JPH02217777A - Method and device for drying granular body - Google Patents

Method and device for drying granular body

Info

Publication number
JPH02217777A
JPH02217777A JP3609389A JP3609389A JPH02217777A JP H02217777 A JPH02217777 A JP H02217777A JP 3609389 A JP3609389 A JP 3609389A JP 3609389 A JP3609389 A JP 3609389A JP H02217777 A JPH02217777 A JP H02217777A
Authority
JP
Japan
Prior art keywords
drying
dried
gas
bed dryer
jet stream
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP3609389A
Other languages
Japanese (ja)
Inventor
Shinji Matsuura
真司 松浦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ube Corp
Original Assignee
Ube Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ube Industries Ltd filed Critical Ube Industries Ltd
Priority to JP3609389A priority Critical patent/JPH02217777A/en
Publication of JPH02217777A publication Critical patent/JPH02217777A/en
Pending legal-status Critical Current

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  • Drying Of Solid Materials (AREA)

Abstract

PURPOSE:To obtain a given drying degree while shortening temperature rising time and preventing variability in stagnation and contrive the shortening of drying time by a method wherein jet stream layer drying and the moving layer drying of bodies to be dried, which have finished the jet stream layer drying already, are effected in parallel at the same time. CONSTITUTION:A supplying valve 3a at the lower part of a material supplying hopper 3 is opened and bodies to be dried or nylon chips 10 are thrown until they arrive at a predetermined height of layer in the annular section A of a jet stream layer drier 2, then, the supplying valve 3a is closed. At this moment, a moving layer drier 11 is filled with the nylon chips 10, which have finished jet stream layer drying already, high-temperature N2 gas, having the temperature of 130 deg.C for example, is injected through the multitude of small holes of a distributing tube 12 arranged in the lower zone of the drier 11 to make the gas flow upward through gaps between the filled nylon chips 10 and the speed of the gas is increased at the part of a throat to form jet stream layer and effect the preheating drying of the nylon chips 10 in the jet stream layer drier 2. Subsequently, the amount of the N2 gas is reduced and the nylon chips 10, stagnating in the jet stream layer drier 2 while being circulated, are droppin into the moving layer drier 11.

Description

【発明の詳細な説明】 [産業上の利用分野] 本発明は、粒状物の乾燥方法および装置に係り、特に、
ナイロンチップ等の内部水を含む吸水性樹脂チップの乾
燥に好適な噴流層と移動層とを組み合わせた粒状物の乾
燥方法および装置に関する。
DETAILED DESCRIPTION OF THE INVENTION [Field of Industrial Application] The present invention relates to a method and apparatus for drying granular materials, and in particular,
The present invention relates to a method and apparatus for drying granular materials that combine a spouted bed and a moving bed, suitable for drying water-absorbing resin chips containing internal water, such as nylon chips.

[従来の技術] 従来1 このような樹脂チップ等の被乾燥物を乾燥する
粒状物乾燥装置として第6図に示すような円錐型回転真
空乾燥機100がある0円錐型回転真空乾燥機100は
円錐形の容器lO1を2つ組み合わせて回転自在に配設
されている。容器101の内部にはスチームジャケット
102およびスチームバイパス(伝熱管)103が設け
られ、外部から加熱スチームが供給され円錐形の容器の
内部を加熱するようになっている。
[Prior Art] Conventional 1 There is a conical rotary vacuum dryer 100 as shown in FIG. 6 as a granular material drying device for drying materials to be dried such as resin chips. Two conical containers 1O1 are combined and arranged so as to be freely rotatable. A steam jacket 102 and a steam bypass (heat transfer tube) 103 are provided inside the container 101, and heated steam is supplied from the outside to heat the inside of the conical container.

一方、容器101の内部には、容器101内で発生する
ガスを吸引するガス吸引口104が設けられている。こ
の容器101は外部に設けられた回転装置105により
2回転されるようになって容器中に被乾燥材を収容し、
下部から熱ガスを供いる。
On the other hand, a gas suction port 104 is provided inside the container 101 to suck gas generated within the container 101. This container 101 is rotated twice by a rotating device 105 provided outside, and the material to be dried is stored in the container.
Hot gas is supplied from the bottom.

