JPH03120353A - Surface coated super hard member for cutting or wear resistant tool - Google Patents

Surface coated super hard member for cutting or wear resistant tool

Info

Publication number
JPH03120353A
JPH03120353A JP1254492A JP25449289A JPH03120353A JP H03120353 A JPH03120353 A JP H03120353A JP 1254492 A JP1254492 A JP 1254492A JP 25449289 A JP25449289 A JP 25449289A JP H03120353 A JPH03120353 A JP H03120353A
Authority
JP
Japan
Prior art keywords
cutting
base material
layer
wear
resistance
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP1254492A
Other languages
Japanese (ja)
Other versions
JP2861113B2 (en
Inventor
Naoya Omori
直也 大森
Kazuo Yamagata
一夫 山縣
Toshio Nomura
俊雄 野村
Masaaki Tobioka
正明 飛岡
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Electric Industries Ltd
Original Assignee
Sumitomo Electric Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Electric Industries Ltd filed Critical Sumitomo Electric Industries Ltd
Priority to JP25449289A priority Critical patent/JP2861113B2/en
Priority to DE69008511T priority patent/DE69008511T2/en
Priority to US07/691,020 priority patent/US5266389A/en
Priority to EP90914429A priority patent/EP0446375B1/en
Priority to PCT/JP1990/001258 priority patent/WO1991005076A1/en
Publication of JPH03120353A publication Critical patent/JPH03120353A/en
Priority to KR9170538A priority patent/KR940002749B1/en
Application granted granted Critical
Publication of JP2861113B2 publication Critical patent/JP2861113B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Abstract

PURPOSE:To maintain the strength of a base material and to improve wear resistance at the time of high speed cutting by alternately forming a TiN layer and an AlN layer of respectively specified thicknesses on the surface of a base material into plural layers. CONSTITUTION:A TiN layer and an AlN layer having 0.01-0.2mum layer thickness, respectively, are alternately formed on the surface of a base material made of sintered hard alloy, etc., for cutting or wear resistant tool into >=10 layers by an ion plating method, etc. The thickness of the above coating layers as a whole is regulated to 0.5-8mum. This surface coated super hard member has superior wear resistance, deposition resistance, and breaking resistance and shows excellent machinability over a long period as a cutting tool or a wear resistant tool in high speed cutting as well as in low speed cutting.

Description

【発明の詳細な説明】 〔産業上の利用分野〕 本発明は、切削工具又は耐摩工具の表面に被覆層を設け
、耐摩耗性を改善向上させた切削・耐摩工具用表面被覆
超硬部材に関する。
Detailed Description of the Invention [Field of Industrial Application] The present invention relates to a surface-coated carbide member for cutting and wear-resistant tools, which has improved wear resistance by providing a coating layer on the surface of the cutting tool or wear-resistant tool. .

〔従来の技術〕[Conventional technology]

従来、切削工具や耐摩工具の材質は、炭化タングステン
(we )基等の超硬合金、炭化チタン(TiC)系等
の各種サーメット、高速度工具鋼等の鋼や硬質合金、炭
化珪素や窒化珪素等のセラミックスが主であった。
Conventionally, the materials used for cutting tools and wear-resistant tools include cemented carbide such as tungsten carbide (WE), various cermets such as titanium carbide (TiC), steel and hard alloys such as high-speed tool steel, silicon carbide and silicon nitride. The main products were ceramics such as

