JPH04169513A - Production of beautifying cosmetic utilizing ultra-fine powdery eggshell - Google Patents
Production of beautifying cosmetic utilizing ultra-fine powdery eggshellInfo
- Publication number
- JPH04169513A JPH04169513A JP29866590A JP29866590A JPH04169513A JP H04169513 A JPH04169513 A JP H04169513A JP 29866590 A JP29866590 A JP 29866590A JP 29866590 A JP29866590 A JP 29866590A JP H04169513 A JPH04169513 A JP H04169513A
- Authority
- JP
- Japan
- Prior art keywords
- eggshell
- amino acids
- cosmetic
- lactic acid
- ultra
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 210000003278 egg shell Anatomy 0.000 title claims abstract description 26
- 239000002537 cosmetic Substances 0.000 title claims abstract description 16
- 102000002322 Egg Proteins Human genes 0.000 title claims abstract description 15
- 108010000912 Egg Proteins Proteins 0.000 title claims abstract description 15
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000006071 cream Substances 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 12
- 239000004310 lactic acid Substances 0.000 claims abstract description 10
- 235000014655 lactic acid Nutrition 0.000 claims abstract description 10
- 230000003796 beauty Effects 0.000 claims description 10
- 150000001413 amino acids Chemical class 0.000 abstract description 12
- 102000008186 Collagen Human genes 0.000 abstract description 11
- 108010035532 Collagen Proteins 0.000 abstract description 11
- 229920001436 collagen Polymers 0.000 abstract description 11
- 239000012528 membrane Substances 0.000 abstract description 7
- 239000000126 substance Substances 0.000 abstract description 4
- 239000002699 waste material Substances 0.000 abstract description 2
- 239000000080 wetting agent Substances 0.000 abstract description 2
- 230000003213 activating effect Effects 0.000 abstract 1
- 238000007796 conventional method Methods 0.000 abstract 1
- 230000002500 effect on skin Effects 0.000 abstract 1
- 239000002304 perfume Substances 0.000 abstract 1
- 230000001172 regenerating effect Effects 0.000 abstract 1
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 9
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 229940057995 liquid paraffin Drugs 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 229920001214 Polysorbate 60 Polymers 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- QMMJWQMCMRUYTG-UHFFFAOYSA-N 1,2,4,5-tetrachloro-3-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=C(Cl)C(Cl)=CC(Cl)=C1Cl QMMJWQMCMRUYTG-UHFFFAOYSA-N 0.000 description 1
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- 235000021355 Stearic acid Nutrition 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000008278 cosmetic cream Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000000909 electrodialysis Methods 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000001815 facial effect Effects 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 239000010794 food waste Substances 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- -1 liquid paraffin Substances 0.000 description 1
- 230000007721 medicinal effect Effects 0.000 description 1
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 239000012744 reinforcing agent Substances 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 230000036560 skin regeneration Effects 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000003655 tactile properties Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
Description
【発明の詳細な説明】
「産業上の利用分野」
この発明は、超微粉末のエッグシェルを利用した素肌や
顔などの美容のための、エッグシェルを利用した美容化
粧料の製造法に関するものである。[Detailed Description of the Invention] "Industrial Application Field" This invention relates to a method for producing beauty cosmetics using eggshell for the beauty of bare skin, face, etc. using ultrafine eggshell powder. It is.
「従来の技術」
従来、エッグシェルは微粉末の状態で、直接力ルシュウ
ム強化原料として、主に食品添加剤あるいは付堝コラー
ゲン膜を抽出、溶解し、コラーゲン入りクリームとして
、また殻内の有機成分を電気透析などの方法でアミノ酸
の形で回収し、アミノ酸入りクリームなどとして利用さ
れている。``Conventional technology'' Traditionally, eggshells are in the form of a fine powder, and used as a raw material for directly reinforcing the lucium, mainly by extracting and dissolving the collagen membrane in a food additive or in a pot, and then producing a collagen-containing cream or using the organic components inside the shells. It is recovered in the form of amino acids using methods such as electrodialysis and used as amino acid-containing creams.
[発明が解決しようとする課題」
エッグシェルは、炭酸力ルシュウムの代用品として、微
粉末にしたものを直接力ルシュウム強化剤として用いら
れる場合、付着コラーゲン膜、含有アミノ酸の特性は生
かしきれていない。また付加価値を高めるために、これ
らを分離して利用するためには種々の化学的方法が必要
となり経済的に不利となる。[Problem to be solved by the invention] When eggshell is used as a substitute for rhusium carbonate, and when it is ground into fine powder and used directly as a reinforcing agent, the characteristics of the attached collagen membrane and the amino acids it contains cannot be fully utilized. . Moreover, in order to increase added value, various chemical methods are required to separate and utilize these, which is economically disadvantageous.