このように構成された円錐型回転真空乾燥機100に、
上方に供給口106から被乾燥物、例えば、ナイロンチ
ップ等の被乾燥物を供給し、供給口106を閉じる。
In the conical rotary vacuum dryer 100 configured in this way,
A material to be dried, such as a nylon chip, is supplied upward from the supply port 106, and the supply port 106 is closed.

次に1円錐型回転真空乾燥機100を回転させスチーム
ジャケラ)102およびスチームバイパス1.03にス
チームを供給して内部の被乾燥物を加熱しながら乾燥す
る。
Next, the one-cone rotary vacuum dryer 100 is rotated to supply steam to the steam jacket 102 and the steam bypass 1.03, thereby drying the material to be dried inside while heating it.

また、他の従来の装置として流動層乾燥装置が用いられ
ている。
Additionally, a fluidized bed dryer is used as another conventional device.

この種の乾燥装置の一例として、例えば特公昭60−1
2555号公報には、整流網(多孔板)の下方から熱風
を送入して流動層を形成し、被乾燥物と熱風との間で熱
の伝達と水分の移動を行なわせ、被乾燥物を乾燥させる
ようにした装置が示されている。
As an example of this type of drying device, for example,
Publication No. 2555 discloses that hot air is introduced from below a rectifying net (perforated plate) to form a fluidized bed, and heat is transferred and moisture is transferred between the material to be dried and the hot air. An apparatus for drying is shown.

また、他に、図示しないが、円筒移動層ドライヤがある
。この円筒移動層ドライヤは、円筒形の給して向流で流
して、被乾燥材を乾燥するようになっている。
In addition, although not shown, there is a cylindrical moving bed dryer. This cylindrical moving bed dryer is designed to dry the material to be dried by supplying a cylindrical material and flowing the material in countercurrent.

ところで、従来は上記のように円錐型回転真空乾燥機1
00や、流動層乾燥装置1円筒移動層型ドライヤが用い
られてきたが、ナイロンには、−NHCO−という親木
性基があるため、吸湿した水分は、表面水分だけでなく
、内部水分として存在し、乾燥が拡散律速であるため、
温度を上げないと容易に乾燥できない、ところが、温度
を上げると、酸素が存在する雰囲気では、容易に酸化劣
化、M変し、製品品質を維持できなくなるため、真空雰
囲気または、N2雰囲気で乾燥されている。
By the way, conventionally, as mentioned above, the conical rotary vacuum dryer 1
00 and fluidized bed dryer 1 cylindrical moving bed dryers have been used, but since nylon has a wood-philic group called -NHCO-, absorbed moisture is absorbed not only as surface moisture but also as internal moisture. exists and drying is diffusion-limited,
It cannot be easily dried without raising the temperature.However, if the temperature is raised, in an atmosphere where oxygen is present, it will easily undergo oxidative deterioration and M change, making it impossible to maintain product quality, so it is dried in a vacuum atmosphere or N2 atmosphere. ing.

[発明が解決しようとする課′g!U]しかしながら、
このような性状を有するナイロンチップ等の被乾燥物を
上記したような従来技術の乾燥機によって乾燥する場合
には1次のような問題点がある。
[The problem that the invention aims to solve! U] However,
When drying an object to be dried such as a nylon chip having such properties using a conventional dryer as described above, there are the following problems.

円錐型回転真空乾燥機100では、伝熱は、ベレット同
士の熱伝導で行なわれるため、均一な温度になるまで時
間がかかっていた。したがって。
In the conical rotary vacuum dryer 100, heat is transferred between pellets, so it takes time to reach a uniform temperature. therefore.

例えば120℃の蒸気で加熱しても、水分1.0%から
所定の水分0.05%まで乾燥するのに12hrかかっ
ていた。しかも、これはバッチ式であるため、切替えに
人手を必要とした。
For example, even when heated with steam at 120° C., it took 12 hours to dry from 1.0% moisture to the predetermined moisture content of 0.05%. Moreover, since this was a batch type, manual switching was required.

