JPH0319250B2 - - Google Patents
Info
- Publication number
- JPH0319250B2 JPH0319250B2 JP60026619A JP2661985A JPH0319250B2 JP H0319250 B2 JPH0319250 B2 JP H0319250B2 JP 60026619 A JP60026619 A JP 60026619A JP 2661985 A JP2661985 A JP 2661985A JP H0319250 B2 JPH0319250 B2 JP H0319250B2
- Authority
- JP
- Japan
- Prior art keywords
- mixture
- catalyst
- cyclopolysiloxane
- screw extruder
- chain terminator
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/06—Preparatory processes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Silicon Polymers (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US584060 | 1984-02-27 | ||
| US06/584,060 US4551515A (en) | 1984-02-27 | 1984-02-27 | Process for the continuous manufacture of silicone gums |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS60202124A JPS60202124A (ja) | 1985-10-12 |
| JPH0319250B2 true JPH0319250B2 (enExample) | 1991-03-14 |
Family
ID=24335766
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP60026619A Granted JPS60202124A (ja) | 1984-02-27 | 1985-02-15 | シリコーンガムの連続的製造方法 |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US4551515A (enExample) |
| JP (1) | JPS60202124A (enExample) |
| CA (1) | CA1240093A (enExample) |
| GB (1) | GB2154596A (enExample) |
Families Citing this family (34)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0610262B2 (ja) * | 1985-05-28 | 1994-02-09 | 東レ・ダウコーニング・シリコーン株式会社 | シリコ−ン重合体−充填剤混合物の製造方法 |
| DE3519411A1 (de) * | 1985-05-30 | 1986-12-04 | Wacker-Chemie GmbH, 8000 München | Kontinuierliches verfahren zur aenderung des molekulargewichts von organosiliciumverbindungen |
| US4701491A (en) * | 1986-10-27 | 1987-10-20 | Dow Corning Corporation | Silicone extrusion stock |
| US4719276A (en) * | 1986-10-27 | 1988-01-12 | Dow Corning Corporation | Neutralization of catalyst in polymerization of polydiorganosiloxane |
| US4780519A (en) * | 1986-10-27 | 1988-10-25 | Dow Corning Corporation | Method of producing polydiorganosiloxane gum |
| US4766192A (en) * | 1987-07-10 | 1988-08-23 | Dow Corning Corporation | Silicone polymer termination |
| US4766191A (en) * | 1987-07-10 | 1988-08-23 | Dow Corning Corporation | Silicone polymer termination |
| DE3914912A1 (de) * | 1989-05-05 | 1990-11-08 | Wacker Chemie Gmbh | Verfahren zur kontinuierlichen herstellung von hochmolekularen organosiliciumverbindungen |
| US5079291A (en) * | 1989-11-20 | 1992-01-07 | General Electric Company | Polar aprotic catalysts for formation of fluorosilicone fluids |
| DE4007312C2 (de) * | 1990-03-08 | 2000-04-27 | Basf Ag | Verfahren zur Herstellung von feinteiligen, wasserlöslichen, Vinylamin-Einheiten enthaltenden Polymerisaten |
| US5173558A (en) * | 1991-05-20 | 1992-12-22 | Dow Corning Corporation | Base catalyzed preparation of polyorganosiloxanes with controlled low levels of hydroxy substitution |
| EP0546747A1 (en) * | 1991-12-05 | 1993-06-16 | General Electric Company | Polymerisation process |
| US5481014A (en) * | 1995-05-08 | 1996-01-02 | Dow Corning Corporation | Silyl phosphonate as stabilizing agent for polydiorganosiloxanes |
