JPH029334B2 - - Google Patents
Info
- Publication number
- JPH029334B2 JPH029334B2 JP59127195A JP12719584A JPH029334B2 JP H029334 B2 JPH029334 B2 JP H029334B2 JP 59127195 A JP59127195 A JP 59127195A JP 12719584 A JP12719584 A JP 12719584A JP H029334 B2 JPH029334 B2 JP H029334B2
- Authority
- JP
- Japan
- Prior art keywords
- image
- receiving element
- parts
- weight
- manufactured
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000203 mixture Substances 0.000 claims description 14
- 150000001875 compounds Chemical class 0.000 claims description 2
- 230000005855 radiation Effects 0.000 claims 1
- 230000000052 comparative effect Effects 0.000 description 5
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- 239000010410 layer Substances 0.000 description 3
- SZCWBURCISJFEZ-UHFFFAOYSA-N (3-hydroxy-2,2-dimethylpropyl) 3-hydroxy-2,2-dimethylpropanoate Chemical compound OCC(C)(C)COC(=O)C(C)(C)CO SZCWBURCISJFEZ-UHFFFAOYSA-N 0.000 description 2
- ZDQNWDNMNKSMHI-UHFFFAOYSA-N 1-[2-(2-prop-2-enoyloxypropoxy)propoxy]propan-2-yl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COCC(C)OC(=O)C=C ZDQNWDNMNKSMHI-UHFFFAOYSA-N 0.000 description 2
- FIHBHSQYSYVZQE-UHFFFAOYSA-N 6-prop-2-enoyloxyhexyl prop-2-enoate Chemical compound C=CC(=O)OCCCCCCOC(=O)C=C FIHBHSQYSYVZQE-UHFFFAOYSA-N 0.000 description 2
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 231100000987 absorbed dose Toxicity 0.000 description 2
- 125000004386 diacrylate group Chemical group 0.000 description 2
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 description 2
- 239000000975 dye Substances 0.000 description 2
- 238000010894 electron beam technology Methods 0.000 description 2
- 229920000728 polyester Polymers 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 2
- 229940042596 viscoat Drugs 0.000 description 2
- PAPBSGBWRJIAAV-UHFFFAOYSA-N ε-Caprolactone Chemical compound O=C1CCCCCO1 PAPBSGBWRJIAAV-UHFFFAOYSA-N 0.000 description 2
- DMYOHQBLOZMDLP-UHFFFAOYSA-N 1-[2-(2-hydroxy-3-piperidin-1-ylpropoxy)phenyl]-3-phenylpropan-1-one Chemical compound C1CCCCN1CC(O)COC1=CC=CC=C1C(=O)CCC1=CC=CC=C1 DMYOHQBLOZMDLP-UHFFFAOYSA-N 0.000 description 1
- YNSNJGRCQCDRDM-UHFFFAOYSA-N 1-chlorothioxanthen-9-one Chemical compound S1C2=CC=CC=C2C(=O)C2=C1C=CC=C2Cl YNSNJGRCQCDRDM-UHFFFAOYSA-N 0.000 description 1
- OEPOKWHJYJXUGD-UHFFFAOYSA-N 2-(3-phenylmethoxyphenyl)-1,3-thiazole-4-carbaldehyde Chemical compound O=CC1=CSC(C=2C=C(OCC=3C=CC=CC=3)C=CC=2)=N1 OEPOKWHJYJXUGD-UHFFFAOYSA-N 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 229920001079 Thiokol (polymer) Polymers 0.000 description 1
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- WXNRYSGJLQFHBR-UHFFFAOYSA-N bis(2,4-dihydroxyphenyl)methanone Chemical group OC1=CC(O)=CC=C1C(=O)C1=CC=C(O)C=C1O WXNRYSGJLQFHBR-UHFFFAOYSA-N 0.000 description 1
- 239000011247 coating layer Substances 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000001678 irradiating effect Effects 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 description 1
- 229920005668 polycarbonate resin Polymers 0.000 description 1
- 239000004431 polycarbonate resin Substances 0.000 description 1
- -1 polyethylene Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/50—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording
- B41M5/52—Macromolecular coatings
- B41M5/5254—Macromolecular coatings characterised by the use of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds, e.g. vinyl polymers
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Thermal Transfer Or Thermal Recording In General (AREA)
Description
ヒドロキシピバリン酸ネオペンチルグリコール／
カプロラクトン／ジアクリレート（日本化薬社製
HX−620） 100重量部
〔組成物２〕
