JPH0260307B2 - - Google Patents
Info
- Publication number
- JPH0260307B2 JPH0260307B2 JP58028301A JP2830183A JPH0260307B2 JP H0260307 B2 JPH0260307 B2 JP H0260307B2 JP 58028301 A JP58028301 A JP 58028301A JP 2830183 A JP2830183 A JP 2830183A JP H0260307 B2 JPH0260307 B2 JP H0260307B2
- Authority
- JP
- Japan
- Prior art keywords
- fruit juice
- drinks
- odor
- beverage
- present
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 235000015203 fruit juice Nutrition 0.000 claims description 35
- 238000004519 manufacturing process Methods 0.000 claims description 15
- 235000013361 beverage Nutrition 0.000 claims description 13
- AHRFRRASJMTTQU-UHFFFAOYSA-N 6-methyl-2,2-dioxooxathiazin-4-one;potassium Chemical compound [K].CC1=CC(=O)NS(=O)(=O)O1 AHRFRRASJMTTQU-UHFFFAOYSA-N 0.000 claims description 2
- 235000019645 odor Nutrition 0.000 description 14
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 12
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 11
- WBZFUFAFFUEMEI-UHFFFAOYSA-M Acesulfame k Chemical compound [K+].CC1=CC(=O)[N-]S(=O)(=O)O1 WBZFUFAFFUEMEI-UHFFFAOYSA-M 0.000 description 10
- 239000000619 acesulfame-K Substances 0.000 description 9
- 239000000796 flavoring agent Substances 0.000 description 9
- 235000019634 flavors Nutrition 0.000 description 8
- 235000003599 food sweetener Nutrition 0.000 description 7
- 235000000346 sugar Nutrition 0.000 description 7
- 239000003765 sweetening agent Substances 0.000 description 7
- 241001672694 Citrus reticulata Species 0.000 description 5
- 238000007796 conventional method Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 4
- 229930003268 Vitamin C Natural products 0.000 description 4
- 230000032683 aging Effects 0.000 description 4
- 235000019658 bitter taste Nutrition 0.000 description 4
- 235000015165 citric acid Nutrition 0.000 description 4
- 235000013399 edible fruits Nutrition 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- 235000019154 vitamin C Nutrition 0.000 description 4
- 239000011718 vitamin C Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 241000220225 Malus Species 0.000 description 3
- 235000020971 citrus fruits Nutrition 0.000 description 3
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 description 2
- 239000005715 Fructose Substances 0.000 description 2
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- 244000061456 Solanum tuberosum Species 0.000 description 2
- 235000002595 Solanum tuberosum Nutrition 0.000 description 2
- 241000219094 Vitaceae Species 0.000 description 2
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 2
- 235000015197 apple juice Nutrition 0.000 description 2
- 235000021016 apples Nutrition 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- -1 etc.) Natural products 0.000 description 2
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 2
- 239000008103 glucose Substances 0.000 description 2
- 235000019674 grape juice Nutrition 0.000 description 2
- 235000021021 grapes Nutrition 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 239000001630 malic acid Substances 0.000 description 2
- 235000011090 malic acid Nutrition 0.000 description 2
- 235000015205 orange juice Nutrition 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 235000014214 soft drink Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 235000019640 taste Nutrition 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- HMUNWXXNJPVALC-UHFFFAOYSA-N 1-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperazin-1-yl]-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)N1CCN(CC1)C(CN1CC2=C(CC1)NN=N2)=O HMUNWXXNJPVALC-UHFFFAOYSA-N 0.000 description 1
- XLXCHZCQTCBUOX-UHFFFAOYSA-N 1-prop-2-enylimidazole Chemical compound C=CCN1C=CN=C1 XLXCHZCQTCBUOX-UHFFFAOYSA-N 0.000 description 1
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 1
- 244000144730 Amygdalus persica Species 0.000 description 1
