceptor for vapor phase growth of the present invention prevents the wafer pocket from being etched by placing a thin plate on the wafer pocket of the susceptor when removing a polysilicon film with hydrochloric acid gas, thereby improving quality. Not only can a stable epitaxial layer be obtained, but also the excellent effect of increasing the life of the susceptor can be obtained.
第1図(al、 (blは本発明の実施例における気相
成長用サセプタのエツチング方法の断面図、第2図は従
来の気相成長用サセプタのエツチング方法の断面図であ
る。
1・・・・・・シリコンウェハ、2・・・・・・サセプ
タ、3・・・・・・ウェハポケット、4・・・・・・エ
ピタキシャル層、5・・・・・・ポリシリコン膜、6・
・・・・・薄板。FIG. 1 (al, (bl) is a sectional view of the etching method for a susceptor for vapor phase growth in an embodiment of the present invention, and FIG. 2 is a sectional view of a conventional etching method for a susceptor for vapor phase growth. 1. ... Silicon wafer, 2 ... Susceptor, 3 ... Wafer pocket, 4 ... Epitaxial layer, 5 ... Polysilicon film, 6.
...Thin plate.
Claims (2)
上に堆積したポリシリコン膜を塩酸ガスによって除去す
る際に、半導体ウェハ載置部分に前記半導体ウェハと同
一形状の薄板を載置することを特徴とする気相成長用サ
セプタのエッチング方法。(1) A vapor phase characterized in that when a polysilicon film deposited on a susceptor by a predetermined number of epitaxial growths is removed using hydrochloric acid gas, a thin plate having the same shape as the semiconductor wafer is placed on the semiconductor wafer placement area. Etching method for growth susceptor.
範囲第1項記載の気相成長用サセプタのエッチング方法
。(2) A method for etching a susceptor for vapor phase growth according to claim 1, wherein the thin plate is made of SiC.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP31906690A JPH04188720A (en) | 1990-11-21 | 1990-11-21 | Etching of vapor growth susceptor |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP31906690A JPH04188720A (en) | 1990-11-21 | 1990-11-21 | Etching of vapor growth susceptor |
Publications (1)
Publication Number | Publication Date |
---|---|
JPH04188720A true JPH04188720A (en) | 1992-07-07 |
Family
ID=18106120
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP31906690A Pending JPH04188720A (en) | 1990-11-21 | 1990-11-21 | Etching of vapor growth susceptor |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPH04188720A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2011159978A (en) * | 2010-02-03 | 2011-08-18 | Siltronic Ag | Method of manufacturing semiconductor wafer composed of silicon with epitaxially deposited layer |
JP4772918B1 (en) * | 2010-12-21 | 2011-09-14 | エー・イー・テック株式会社 | Method and apparatus for manufacturing gallium nitride (GaN) free-standing substrate |
JP2012131692A (en) * | 2011-04-28 | 2012-07-12 | Aetech Corp | METHOD AND APPARATUS FOR MANUFACTURING GALLIUM NITRIDE (GaN) SELF-SUPPORTING SUBSTRATE |
-
1990
- 1990-11-21 JP JP31906690A patent/JPH04188720A/en active Pending
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2011159978A (en) * | 2010-02-03 | 2011-08-18 | Siltronic Ag | Method of manufacturing semiconductor wafer composed of silicon with epitaxially deposited layer |
US9410265B2 (en) | 2010-02-03 | 2016-08-09 | Siltronic Ag | Method for producing a semiconductor wafer composed of silicon with an epitaxially deposited layer |
JP4772918B1 (en) * | 2010-12-21 | 2011-09-14 | エー・イー・テック株式会社 | Method and apparatus for manufacturing gallium nitride (GaN) free-standing substrate |
WO2012086212A1 (en) * | 2010-12-21 | 2012-06-28 | エー・イー・テック株式会社 | METHOD AND DEVICE FOR MANUFACTURING SELF-SUPPORTING GALLIUM NITRIDE (GaN) SUBSTRATE |
JP2012131662A (en) * | 2010-12-21 | 2012-07-12 | Aetech Corp | METHOD AND APPARATUS FOR MANUFACTURING GALLIUM NITRIDE (GaN) SELF-SUPPORTING SUBSTRATE |
KR101356381B1 (en) * | 2010-12-21 | 2014-01-27 | 에이.이. 테크 가부시키가이샤 | Method and apparatus for manufacturing gallium nitride free-standing substrate |
JP2012131692A (en) * | 2011-04-28 | 2012-07-12 | Aetech Corp | METHOD AND APPARATUS FOR MANUFACTURING GALLIUM NITRIDE (GaN) SELF-SUPPORTING SUBSTRATE |
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