ポリエステルアクリレート（大阪有機化学工業社
製 ビスコート3700） 60重量部
１，６−ヘキサンジオールジアクリレート
10重量部
トリプロピレングリコールジアクリレート
30重量部
〔組成物３〕
アクリル変性ポリウレタン（チオコール社製
UVITHAN783） 20重量部
ヒドロキシピバリン酸ネオペンチルグリコール／
カプロラクトン／ジアクリレート（日本化薬社製
HX−620） 60重量部
トリメチロールプロパントリアクリレート
10重量部
アセトン 10重量部
〔組成物４〕
ポリエステルアクリレート（大坂有機化学工業社
製 ビスコート3700） 56重量部
トリプロピレングリコールジアクリレート
30重量部
１，６−ヘキサンジオールジアクリレート
10重量部
ベンゾフエノン ２重量部
１−クロロチオキサントン ２重量部
上記組成物１〜３は、乾燥膜厚が20μｍとなる
よう写真用パライタ紙上に塗設し、200KVの加
速電圧で6Mradの吸収線量となるよう電子線を
照射して塗設層を硬化した。
上記組成物４は、乾燥膜厚が10μｍとなるよう
写真用パライタ紙上に塗設し、出力800W／cmの
高圧水銀ランプを用い、ランプ下10cmの距離にお
いて２秒間紫外線を照射して塗設層を硬化した。
上記各組成物１〜４から得られた受像要素の試
料No.をそれぞれ１、２、３、４とする。
また、比較用の受像要素として、以下に示す比
較組成物１〜３を写真用パライタ紙上に乾燥膜厚
が20μｍとなるように塗布し、乾燥した。比較組
成粉１〜３から得られた受像要素の試験No.をそれ
ぞれ比較１、２、３とする。
〔比較組成物１〕
ポリ塩化ビニル（和光純薬社製） 10ｇ
テトラヒドロフラン 100ml
〔比較組成物２〕
サランＬ−501（塩化ビニリデン、旭ダウケミカル
社製） 10ｇ
テトラヒドロフラン 100ml
〔比較組成物３〕
ポリカーボネートレジン（パンライト、帝人社
製） 10ml
塩化メチレン 100ml
ジブチルフタレート 1.0ｇ
前記露光済の試料と受像要素を重ねて、表面温
度が150℃の電気アイロン型ヒートブロツクで30
秒間圧着加熱を行なつた後、すみやかにひきはが
した。
受像要素表面に得られたステツプウエツジ像の
642nｍにおける最大反射濃度、最小反射濃度
（カブリ）、および、各々画像が転写されていない
同じ受像要素を面々接触させて、55℃、相対湿度
30％〜40％の雰囲気下に放置した時、再転写した
画像の最大反射濃度、さらに熱転写処理後の受像
要素の表面光沢を測定、観察した。結果を表−１
に示す。
Neopentyl glycol hydroxypivalate/
Caprolactone/diacrylate (manufactured by Nippon Kayaku Co., Ltd.)
HX-620) 100 parts by weight [Composition 2] Polyester acrylate (Viscoat 3700, Osaka Organic Chemical Industry Co., Ltd.) 60 parts by weight 1,6-hexanediol diacrylate
10 parts by weight tripropylene glycol diacrylate
30 parts by weight [Composition 3] Acrylic modified polyurethane (manufactured by Thiokol)
UVITHAN783) 20 parts by weight Neopentyl glycol hydroxypivalate/
Caprolactone/diacrylate (manufactured by Nippon Kayaku Co., Ltd.)
HX-620) 60 parts by weight trimethylolpropane triacrylate
10 parts by weight Acetone 10 parts by weight [Composition 4] Polyester acrylate (Viscoat 3700 manufactured by Osaka Organic Chemical Industry Co., Ltd.) 56 parts by weight Tripropylene glycol diacrylate
30 parts by weight 1,6-hexanediol diacrylate
10 parts by weight 2 parts by weight of benzophenone 2 parts by weight of 1-chlorothioxanthone The above compositions 1 to 3 were coated on photographic parametric paper so that the dry film thickness was 20 μm, and the absorbed dose was 6 Mrad at an accelerating voltage of 200 KV. The coating layer was cured by irradiation with an electron beam. The above composition 4 was coated on photographic Paraita paper so that the dry film thickness was 10 μm, and the coated layer was irradiated with ultraviolet rays for 2 seconds at a distance of 10 cm below the lamp using a high-pressure mercury lamp with an output of 800 W/cm. hardened. The sample numbers of the image receiving elements obtained from each of the above compositions 1 to 4 are designated as 1, 2, 3, and 4, respectively. Further, as image-receiving elements for comparison, Comparative Compositions 1 to 3 shown below were coated on photographic Paraita paper to a dry film thickness of 20 μm and dried. The test numbers of the image receiving elements obtained from Comparative Composition Powders 1 to 3 are referred to as Comparisons 1, 2, and 3, respectively. [Comparative composition 1] Polyvinyl chloride (manufactured by Wako Pure Chemical Industries, Ltd.) 10 g Tetrahydrofuran 100 ml [Comparative composition 2] Saran L-501 (vinylidene chloride, manufactured by Asahi Dow Chemical Company) 10 g Tetrahydrofuran 100 ml [Comparative composition 3] Polycarbonate resin (Panlight, manufactured by Teijin) 10 ml Methylene chloride 100 ml Dibutyl phthalate 1.0 g The exposed sample and image receiving element were stacked and heated for 30 minutes using an electric iron type heat block with a surface temperature of 150°C.