又、切削工具や耐摩工具の耐摩耗性を改善向上させるた
めに、その全表面又は切刃部分の表面上に、物理気相蒸
着法(PVD法)や化学気相蒸着法(cvn法)により
、チタン(Tt) 、ハフニウム(Hf)、ジルコニウ
ム(Zr)の炭化物、窒化物又は炭窒化物、若しくはア
ルミニウム(Aりの酸化物等を単層又は複層に形成した
表面被覆硬質部材が開発され、最近では広く実用に供さ
れている。特に、PVD法で形成した被覆層を有する切
削工具や耐摩工具は、母材強度の劣化なしに耐摩耗性を
向上できるため、ドリル、エンドミル、フライス切削用
スローアウェイチップ等の強度を要求される切削用途に
適している。
In addition, in order to improve the wear resistance of cutting tools and wear-resistant tools, the entire surface or the surface of the cutting edge is coated with physical vapor deposition (PVD) or chemical vapor deposition (CVN). , titanium (Tt), hafnium (Hf), zirconium (Zr) carbides, nitrides, or carbonitrides, or aluminum (A) oxides, etc., have been developed in a single or multilayer surface-coated hard member. In recent years, cutting tools and wear-resistant tools with a coating layer formed by the PVD method can improve wear resistance without degrading the strength of the base material, so they can be used for drilling, end mills, and milling. Suitable for cutting applications that require strength, such as indexable inserts.

しかし、PVD法が母材強度の劣化なしに被覆層を形成
できる点でcvn法より優れているとは云え、I’VD
法では母材上にAlの酸化物を安定して被覆することが
困難であるためA/酸化物の被覆層は実用化に至ってお
らず、現状のPVD法で形成できるT1、Hf5Zrの
炭化物、窒化物、炭窒化物等の被覆層では特に高速切削
での耐摩耗性が不足するため早期に寿命に至るものが多
かった。
However, although the PVD method is superior to the CVN method in that it can form a coating layer without deteriorating the strength of the base material, I'VD
Since it is difficult to stably coat the base material with Al oxide using the PVD method, the A/oxide coating layer has not been put into practical use. Coating layers made of nitrides, carbonitrides, etc. often reach the end of their service life early because of their lack of wear resistance, especially during high-speed cutting.

〔発明が解決しようとする課題〕[Problem to be solved by the invention]

本発明はかかる従来の事情に鑑み、切削工具や耐摩工具
の母材強度を維持し、同時に耐摩耗性に優れた被覆層を
設けることにより、特に高速切削において従来よりも耐
摩耗性が改善された切削・耐摩工具用表面被覆超硬部材
を提供することを目的とする。
In view of such conventional circumstances, the present invention maintains the strength of the base material of cutting tools and wear-resistant tools, and at the same time provides a coating layer with excellent wear resistance, thereby improving wear resistance compared to conventional ones, especially in high-speed cutting. The purpose of the present invention is to provide a surface-coated carbide member for cutting and wear-resistant tools.

〔課題を解決するための手段〕[Means to solve the problem]

上記目的を達成するため、本発明の切削・耐摩工具用表
面被覆超硬部材においては、切削工具又は耐摩工具から
なる母材の表面に、層厚0.01〜0.2μmのTIN
とAINを交互に10層以上積層して全体の層厚0.5
〜8μmの被覆層を設けたことを特徴とする。
In order to achieve the above object, in the surface-coated carbide member for cutting and wear-resistant tools of the present invention, a layer of TIN with a thickness of 0.01 to 0.2 μm is coated on the surface of the base material of the cutting tool or the wear-resistant tool.
Alternately stack 10 or more layers of AIN and AIN to create a total layer thickness of 0.5
It is characterized by providing a coating layer of ~8 μm.

尚、被覆層は切削工具又は耐摩工具の全表面に設けても
良いし、切刃部分の表面にのみ設けても良い。又、被覆
層の形成方法は従来公知の方法を利用できるが、スパッ
タリング法、イオンブレーティング法等のPVD法が母
材強度を容易に維持出来る点で好ましい。
The coating layer may be provided on the entire surface of the cutting tool or wear-resistant tool, or may be provided only on the surface of the cutting edge portion. Although conventionally known methods can be used to form the coating layer, PVD methods such as sputtering and ion blasting are preferred because the strength of the base material can be easily maintained.

〔作用〕[Effect]

本発明の表面被覆超硬部材は、切削工具又は耐摩工具と
して、低速切削は勿論高速切削においても耐摩耗性、耐
溶着性、耐欠損性に優れ、長期に亘って優れた切削性能
を示す。
As a cutting tool or a wear-resistant tool, the surface-coated carbide member of the present invention has excellent wear resistance, adhesion resistance, and chipping resistance not only in low-speed cutting but also in high-speed cutting, and exhibits excellent cutting performance over a long period of time.