本発明は以上の欠点を解決し、エッグシェルのすべての
成分の特性をうまく利用した美容化粧料への製造に関す
るものである。The present invention solves the above-mentioned drawbacks and relates to the production of beauty cosmetics that take advantage of the properties of all the ingredients of eggshell.
「課題を解決するための手段」
超微粉末化(200メツシユ以下)されたエッグシェル
は、主成分であるアミノ酸を含む殻および付着コラーゲ
ン膜のいずれも、適当量の乳酸溶液を加えることによっ
て溶解し、常温でクリーム状の均一生成物となる。``Means for solving the problem'' Eggshells that have been made into ultrafine powder (200 mesh or less) can be dissolved by adding an appropriate amount of lactic acid solution to both the shell containing amino acids, which is the main component, and the attached collagen membrane. It becomes a creamy homogeneous product at room temperature.
エッグシェルは通常のボールミルなどの粉砕機を用いて
やや長時間、超微粉末化することで、エッグシェルのす
べてを無駄な(利用した高アミノ酸含有の美容化粧料が
得られる。By pulverizing eggshells into ultra-fine powder for a relatively long period of time using a grinder such as a regular ball mill, beauty cosmetics with a high amino acid content can be obtained by making use of all the eggshells.
美容化粧料としての付加価値を高めるためには、従来か
ら知られている、プロピレングリコールなどの湿潤剤、
流動パラフィンなどの油剤、香料などを添加することが
できる。以上の製造法からなる超微粉末エッグシェルを
利用した美容化粧料の製造法。In order to increase the added value of beauty cosmetics, it is necessary to use conventionally known humectants such as propylene glycol,
Oil agents such as liquid paraffin, fragrances, etc. can be added. A method for producing beauty cosmetics using ultrafine powdered eggshell, which consists of the above production method.
「作用」
200メツシュ以上程度の粒径のエッグシェルでは、付
着コラーゲン膜は乳酸に不溶性であるが、それ以下の超
微粉末にすると徐々に乳化しながら溶解してい(、これ
は超微粉末にするための摩擦効果の過程で、繊維状に成
長している高分子のコラーゲン膜が、機械的に切断され
比較的単繊維化されるためと考久られる。``Effect'' In eggshells with a particle size of about 200 mesh or more, the attached collagen membrane is insoluble in lactic acid, but when it is made into an ultrafine powder of less than 200 mesh, it gradually emulsifies and dissolves. It is thought that this is because the polymeric collagen film, which has grown into fibers, is mechanically cut and becomes relatively single fibers during the frictional process.
超微粉末エッグシェルを利用した美容化粧料は、殻内の
有機質として存在している、7%前後のアミノ酸および
コラーゲン膜の乳化、分解による3%前後のアミノ酸の
合計、10部程度の高い含有率をもち、これらの成分は
素肌の活性化や皮膚の再生効果を促す、また乳酸および
乳酸力ルシュウムは、ある種の菌に対して殺菌作用も認
められており、薬用効果も期待される。Beauty cosmetics using ultra-fine powdered eggshells have a high content of around 10 parts, a total of around 7% amino acids present as organic substances within the shells and around 3% amino acids resulting from emulsification and decomposition of the collagen membrane. These ingredients promote the activation of bare skin and skin regeneration effects.Also, lactic acid and lactic acid lucium have been shown to have bactericidal effects on certain types of bacteria, and are expected to have medicinal effects.
「実施例」 以下1本発明について説明する。"Example" One aspect of the present invention will be explained below.
第1工程 エッグシェルを水洗、乾燥後、ボールミルな
どを用いて200メツシユ以下の超微粉末粒子とする。1st Step: After washing the eggshell with water and drying, it is made into ultrafine powder particles of 200 mesh or less using a ball mill or the like.
内容積5dm”のミルに3.5Kgのエッグシェル原料
を入れ、1個当たり直径が2.5−3.5cm、重さ3
5−55gのボール35個を投入して、1分間に60回
転の速度で40時間程度以上粉砕すると、手の指でされ
っても抵抗がない粉状となり、はぼ粒径は200メツシ
ユ以下となる。Put 3.5kg of eggshell raw material into a mill with an internal volume of 5dm, and each eggshell has a diameter of 2.5-3.5cm and a weight of 3.