- 244000099147 Ananas comosus Species 0.000 description 1
- 235000007119 Ananas comosus Nutrition 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 235000005976 Citrus sinensis Nutrition 0.000 description 1
- 240000002319 Citrus sinensis Species 0.000 description 1
- 241000555678 Citrus unshiu Species 0.000 description 1
- 240000000560 Citrus x paradisi Species 0.000 description 1
- CIWBSHSKHKDKBQ-DUZGATOHSA-N D-araboascorbic acid Natural products OC[C@@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-DUZGATOHSA-N 0.000 description 1
- 229930091371 Fructose Natural products 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 240000008790 Musa x paradisiaca Species 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 235000006040 Prunus persica var persica Nutrition 0.000 description 1
- 241000220324 Pyrus Species 0.000 description 1
- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
- 235000014787 Vitis vinifera Nutrition 0.000 description 1
- VLSOAXRVHARBEQ-UHFFFAOYSA-N [4-fluoro-2-(hydroxymethyl)phenyl]methanol Chemical compound OCC1=CC=C(F)C=C1CO VLSOAXRVHARBEQ-UHFFFAOYSA-N 0.000 description 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
- 229940024606 amino acid Drugs 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 235000010323 ascorbic acid Nutrition 0.000 description 1
- 239000011668 ascorbic acid Substances 0.000 description 1
- 229960005070 ascorbic acid Drugs 0.000 description 1
- 235000021015 bananas Nutrition 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 235000010350 erythorbic acid Nutrition 0.000 description 1
- 239000004318 erythorbic acid Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 239000001530 fumaric acid Substances 0.000 description 1
- 235000011087 fumaric acid Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229940026239 isoascorbic acid Drugs 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- XIMSTDAFGWROBF-UHFFFAOYSA-N oxathiazine 2-oxide Chemical class O=S1OC=CC=N1 XIMSTDAFGWROBF-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 235000019629 palatability Nutrition 0.000 description 1
- 235000021017 pears Nutrition 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical class [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 1
- 235000020357 syrup Nutrition 0.000 description 1
- 239000006188 syrup Substances 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 239000011716 vitamin B2 Substances 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Landscapes
- Non-Alcoholic Beverages (AREA)
Description
本発明は果汁飲料の製造法に関する。
果汁飲料は、現代の嗜好にマツチした飲料とし
て広く行きわたつており、果汁の種類もミカン等
の柑橘類をはじめとしてブドウ、リンゴなど多く
のものが使われている。また製品の包装もビン
詰、缶詰、カートンボツクス入りなど多彩であ
る。
果汁飲料は製造直後における風味は良くても、
徐々に日向臭とか枯草臭とかイモ臭などいわれる
経日臭が生成して来る欠点をもつている。このよ
うな経日臭は、果汁に由来する油脂の酸化や製品
中の糖類とアミノ酸類による褐変などが原因とな
ると云われているが、まだ解明されるにいたつて
いない。従来、経日臭の防止のために、原料の果
汁には亜硫酸塩やL−システイン塩酸塩が、また
果汁飲料の製造に際してはビタミンC、エリソル
ビン酸、重合リン酸塩などが使われているが、効
果が不充分であつたりして満足されていない。
本発明者は、嗜好性の高く、経日臭の生成しな
い果汁飲料の製造法につき種々検討していたとこ
ろ、ある種のオキサチアジノン誘導体を特定濃度
で添加すると、得られた製品は長期間保存しても
経日臭の生成がなく、きわめて嗜好性が高いこと
を見出し、さらに検討して本発明を完成した。
すなわち、本発明は果汁飲料の製造に際し、該
飲料に対し約0.0006〜0.006重量%の6−メチル
−3,4−ジヒドロ−1,2,3−オキサチアジ
ン−4−オン−2,2−ジオキシド−カリウムを
添加することを特徴とする果汁飲料の製造法であ
る。
本発明において用いる6−メチル−3,4−ジ
ヒドロ−1,2,3−オキサチアジン−4−オン
−2,2−ジオキシド−カリウムは公知の甘味料
物質であつて、たとえば特開昭51−34182号に記
載の製造法によつて得られるものである。本願明
細書では、以下の記載において、上記甘味物質を
「アセスルフアムK」と称する。
次に、本発明でいう果汁飲料とは、果実をしぼ
つた汁液、あるいはこれを原料とし適宜に加工し
て得られる飲料を対象とする。すなわち、温州ミ
カン、バレンシアオレンジ、夏ミカン、グレープ
フレーツなどの柑橘類、ブドウ、リンゴ、パイン
アツプル、モモ、洋ナシ、バナナなどの果実を常
法により搾汁したもの、これを原果汁とする稀釈
果汁あるいは濃縮果汁が挙げられる。とりわけ、
柑橘類を原料とする果汁飲料に対し好ましく適用
される。果汁含量は、通常の果汁飲料に含まれる
範囲であれば全て対象とすることができ、たとえ
ば原果汁を100%であらわした場合、約5〜600%
の果汁含量のものである。果汁飲料には、甘味料
(例、砂糖、異性化糖、ぶどう糖、果糖など)、酸
味料(例、クエン酸、フマル酸、リンゴ酸、乳酸
など)、ビタミン類(例、ビタミンC、ビタミン
B1、ビタミンB2など)、着色料、着香料などを、
果汁飲料の種類により必要に応じて含有するもの
であつてもよく、さらに砂のう、パルプ質を適量
に含有するタイプであつてもよい。
本発明の製造法において、アセスルフアムKは
果汁飲料中に約0.0006〜0.006重量%となるよう
に含有せしめられる。この添加量よりも少ないと