その理由は、母材表面に薄いTiN層とAtN層を交互
に積層することにより、TiNが被覆層の硬度を高めな
がら母材との密着性を改善し、一方AINが被覆層の耐
欠損性を向上させ且っTiHの結晶粒を微細なものにす
るなど、各TiN層とAtN層が相乗的に作用すること
によって、全体として優れた耐摩耗性、耐溶着性及び耐
欠損性を兼ね備えた被覆層となるためと考えられる。
The reason for this is that by alternately laminating thin TiN and AtN layers on the surface of the base material, TiN increases the hardness of the coating layer and improves its adhesion to the base material, while AIN improves the fracture resistance of the coating layer. The TiN layer and the AtN layer work synergistically to improve the wear resistance and make the TiH crystal grains finer, resulting in excellent wear resistance, welding resistance, and chipping resistance as a whole. This is thought to be because it becomes a covering layer.

交互に積層されるTiN層とAtN層の層厚は薄いほど
好ましいが、通常の方法では0.01μmより薄く形成
することが難しく、又0,2μmを超えると各TiN層
とAtN層が厚くなりすぎ、上記した相互作用により全
体として優れた耐摩耗性、耐溶着性及び耐欠損性を兼ね
備えた被NNとすることが困難であるから、0.01〜
0.2μmの範囲とする。又、TiN層とAtN層の積
層数が10層未満でも、上記相互作用による全体として
優れた耐摩耗性、耐溶着性及び耐欠損性を兼ね備えた被
覆層が得られない。
The thinner the layer thicknesses of the TiN layers and AtN layers stacked alternately are, the better; however, it is difficult to form the layers thinner than 0.01 μm using normal methods, and if the thickness exceeds 0.2 μm, each TiN layer and AtN layer becomes thicker. 0.01 to
The range is 0.2 μm. Furthermore, even if the number of laminated TiN layers and AtN layers is less than 10, a coating layer having excellent wear resistance, adhesion resistance, and chipping resistance as a whole cannot be obtained due to the above-mentioned interaction.

被覆層全体の層厚を0.5〜8μmとするのは、0.5
μm未満では被覆層による耐摩耗性の向上が認められな
いためであり、8μmを超えると被覆層中の残留応力が
大きくなり母材との密着強度が低下するためである。
The thickness of the entire coating layer is 0.5 to 8 μm.
This is because if the thickness is less than 8 μm, no improvement in wear resistance is observed due to the coating layer, and if it exceeds 8 μm, the residual stress in the coating layer increases and the adhesion strength with the base material decreases.

〔実施例〕〔Example〕

母材として、組成が、TIS規格P30 (具体的には
WC−20wt%Tie−10wt%Co)、形状が同
SNG 432の超硬合金製切削チップを用意し、その
表面に下記の如く真空アーク放電を用いたイオンブレー
ティング法により、下記第2表に示す被覆層を形成して
本発明例の被覆切削チップ試料とした。
As a base material, a cemented carbide cutting tip with a composition of TIS standard P30 (specifically, WC-20wt%Tie-10wt%Co) and a shape of the same SNG432 was prepared, and its surface was heated with a vacuum arc as shown below. A coating layer shown in Table 2 below was formed by an ion blating method using electric discharge to obtain a coated cutting chip sample of an example of the present invention.