| US5710300A (en) * | 1997-04-11 | 1998-01-20 | Dow Corning Corporation | Siloxy phosphonate as stabilizing agent for polydiorganosiloxanes |
| US6103847A (en) * | 1997-05-27 | 2000-08-15 | Witco Corporation | Siloxane-polyether copolymers with unsaturated functionalities, and process for making them |
| US6103839A (en) * | 1998-05-11 | 2000-08-15 | Nalco Chemical Company | Horizontally flowing continuous free radical polymerization process for manufacturing water-soluble polymers from monomers in aqueous solution |
| GB9818539D0 (en) * | 1998-08-26 | 1998-10-21 | Dow Corning | Process for producing a silicone polymer |
| GB9818541D0 (en) * | 1998-08-26 | 1998-10-21 | Dow Corning | Continuous process for producing a silicone polymer |
| GB9818543D0 (en) * | 1998-08-26 | 1998-10-21 | Dow Corning | Continuous process for producing a silicone polymer |
| JP3546728B2 (ja) | 1998-12-02 | 2004-07-28 | 信越化学工業株式会社 | オルガノポリシロキサンガムの連続製造方法 |
| TW500768B (en) * | 1998-12-02 | 2002-09-01 | Shinetsu Chemical Co | Preparation of organopolysiloxane gum |
| JP2004217850A (ja) * | 2003-01-17 | 2004-08-05 | Dow Corning Toray Silicone Co Ltd | オルガノポリシロキサン組成物および硬化性オルガノポリシロキサン組成物 |
| DE102004014218A1 (de) * | 2004-03-23 | 2005-10-13 | Wacker-Chemie Gmbh | Verfahren zur Herstellung von aminofunktionellen Organopolysiloxanen |
| CN100347264C (zh) * | 2005-12-05 | 2007-11-07 | 叶照光 | 一种硅酮密封结构胶全自动生产、灌装、分装方法 |
| JP5207627B2 (ja) * | 2006-12-27 | 2013-06-12 | 東レ・ダウコーニング株式会社 | オルガノポリシロキサンの熱安定性を改善する方法およびオルガノポリシロキサン混合物 |
| DE102007036069A1 (de) * | 2007-08-01 | 2009-02-05 | Wacker Chemie Ag | Mehrstufiges Verfahren zur Herstellung von Aminoalkylgruppen aufweisenden Organopolysiloxanen |
| CN102421828B (zh) | 2009-05-13 | 2014-12-10 | 陶氏康宁公司 | 聚合和乳化硅氧烷的连续法 |
| CN102070785A (zh) * | 2010-11-26 | 2011-05-25 | 杭州赛默科技有限公司 | 一种羟基封端聚甲基苯基硅氧烷的制备方法 |
| CN103459027A (zh) * | 2011-03-31 | 2013-12-18 | 道康宁公司 | 包含膦酸酯催化剂的组合物以及制备和使用组合物的方法 |
| CN102492145A (zh) * | 2011-12-07 | 2012-06-13 | 江苏宏达新材料股份有限公司 | 一种高分子量甲基苯基硅橡胶生胶的制备方法 |
| CN102924721B (zh) * | 2012-11-22 | 2013-12-25 | 深圳市森日有机硅材料有限公司 | 一种乙烯基硅油的连续化制备方法 |
| CN105111445A (zh) * | 2015-09-30 | 2015-12-02 | 桂林健评环保节能产品开发有限公司 | 一种led灌封胶用甲基苯基硅油及其制备方法 |
| JP2025516012A (ja) | 2022-05-09 | 2025-05-23 | ダウ シリコーンズ コーポレーション | シロキサンポリマーの重合 |
| CN115417991B (zh) * | 2022-09-06 | 2024-02-09 | 江西蓝星星火有机硅有限公司 | 连续生产有机聚硅氧烷的聚合-终止装置及方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2546036A (en) * | 1946-06-11 | 1951-03-20 | Gen Electric | Method of preparation of dimethyl silicone gums |
| US2634252A (en) * | 1949-05-25 | 1953-04-07 | Dow Corning | Method of polymerizing organosiloxanes with alkoxides and alcohol-hydroxide complexes |
| FR1583057A (enExample) * | 1967-05-09 | 1969-10-17 | ||
| US3433765A (en) * | 1967-08-07 | 1969-03-18 | Stauffer Chemical Co | Method for the production of silicone gums |
| US3803084A (en) * | 1968-03-23 | 1974-04-09 | Bayer Ag | Process for the production of high-polymer organo-siloxanes |
| GB1436883A (en) * | 1972-07-20 | 1976-05-26 | Gen Electric | Process for the production of silanol-stopped diorganopoly siloxanes |