きには、本発明の目的とする果汁飲料の経日臭の
生成を防止する効果が顕著ではなく、また上記の
範囲を越えて添加すると苦味が感ぜられて好まし
くないことがある。具体的な添加量は、原料果実
の種類、砂糖・ブドウ糖等の甘味料の濃度等を考
慮し、上記の範囲内で適宜に選択される。
アセスルフアムKの果汁飲料への添加は、出来
上りの果汁飲料中に上記の範囲量で含有せしめれ
ばよく、添加の方法および時期は特に限定されな
い。たとえば、原料果汁あるいはシロツプに直接
に溶解する方法、甘味料、酸味料、着香料、着色
料等と予じめ混合して添加する方法などが適宜に
選択できる。その他、本発明の果汁飲料製造法
は、アセスルフアムKを添加すること以外は、通
常の果汁飲料の製造法に従つて実施すればよい。
本発明の製造法により得られた果汁飲料は、製
造直後の良好な風味を長期間保持することがで
き、嗜好性の高いものである。すなわち、通常の
製造法により得たものは、保存中にいわゆる日向
臭、枯草臭、イモ臭といわれる経日臭が発生して
くるのに対し、本製造法によりアセスルフアムK
を果実飲料に添加することにより、このような風
味劣化が商品価値上、問題とならない程度までに
抑制することができる。またアセスルフアムKは
苦味をともなう甘味料であるが、本発明にて用い
られる濃度程度では苦味がほとんど感じられな
い。
以下、実験例および実施例により、本発明をさ
らに詳細に説明する。
実施例 1
常法により得た6倍濃縮温州ミカン果汁1.7g、
クエン酸0.2g、アスコルビン酸0.05gに表−1
に示すような甘味料を加え、次いで100mlになる
ように水を加えてから、98℃で15秒間加熱減菌
後、冷却しビンに詰めて10%果汁含有清涼飲料を
調製した。
これらの試料について、製造直後ならびに40℃
1ケ月保存後に、味覚パネル16名を用いて二点比
較法による官能検査法にて、甘味料として蔗糖だ
けを用いた試料を対照として比較評価した。
The present invention relates to a method for producing a fruit juice beverage. Fruit juice drinks are widely used as drinks that match modern tastes, and many types of fruit juices are used, including citrus fruits such as mandarin oranges, grapes, and apples. The products are also packaged in a variety of ways, including bottled, canned, and carton boxes. Fruit juice drinks may have good flavor immediately after production, but
It has the disadvantage of gradually producing a sun-related odor, such as a sun odor, a hay odor, or a potato odor. It is said that such aging odor is caused by oxidation of oils and fats derived from fruit juice and browning due to sugars and amino acids in the product, but this has not yet been clarified. Conventionally, in order to prevent aging odor, sulfites and L-cysteine hydrochloride have been used in the raw fruit juice, and vitamin C, erythorbic acid, polymerized phosphates, etc. have been used in the production of fruit juice drinks. However, the results are not satisfactory due to insufficient effects. The inventor of the present invention has been studying various methods for producing fruit juice drinks that are highly palatable and do not produce odors over time, and found that when a certain oxathiazinone derivative is added at a specific concentration, the resulting product can be stored for a long period of time. They found that it has very high palatability and does not produce any odor due to aging, and after further study, they completed the present invention. That is, in the production of a fruit juice beverage, the present invention provides about 0.0006 to 0.006% by weight of 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-one-2,2-dioxide to the beverage. This is a method for producing a fruit juice drink characterized by adding potassium. 6-Methyl-3,4-dihydro-1,2,3-oxathiazin-4-one-2,2-dioxide-potassium used in the present invention is a known sweetener substance, for example, in Japanese Patent Application Laid-Open No. 51-34182. It is obtained by the manufacturing method described in No. In the present specification, the sweet substance is referred to as "acesulfame K" in the following description. Next, the fruit juice beverage as used in the present invention refers to juice obtained by squeezing fruit, or a beverage obtained by appropriately processing this as a raw material. In other words, citrus fruits such as Satsuma mandarin oranges, Valencia oranges, summer mandarin oranges, and grapefruits, fruits such as grapes, apples, pine apples, peaches, pears, and bananas are squeezed using conventional methods, and dilutions using this as original fruit juice. Examples include fruit juice or concentrated fruit juice. Above all,
It is preferably applied to fruit juice drinks made from citrus fruits. The fruit juice content can be anything within the range that is included in normal fruit juice drinks; for example, if the original fruit juice is expressed as 100%, it is about 5 to 600%.