After applying pressure and heating for a second, it was immediately peeled off. of the step wedge image obtained on the surface of the image receiving element.
The maximum reflection density at 642 nm, the minimum reflection density (fog), and the same image-receiving elements on which no images have been transferred are brought into contact face-to-face at 55°C and relative humidity.
When left in an atmosphere of 30% to 40%, the maximum reflection density of the retransferred image and the surface gloss of the image receiving element after thermal transfer processing were measured and observed. Table 1 shows the results.
Shown below.
【表】【table】
【表】
表面光沢については、未処理の受像要素と同程
度の光沢を維持しているものを○、表面光沢が感
光要素と受像要素を加熱圧着することによりかな
り失なわれているものを△、全面的に失なわれて
いるものを×とした。
上記表−１からも明らかなように、本発明の受
像要素を用いた場合には、カブリが抑制され、良
好な転写色素の最大濃度を示すと同時に再転写性
が改良されて再転写の発生が認められず、また、
処理後も、表面光沢の失われることのない優れた
受像要素であることがわかる。
実施例 ２
本実施例では実施例１において用いられたＸ−
１の代りに下記化合物Ｘ−２、Ｘ−３ならびにＸ
−４をそれぞれ用いた以外は実施例１と全く同様
にして試料を作成し、実施例１と同じ方法で処理
して受像要素の再転写性を試験したが、実施例１
で得られた結果と全く同様に本発明の試料では、
全く再転写の発生は認められなかつた。
実施例 ３
感熱転写要素として以下のものを作製した。２
ｇ／m2のゼラチン下引を有する厚さ20μｍの透明
ポリエチレンチレフタレートフイルム上に、1.46
ｇ／m2の水溶性ポリビニルブチラール（エスレツ
クスＷ−201、積水化学社製）を含む層を設けて、
該層中に、それぞれアルミナボールミルにより分
散された下記色素(A)を、2.0×10-3mol／m2含有さ
せた。
一方、感熱転写用受線要素として、アート紙
（試料−１）、アート紙表面に実施例−１の組成物
３を２ｇ／m2塗設し、200KVの加速電圧で
6Mradの吸収線量となるよう電子線照射して硬
化したもの（試料２）を作製した。
前記、感熱転写要素と、感熱転写用受像要素と
をそれぞれ重ね合わせ、感熱転写要素側から、サ
ーマルヘツドにて、印加電力を0.8W／dotで一定
とし、パルス幅を５ｍＳから40ｍＳまで段階的に
印加すると、受像要素表面には、マゼンタのステ
ツプウエツジ像が得られた。
再転写試験として試料１、２の表面にそれぞれ
アイボリー紙を重ね、500ｇ／ｄm2の圧力を与え
て40℃、相対湿度60％の雰囲気に40日間放置し
た。
熱転写した時に、受像要素表面に得られた最大
反射濃度、および再転写試験によつてアイボリー
紙表面に再転写して得られた最大反射濃度を表−
２に示す。[Table] Regarding surface gloss, those that maintain the same level of gloss as untreated image-receiving elements are ○, and those whose surface gloss has been significantly lost by heat-pressing the photosensitive element and image-receiving element are △. , Items that have been completely lost are marked as ×. As is clear from Table 1 above, when the image-receiving element of the present invention is used, fogging is suppressed and a good maximum density of transferred dye is exhibited, while at the same time retransferability is improved and retransfer does not occur. is not recognized, and
It can be seen that this is an excellent image-receiving element that does not lose its surface gloss even after processing. Example 2 In this example, the X-
In place of 1, the following compounds X-2, X-3 and X
Samples were prepared in exactly the same manner as in Example 1 except that -4 was used, and were processed in the same manner as in Example 1 to test the retransferability of the image-receiving element.
In the sample of the present invention, exactly similar to the results obtained in
No retranscription was observed at all. Example 3 The following thermal transfer elements were produced. 2
1.46 g/m 2 on a 20 μm thick transparent polyethylene tyrephthalate film with gelatin subbing.
A layer containing g/m 2 of water-soluble polyvinyl butyral (ESLEX W-201, manufactured by Sekisui Chemical Co., Ltd.) was provided,
The following dyes (A) each dispersed by an alumina ball mill were contained in the layer at 2.0×10 −3 mol/m 2 . On the other hand, as a wire-receiving element for thermal transfer, art paper (sample-1) was coated with 2 g/m 2 of composition 3 of Example-1 on the surface of the art paper, and was applied at an accelerating voltage of 200 KV.