| DE2705563C2 (de) * | 1977-02-10 | 1982-10-14 | Bayer Ag, 5090 Leverkusen | Verfahren zur kontinuierlichen Herstellung von hochviskosen Polydiorganosiloxanen |
| AU5900880A (en) * | 1979-06-18 | 1981-01-08 | General Electric Company | Continuous manufacture of siloxane polymers |
| JPS5626248A (en) * | 1979-08-10 | 1981-03-13 | Kawasaki Steel Corp | Observing device for x-ray kossel diffraction pattern |
| GB2052539B (en) * | 1980-06-03 | 1984-06-20 | Gen Electric | Process for the continuous manufacture of diorganopolysiloxane polymers |
-
1984
- 1984-02-27 US US06/584,060 patent/US4551515A/en not_active Expired - Lifetime
- 1984-10-17 GB GB08426177A patent/GB2154596A/en not_active Withdrawn
-
1985
- 1985-02-08 CA CA000473933A patent/CA1240093A/en not_active Expired
- 1985-02-15 JP JP60026619A patent/JPS60202124A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS60202124A (ja) | 1985-10-12 |
| CA1240093A (en) | 1988-08-02 |
| GB2154596A (en) | 1985-09-11 |
| GB8426177D0 (en) | 1984-11-21 |
| US4551515A (en) | 1985-11-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JPH0319250B2 (enExample) | ||
| DE69117094T2 (de) | Verfahren zur Herstellung von Kopolymeren mit Diphenyl- und Dimethylsiloxankettensegmenten | |
| KR840001490B1 (ko) | 실옥산 중합체의 연속 제조방법 | |
| US4486567A (en) | Method of polymerizing hydroxyl endblocked polydiorganosiloxane using quaternary ammonium carboxylate-carboxylic acid catalyst | |
| US4990555A (en) | Preparation of hydroxy terminated polysiloxanes | |
| US5109094A (en) | Process for the production of organosilicon compounds | |
| CA1108171A (en) | Process for the continuous preparation of polydiorganosiloxanes | |
| KR20000017556A (ko) | 실리콘 중합체의 연속 제조방법 | |
| KR100643547B1 (ko) | 실리콘 중합체의 연속 제조방법 | |
| US4722987A (en) | Method for the preparation of an organopolysiloxane | |
| US2834754A (en) | Process for removing volatile organopolysiloxanes from high molecular weight organopolysiloxanes by stripping gas and kneading | |
| US3153007A (en) | Process for making organopolysiloxanes using bromoalkane decatalyzing agents for excess alkali-metal catalysts | |
| CA1282521C (en) | Method for producing a silicone polymer-filler mixture | |
| JPS6317093B2 (enExample) | ||
| EP0266075B1 (en) | Neutralization of catalyst in polymerization of polydiorganosiloxane | |
| CA1305817C (en) | Silicone polymer termination | |
| US6492479B2 (en) | Process for producing fluorosilicon polymers | |
| US2469883A (en) | Preparation of methyl silicone elastomers | |
| US3803084A (en) | Process for the production of high-polymer organo-siloxanes | |
| JPH0474371B2 (enExample) | ||
| JP3546728B2 (ja) | オルガノポリシロキサンガムの連続製造方法 | |
| EP0314316B1 (en) | Preparation of modified polysiloxanes | |
| JPH062816B2 (ja) | 水酸基不含ポリジオルガノシロキサンの製法 | |
| JP2650593B2 (ja) | シロキサンガムの製造方法 | |
| JP3546727B2 (ja) | オルガノポリシロキサンガムの製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| R250 | Receipt of annual fees |
Free format text: JAPANESE INTERMEDIATE CODE: R250 |
|
| EXPY | Cancellation because of completion of term |