of fruit juice content. Fruit juice drinks contain sweeteners (e.g., sugar, high-fructose sugar, glucose, fructose, etc.), acidulants (e.g., citric acid, fumaric acid, malic acid, lactic acid, etc.), and vitamins (e.g., vitamin C, vitamin A, etc.).
B1 , vitamin B2 , etc.), colorants, flavorings, etc.
It may be contained as needed depending on the type of fruit juice beverage, and it may also be of a type containing appropriate amounts of sandbags and pulp. In the production method of the present invention, acesulfame K is contained in the fruit juice beverage in an amount of about 0.0006 to 0.006% by weight. If the amount added is less than this amount, the effect of preventing the generation of aging odor in fruit juice drinks, which is the objective of the present invention, will not be significant, and if added beyond the above range, bitterness may be felt and may be undesirable. be. The specific amount to be added is appropriately selected within the above range, taking into consideration the type of raw fruit, the concentration of sweeteners such as sugar and glucose, and the like. Acesulfum K can be added to a fruit juice beverage by just containing it in the above-mentioned range of amount in the finished fruit juice beverage, and the method and timing of addition are not particularly limited. For example, a method of directly dissolving it in raw fruit juice or syrup, a method of adding it by mixing it with a sweetener, an acidulant, a flavoring agent, a coloring agent, etc. in advance can be selected as appropriate. In addition, the method for producing a fruit juice beverage of the present invention may be carried out in accordance with a conventional method for producing a fruit juice beverage, except for adding acesulfame K. The fruit juice beverage obtained by the production method of the present invention can maintain a good flavor immediately after production for a long period of time, and is highly palatable. In other words, products obtained by conventional manufacturing methods develop odors such as sunlight, dried grass, and potato odors during storage, but with this manufacturing method, acesulfam K
By adding to fruit drinks, such flavor deterioration can be suppressed to the extent that it does not pose a problem in terms of commercial value. Acesulfame K is a sweetener with a bitter taste, but at the concentration used in the present invention, the bitter taste is hardly felt. Hereinafter, the present invention will be explained in further detail using experimental examples and examples. Example 1 1.7 g of 6-fold concentrated unshiu mandarin juice obtained by a conventional method,
Table 1 for citric acid 0.2g and ascorbic acid 0.05g
A sweetener as shown above was added thereto, water was added to make up to 100 ml, the mixture was sterilized by heating at 98°C for 15 seconds, cooled, and bottled to prepare a soft drink containing 10% fruit juice. For these samples, immediately after production and at 40℃
After storage for one month, a sensory evaluation using a two-point comparison method was conducted using 16 taste panelists, using a sample using only sucrose as a sweetener as a control.