A cured product (Sample 2) was prepared by irradiating it with an electron beam so that the absorbed dose was 6 Mrad. The heat-sensitive transfer element and the image-receiving element for heat-sensitive transfer are superimposed on each other, and from the heat-sensitive transfer element side, the applied power is kept constant at 0.8 W/dot, and the pulse width is stepped from 5 mS to 40 mS. When applied, a magenta step wedge image was obtained on the surface of the image receiving element. As a retransfer test, ivory paper was layered on the surface of Samples 1 and 2, and a pressure of 500 g/dm 2 was applied, and the samples were left in an atmosphere of 40° C. and 60% relative humidity for 40 days. The table shows the maximum reflection density obtained on the surface of the image receiving element when thermally transferred, and the maximum reflection density obtained when retransferred to the ivory paper surface in the retransfer test.
Shown in 2.
【表】
表−２から明らかなように、本発明の受像要素
（試料２）は、感熱転写用受像要素としても高い
最大濃度を得ることができ、かつ、再転写を生じ
ない優れたものであることがわかる。[Table] As is clear from Table 2, the image-receiving element of the present invention (sample 2) is an excellent image-receiving element for thermal transfer that can obtain a high maximum density and does not cause re-transfer. I understand that there is something.
Claims (1)
化層を有する受像要素であつて、該硬化層が分子
内にＣ＝Ｃ不飽和二重結合を有する重合性化合物
を含有する組成物より形成されることを特徴とす
る受像要素。1 An image receiving element having a cured layer cured by radiation irradiation on a support, the cured layer being formed from a composition containing a polymerizable compound having a C═C unsaturated double bond in the molecule. An image receiving element characterized by:
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59127195A JPS616649A (en) | 1984-06-20 | 1984-06-20 | Image receiving element |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59127195A JPS616649A (en) | 1984-06-20 | 1984-06-20 | Image receiving element |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP3041009A Division JPH07102745B2 (en) | 1991-02-12 | 1991-02-12 | Image forming method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS616649A JPS616649A (en) | 1986-01-13 |
| JPH029334B2 true JPH029334B2 (en) | 1990-03-01 |
Family
ID=14954045
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP59127195A Granted JPS616649A (en) | 1984-06-20 | 1984-06-20 | Image receiving element |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS616649A (en) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61112693A (en) * | 1984-11-07 | 1986-05-30 | Matsushita Electric Ind Co Ltd | Image receiving body for thermal transfer recording |
| JPS61211092A (en) * | 1985-03-15 | 1986-09-19 | Matsushita Electric Ind Co Ltd | Image-receiving material for transfer-type thermal recording |
| JPS6244495A (en) * | 1985-08-23 | 1987-02-26 | Mitsubishi Rayon Co Ltd | Coating composition for recording body of sublimable thermal transfer recording system |
| JPH062432B2 (en) * | 1985-08-26 | 1994-01-12 | 三菱レイヨン株式会社 | Sublimation type disperse dye thermal transfer recording type recording medium and method for producing the same |
| JPH0684054B2 (en) * | 1986-07-18 | 1994-10-26 | 大日本印刷株式会社 | Microporous sheet |
| JP2625418B2 (en) * | 1986-09-10 | 1997-07-02 | 松下電器産業株式会社 | Sublimation type thermal transfer recording system |
| JP2641196B2 (en) * | 1986-09-18 | 1997-08-13 | 松下電器産業株式会社 | Sublimation type thermal transfer recording system |
| JP2641197B2 (en) * | 1986-09-18 | 1997-08-13 | 松下電器産業株式会社 | Sublimation type thermal transfer recording system |
| JP2542499B2 (en) * | 1986-10-13 | 1996-10-09 | タイホ−工業株式会社 | OHP sheet for thermal transfer |
| JP2542506B2 (en) * | 1987-01-09 | 1996-10-09 | タイホ−工業株式会社 | OHP sheet for thermal transfer |
| JPS6442284A (en) * | 1987-08-11 | 1989-02-14 | Mitsubishi Rayon Co | Recording material for sublimation-type thermal transfer recording system |
| JP2587466B2 (en) * | 1988-08-02 | 1997-03-05 | コニカ株式会社 | Thermal transfer recording material |
| JP4396443B2 (en) | 2004-08-18 | 2010-01-13 | コニカミノルタエムジー株式会社 | Method for producing and using photosensitive lithographic printing plate |
| US20090110832A1 (en) | 2005-11-01 | 2009-04-30 | Konica Minolta Medical & Graphic, Inc. | Planographic printing plate material, planographic printing plate, planographic printing plate preparing process and printing process employing planographic printing plate |
-
1984
- 1984-06-20 JP JP59127195A patent/JPS616649A/en active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS616649A (en) | 1986-01-13 |
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