即ち、成膜装置内に、TiターゲットとAlターゲット
を対向させて配置し、両ターゲット間の中間点を中心と
して回転するリング状の母材保持治具の中心を通る直径
上の2点に、母材である上記切削チップを夫々装着した
。この状態で、切削チップを20 rpmで回転させな
がら、成膜装置内を真空度lXl0””torrのAr
ガス雰囲気に保ち、面切削チップに−2000Vの電圧
をかけて洗浄を行ない、500σまで加熱した後、Ar
ガスを排気した。その後、切削チップの回転を統けたま
ま成膜装置内にN ガスを300 cc/minの割合
で導入し、真空アーク放電によりT1ターゲットとAl
ターゲットを共に蒸発、イオン化させることにより、切
削チップがT1ターゲット近くを通過するときTiNを
及びAlターゲット近くを通過するときAINを夫々切
削チップ上に形成させるようにして、各切削チップ表面
にTiN層とAtN層を交互に積層した。尚、積層する
各TiN層とAtN層の層厚はアーク電流量を調整して
制御し、被覆層全体の層厚は成膜時間によって制御した
That is, a Ti target and an Al target are placed facing each other in a film forming apparatus, and two points on the diameter passing through the center of a ring-shaped base material holding jig that rotates around the midpoint between the two targets, The above-mentioned cutting tips, which were base materials, were respectively attached. In this state, while rotating the cutting tip at 20 rpm, the inside of the film forming apparatus was heated to an Ar gas with a vacuum level of 1X10""torr.
Maintaining the gas atmosphere, apply a voltage of -2000V to the surface cutting tip to clean it, heat it to 500σ, and then apply Ar
Exhausted the gas. After that, while controlling the rotation of the cutting tip, N gas was introduced into the film forming apparatus at a rate of 300 cc/min, and the T1 target and Al were heated by vacuum arc discharge.
By evaporating and ionizing the targets together, TiN is formed on the cutting tip when the cutting tip passes near the T1 target and AIN is formed on the cutting tip when passing near the Al target, so that a TiN layer is formed on the surface of each cutting tip. and AtN layers were alternately stacked. The layer thickness of each TiN layer and AtN layer to be laminated was controlled by adjusting the amount of arc current, and the layer thickness of the entire coating layer was controlled by the film formation time.

又、比較のために通常の成膜装置を使用して真空アーク
放電を用いたイオンブレーティング法により、上記と同
じ組成と形状の切削チップの表面上にTiC,TiN5
TiONを組合せてなる複層の被覆層を形成し、下記第
2表に示す従来例の被覆切削チップ試料を製造した。尚
、通常のCVD法により同じ組成と形状の切削チップの
表面上に下記第2表に示すTiC,At O等の被覆層
を形成した被覆切削チップ試料も用意した。
For comparison, TiC and TiN5 were deposited on the surface of a cutting tip with the same composition and shape as above using an ion blating method using vacuum arc discharge using an ordinary film forming apparatus.
A multi-layer coating layer was formed by combining TiON, and conventional coated cutting chip samples shown in Table 2 below were manufactured. A coated cutting chip sample was also prepared in which a coating layer of TiC, At 2 O, etc. shown in Table 2 below was formed on the surface of a cutting chip having the same composition and shape by a conventional CVD method.

得られた被覆層を有する各被覆切削チップ試料について
、下記第1表の条件による連続切削試験と断続切削試験
を行なって切刃の逃げ面摩耗幅を測定し、結果を第2表
に併せて表示した。
For each coated cutting chip sample having the obtained coating layer, a continuous cutting test and an intermittent cutting test were conducted under the conditions shown in Table 1 below to measure the flank wear width of the cutting edge, and the results are also shown in Table 2. displayed.

第  1  表 第 表 上記の結果から、本発明例の被覆切削チップ試料は、速
読切削及び断続切削の両方において、優れた耐摩耗性と
耐欠損性を兼ね備え、従来例のものよりも優れた切削性
能を示すことが判る。
From the above results in Table 1, it can be seen that the coated cutting tip sample of the present invention has excellent wear resistance and chipping resistance in both rapid cutting and interrupted cutting, and is superior to that of the conventional example. It can be seen that the cutting performance is shown.