【表】
この結果、試料2は保存による日向臭の発生は
少ないものの、製造直後からアセスルフアムKに
よる苦味を感ずるパネルがあり、好ましくない飲
料であつた。一方、試料3および4は、日向臭が
少なく風味もきわめて良好であつた。試料6は、
対照とほとんど変らず日向臭がつよい飲料であつ
た。
またこの実験で、アセスルフアムKが清涼飲料
中できわめて安定性であることも確認された。
実施例 1
常法により得たぶどう果汁4.5、クエン酸9
g、砂糖684g、アセスルフアムK0.38g、ビタ
ミンC5g、グレープエツセンス2mlを水と混合
して10のグレープジユースを調製した。
本品を200mlの内面塗装缶に充填したのち、40
℃で2ケ月保存した風味はきわめて良好であつ
た。
実施例 2
うんしゆうみかん1/6濃縮果汁340g、砂糖990
g、アセスルフアムK0.2g、クエン酸20g、ビ
タミンC5gおよびオレンジエスセンス10gに水
を加えて均一に溶解し、全量を10にしたのち、
約95℃で約20秒間殺菌し、200mlのビンに注入し
てオレンジジユースを調製した。
本品は、40℃で1ケ月保存した後も風味は良好
であつた。
実施例 3
うんしゆうみかん1/5濃縮果汁を常法によつて
製造し、これにアセスルフアムKを0.006%添加
した。
本品を1.8ビンに注入し、40℃2ケ月保存し
たが、経日臭の発生はわずかしか認められず品質
的に良好であつた。
また、本品を原料にして製造したオレンジジユ
ースは、風味のよいものであつた。
実施例 4
りんご1/5濃縮果汁1Kg、リンゴ酸5g、ビタ
ミンC10g、砂糖400g、アセスルフアムK0.1g
およびリンゴエツセンス5gに水を加えて均一に
溶解し、全量を10にしてリンゴジユースを調製
した。
本品を200mlの内面塗装缶に充填したのち、40
℃で2ケ月保存したが、風味は良好であつた。[Table] As a result, although sample 2 did not produce much sunlight odor due to storage, some panels noticed a bitter taste due to acesulfame K immediately after production, and it was an undesirable drink. On the other hand, Samples 3 and 4 had very good flavor with little sunlight odor. Sample 6 is
The drink had a strong sun smell, almost the same as the control. This experiment also confirmed that acesulfame K is extremely stable in soft drinks. Example 1 Grape juice obtained by conventional method 4.5, citric acid 9
10 grape juices were prepared by mixing 684 g of sugar, 0.38 g of acesulfame K, 5 g of vitamin C, and 2 ml of grape essence with water. After filling this product into a 200ml inner-coated can,
The flavor after storage at ℃ for 2 months was very good. Example 2 Unshiyuu mandarin orange 1/6 concentrated fruit juice 340g, sugar 990g
g, Acesulfam K0.2g, citric acid 20g, vitamin C5g and orange essence 10g, add water and dissolve uniformly to bring the total amount to 10, then
Orange juice was prepared by sterilizing it at about 95°C for about 20 seconds and pouring it into a 200ml bottle. This product maintained good flavor even after being stored at 40°C for one month. Example 3 1/5 concentrated fruit juice of Unshiyu mandarin oranges was produced by a conventional method, and 0.006% acesulfame K was added thereto. This product was poured into a 1.8 bottle and stored at 40°C for 2 months, but only a slight odor was observed and the quality was good. In addition, orange juice produced using this product as a raw material had a good flavor. Example 4 Apple 1/5 concentrated fruit juice 1 kg, malic acid 5 g, vitamin C 10 g, sugar 400 g, acesulfame K 0.1 g
Then, water was added to 5 g of apple juice to dissolve it uniformly, and the total amount was adjusted to 10 to prepare apple juice. After filling this product into a 200ml inner-coated can,
Although it was stored at ℃ for 2 months, the flavor remained good.
Claims (1)
0.0006〜0.006重量%の6−メチル−3,4−ジ
ヒドロ−1,2,3−オキサチアジン−4−オン
−2,2−ジオキシド−カリウムを添加すること
を特徴とする果汁飲料の製造法。1. When producing fruit juice drinks, approximately
A method for producing a fruit juice beverage, which comprises adding 0.0006 to 0.006% by weight of 6-methyl-3,4-dihydro-1,2,3-oxathiazin-4-one-2,2-dioxide-potassium.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP58028301A JPS59154969A (en) | 1983-02-21 | 1983-02-21 | Preparation of fruit juice drink |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP58028301A JPS59154969A (en) | 1983-02-21 | 1983-02-21 | Preparation of fruit juice drink |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS59154969A JPS59154969A (en) | 1984-09-04 |
JPH0260307B2 true JPH0260307B2 (en) | 1990-12-14 |
Family
ID=12244793
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP58028301A Granted JPS59154969A (en) | 1983-02-21 | 1983-02-21 | Preparation of fruit juice drink |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS59154969A (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6610647B2 (en) * | 2000-08-15 | 2003-08-26 | International Flavors & Fragrances Inc. | Fragrance molecule |
JP5574662B2 (en) * | 2009-10-01 | 2014-08-20 | 株式会社 伊藤園 | Method for suppressing warming deterioration of fruit juice for warm sale, method for producing fruit juice for warm sale, and fruit juice drink for warm sale |
-
1983
- 1983-02-21 JP JP58028301A patent/JPS59154969A/en active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS59154969A (en) | 1984-09-04 |
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