When 35 balls weighing 5-55g are put in and crushed at a speed of 60 revolutions per minute for about 40 hours, it becomes a powder that does not resist when crushed with fingers, and the grain size is less than 200 mesh. becomes.
第2工程 上記の超微粉末エッグシェルに常温で適当量
の乳酸と水を加え、泡が消失するまでよくかきまぜ、そ
の後40−50分程度放置して全体がクリーム状になり
始めたら再度かきまぜを行ない、均一な状態とする。標
準的な混合比率は以下の通り。2nd step Add appropriate amounts of lactic acid and water to the ultra-fine powdered eggshells above at room temperature, stir well until the bubbles disappear, then leave for about 40-50 minutes and stir again when the whole starts to become creamy. to make it uniform. The standard mixing ratio is as follows.
超微粉末エッグシェル 10部
乳酸 18部
純水 100部
第3工程 第2工程を経てクリーム状になりつつある溶
液をかきまぜながら、湿潤剤としてプロピレングリコー
ルなどの多価アルコール類、油剤として流動パラフィン
や高級脂肪酸、エステル類、中和剤として水酸化カリウ
ム、界面活性剤としてポリオキシエチレン(20)ソル
ビタンモノステアレート、その他、香料や防腐剤などを
配合する。標準的な混合比率は以下の通り。Ultrafine powdered eggshell 10 parts Lactic acid 18 parts Pure water 100 parts 3rd step While stirring the solution that is becoming creamy after the 2nd step, add polyhydric alcohols such as propylene glycol as a wetting agent and liquid paraffin or other oils as an oil agent. Higher fatty acids, esters, potassium hydroxide as a neutralizing agent, polyoxyethylene (20) sorbitan monostearate as a surfactant, and other ingredients such as fragrances and preservatives are blended. The standard mixing ratio is as follows.
プロピレングリコール 20部
流動パラフィン 20部
水酸化カリウム 0,2部
ポリオキシエチレン(20)
ソルビタンモノステアレート 3s
第4工程 第3工程を経たものに、通常の処方で調製さ
れるヴアニシングクリームを適当量加えることによって
、本美容化粧料の使用時の素肌へのなめらかさなどの感
触性を高め、また適度な流動性を確保することができる
。Propylene glycol 20 parts Liquid paraffin 20 parts Potassium hydroxide 0.2 parts Polyoxyethylene (20) Sorbitan monostearate 3s 4th step Add a suitable amount of vanishing cream prepared according to the usual recipe to the product that has gone through the 3rd step. By adding this amount, it is possible to enhance the tactile properties such as smoothness on the bare skin when using the present beauty cosmetic, and to ensure appropriate fluidity.
調製されるヴアニシングクリームの配合比率は以下の通
り。The blending ratio of the Vanishing Cream to be prepared is as follows.
ステアリン酸 8部
ステアリルアルコール 6部
ブチルステアレート 8部
グリセリンモノステアレート 2部
P−パラベン 0.5部
BHT O12部
以上の油層溶液に、
プロピレングリコール 10部
水酸化カリウム 0.2部
純水 90部
上記水層を、それぞれ75−90℃に加温した後、よく
かきまぜて乳化し、均一なりリーム状とする。Stearic acid 8 parts Stearyl alcohol 6 parts Butyl stearate 8 parts Glycerin monostearate 2 parts P-paraben 0.5 parts The aqueous layers are each heated to 75-90°C and then thoroughly stirred to emulsify and form a homogeneous cream.
第5工程 本発明化粧料を調製後、クリーム状となり始
めた時点で、ヴアニシングクリームを加えて、よくかき
まぜ均一な状態とする。標準的な混合比率は以下の通り
。Fifth step After preparing the cosmetic composition of the present invention, when it starts to become creamy, add vanishing cream and stir well to obtain a uniform state. The standard mixing ratio is as follows.