〔発明の効果〕〔Effect of the invention〕

本発明によれば、低速切削は勿論高速切削においても優
れた耐摩耗性と耐欠損性を兼ね備え、長期に亘って優れ
た切削性能を持続しうる切削・耐摩工具用表面被覆超硬
部材を提供することが出来る0 1゜ 手 事件の表示 平成 年 統 特 補 許 正 書 願 (自発) 第254492号′ & 補正をする者 事件との関係
According to the present invention, there is provided a surface-coated carbide member for cutting and wear-resistant tools that has excellent wear resistance and chipping resistance not only in low-speed cutting but also in high-speed cutting, and can maintain excellent cutting performance over a long period of time. 0 1゜Indication of the case that can be made Heisei Unified Patent Amendment Application (Spontaneous) No. 254492'& Person making the amendment Relationship with the case

Claims (1)

【特許請求の範囲】[Claims] (1)切削工具又は耐摩工具からなる母材の表面に、層
厚0.01〜0.2μmのTiN層とAlN層を交互に
10層以上積層して全体の層厚0.5〜8μmの被覆層
を設けたことを特徴とする切削・耐摩工具用表面被覆超
硬部材。
(1) Ten or more TiN layers and AlN layers with a layer thickness of 0.01 to 0.2 μm are alternately laminated on the surface of a base material consisting of a cutting tool or a wear-resistant tool, so that the total layer thickness is 0.5 to 8 μm. A surface-coated carbide member for cutting and wear-resistant tools characterized by providing a coating layer.
JP25449289A 1989-09-29 1989-09-29 Surface-coated carbide members for cutting and wear-resistant tools Expired - Lifetime JP2861113B2 (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
JP25449289A JP2861113B2 (en) 1989-09-29 1989-09-29 Surface-coated carbide members for cutting and wear-resistant tools
DE69008511T DE69008511T2 (en) 1989-09-29 1990-09-28 SURFACE-COVERED HARD MATERIALS FOR CUTTING AND WEAR-RESISTANT TOOLS.
US07/691,020 US5266389A (en) 1989-09-29 1990-09-28 Surface-coated hard material for cutting tools or wear resistance tools
EP90914429A EP0446375B1 (en) 1989-09-29 1990-09-28 Surface-coated hard member for cutting and abrasion-resistant tools
PCT/JP1990/001258 WO1991005076A1 (en) 1989-09-29 1990-09-28 Surface-coated hard member for cutting and abrasion-resistant tools
KR9170538A KR940002749B1 (en) 1989-09-29 1991-05-29 Surface-coated hard member for cutting and abrasion-resistant tods

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP25449289A JP2861113B2 (en) 1989-09-29 1989-09-29 Surface-coated carbide members for cutting and wear-resistant tools

Publications (2)

Publication Number Publication Date
JPH03120353A true JPH03120353A (en) 1991-05-22
JP2861113B2 JP2861113B2 (en) 1999-02-24

Family

ID=17265808

Family Applications (1)

Application Number Title Priority Date Filing Date
JP25449289A Expired - Lifetime JP2861113B2 (en) 1989-09-29 1989-09-29 Surface-coated carbide members for cutting and wear-resistant tools

Country Status (1)

Country Link
JP (1) JP2861113B2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003061884A1 (en) * 2002-01-21 2003-07-31 Mitsubishi Materials Kobe Tools Corporation Surface coated cutting tool member having hard coating layer exhibiting excellent abrasion resistance in high-speed cutting, and method for forming said hard coating layer on surface of cutting tool

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005099945A1 (en) 2004-04-13 2005-10-27 Sumitomo Electric Hardmetal Corp. Surface-coated cutting tool

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003061884A1 (en) * 2002-01-21 2003-07-31 Mitsubishi Materials Kobe Tools Corporation Surface coated cutting tool member having hard coating layer exhibiting excellent abrasion resistance in high-speed cutting, and method for forming said hard coating layer on surface of cutting tool
US7094479B2 (en) 2002-01-21 2006-08-22 Mitsubishi Materials Kobe Tools Corporation Surface-coated cutting tool member having hard coating layer exhibiting superior wear resistance during high speed cutting operation and method for forming hard coating layer on surface of cutting tool

Also Published As

Publication number Publication date
JP2861113B2 (en) 1999-02-24

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