本発明化粧料 80−90部
ヴアニシングクリーム10−20部
「発明の効果」
エッグシェルは、養鶏団地の効率化により大量生産され
る。一方で、菓子製造業などの厨介物として大量に廃棄
されるが、その利用法は一部の大企業でわずかに実施さ
れているに留まっている。また、現在実施されている利
用法はエッグシェルの特性を十分生かし切っていないと
考えられる0本発明は、これらの廃棄物の特性をよく検
討したうえで、より有効な利用法として発明されたもの
である6通常の状態でエッグシェルを乳酸で溶解すると
、付着コラーゲン膜は不溶性のまま生成物中に分散され
、これらは化粧料クリームとして用いられる場合、いわ
ゆるスクラブ粒子として利用することができる。Cosmetic composition of the present invention: 80-90 parts Vanishing cream: 10-20 parts "Effects of the invention" Eggshells are mass-produced by increasing the efficiency of poultry farms. On the other hand, a large amount of food is discarded as food waste in the confectionery manufacturing industry, but its use is only being used by a few large companies. In addition, it is believed that the current usage method does not take full advantage of the characteristics of eggshells.The present invention was invented as a more effective method of using eggshells after careful consideration of the characteristics of these wastes. 6 When eggshells are dissolved in lactic acid under normal conditions, the attached collagen films remain insoluble and dispersed in the product, and these can be utilized as so-called scrub particles when used as cosmetic creams.
しかし、スクラブ洗顔剤では、素肌に塗って長時間保持
することは不溶性のスクラブ粒子の存在のため、外出な
どをするには日常的でなく、短時間内で、最終的には洗
顔によるクリームのはく離をしなければならない。とこ
ろが本発明の超微粉末エッグシェルを利用した美容化粧
料では、不溶性の付着コラーケン膜は乳化、溶解されて
おり、またアミノ酸の供給源ともなり、純粋なりリーム
として長時間素肌に塗ることができ、そのため豊富に含
有されているアミノ酸類の浸透が期待され、皮膚に対す
る活性あるいは再生効果が高い、特にナイトクリームな
どに適しているものと考えられる。However, with scrub facial cleansers, it is not possible to apply them to bare skin and keep them for a long time due to the presence of insoluble scrub particles, so it is not a daily practice for going out, etc. Must be peeled. However, in the beauty cosmetics using the ultrafine powdered eggshell of the present invention, the insoluble attached collagen film is emulsified and dissolved, and it also serves as a source of amino acids, so it can be applied to bare skin as a pure cream for a long time. Therefore, it is expected that the abundant amino acids contained therein will penetrate, and it is considered to have a high activity or regeneration effect on the skin, making it particularly suitable for night creams.
Claims (1)
させたものを、クリーム状にした超微粉末エッグシェル
を利用した美容化粧料の製造法1. A method for producing beauty cosmetics using ultrafine eggshell powder made by reacting ultrafine eggshell powder with an appropriate amount of lactic acid solution and making it into a cream.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP29866590A JPH0717486B2 (en) | 1990-10-29 | 1990-10-29 | Manufacturing method of beauty cosmetics using ultrafine powder egg shell |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP29866590A JPH0717486B2 (en) | 1990-10-29 | 1990-10-29 | Manufacturing method of beauty cosmetics using ultrafine powder egg shell |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH04169513A true JPH04169513A (en) | 1992-06-17 |
JPH0717486B2 JPH0717486B2 (en) | 1995-03-01 |
Family
ID=17862684
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP29866590A Expired - Fee Related JPH0717486B2 (en) | 1990-10-29 | 1990-10-29 | Manufacturing method of beauty cosmetics using ultrafine powder egg shell |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPH0717486B2 (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2001074491A2 (en) * | 2000-04-03 | 2001-10-11 | Joseph Herman Macneil | Eggshell waste processing method and device |
EP2774655A1 (en) | 2013-03-05 | 2014-09-10 | JAO beheer BV | Composition comprising chicken eggshell particles, preparation and use |
-
1990
- 1990-10-29 JP JP29866590A patent/JPH0717486B2/en not_active Expired - Fee Related
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2001074491A2 (en) * | 2000-04-03 | 2001-10-11 | Joseph Herman Macneil | Eggshell waste processing method and device |
WO2001074491A3 (en) * | 2000-04-03 | 2002-02-21 | Joseph Herman Macneil | Eggshell waste processing method and device |
US6899294B2 (en) | 2000-04-03 | 2005-05-31 | The Penn State Research Foundation | Hatchery eggshell waste processing method and device |
EP2774655A1 (en) | 2013-03-05 | 2014-09-10 | JAO beheer BV | Composition comprising chicken eggshell particles, preparation and use |
Also Published As
Publication number | Publication date |
---|---|
JPH0717486B2 (en) | 1995-03-01 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
LAPS | Cancellation because of no payment of annual fees |