伝熱係数の高い流動層乾燥装置は、所定温度に速く、し
かも均一温度にすることができ、例えば、水分1.0%
から所定の水分0.05%にするのに、130℃の熱ガ
スで連続式で約8hr、バッチ式では約6hrと短かい
時間で乾燥できる。しかし、連続装置にするためには、
粒子による滞留時間のバラツキを少なくするため、多段
にする等の工夫が必要な上に、熱ガスを供給するための
ブロアの動力が非常に大であった。
Fluidized bed drying equipment with a high heat transfer coefficient can quickly and uniformly reach a predetermined temperature.
It takes about 8 hours to dry with hot gas at 130° C. continuously, or about 6 hours in a batch method, to reduce the moisture content to the specified 0.05%. However, in order to make it a continuous device,
In order to reduce the variation in residence time due to particles, it was necessary to take measures such as using multiple stages, and the power of the blower for supplying hot gas was extremely large.

また、ナイロンに、ガラス等を混ぜるコンパウンドの場
合、品種が多く、数日毎に品種を切り替えるとき、混ざ
らないよう、乾燥器内部を水洗する必要がある。このと
き、整流網(多孔板)型ディストリビュータを有す通常
の流動層型乾燥装置では、水が空気室側に入ってしまう
という問題がある。
In addition, in the case of compounds that mix nylon with glass, etc., there are many types, and when changing types every few days, it is necessary to wash the inside of the dryer with water to prevent mixing. At this time, in a normal fluidized bed type drying apparatus having a rectifying network (perforated plate) type distributor, there is a problem that water enters the air chamber side.

また、円筒移動層型ドライヤは、連続式ではあるが、下
部から熱ガスを供給し、向流で流すため、入口部の熱ガ
ス温度が下がるため、所定の温度になるまでに時間を要
し、乾燥時間は、例えば110℃の熱ガスで水分1.0
%から所定の水分0.05%にするのに13hr近くか
かる。
In addition, although the cylindrical moving bed dryer is a continuous type, hot gas is supplied from the bottom and flows in countercurrent, so the temperature of the hot gas at the inlet decreases, so it takes time to reach the specified temperature. , the drying time is, for example, 110℃ hot gas and moisture 1.0
% to the specified moisture content of 0.05% takes nearly 13 hours.

このように、連続式流動層乾燥装置ではメリットとして
被乾燥材が早く昇温するが、滞留時間が不均一であり、
かつ、流動化用の熱ガス供給ブロアの動力が非常に高い
とのデメリットを有する一方、円筒移動層型ドライヤは
、滞留時間が均一化するというメリットがあるが、昇温
時間が大11】にかかるというデメリー2トがある。
In this way, the continuous fluidized bed dryer has the advantage that the temperature of the material to be dried rises quickly, but the residence time is uneven,
Moreover, the disadvantage is that the power of the hot gas supply blower for fluidization is very high, while the cylindrical moving bed dryer has the advantage that the residence time is uniform, but the temperature rise time is large11]. There are two disadvantages: it takes a long time.

また、他の従来例においては、昇温時間がかかるという
問題がある。
Further, in other conventional examples, there is a problem that it takes a long time to raise the temperature.

本発明は、上記した従来技術の諸問題点に鑑みなされた
もので、その目的とするところは、噴流層乾燥装置と移
動層型ドライヤとのそれぞれの特徴を生かし、昇温時間
を短かく、滞留のバラッキを防止して一定の乾燥度とす
ることができ、乾燥時間も全体的に短かい粒状物の乾燥
方法および装置を提供することにある。
The present invention has been made in view of the problems of the prior art described above, and its purpose is to shorten the temperature rise time by taking advantage of the respective characteristics of the spouted bed dryer and the moving bed dryer. It is an object of the present invention to provide a method and apparatus for drying granular materials, which can prevent fluctuations in retention, provide a constant degree of dryness, and shorten the overall drying time.

[課題を解決するための手段1 1記目的を達成するために1本発明では、粒状物である
被乾燥物を高温ガスを用いて、噴流層で短かい時間で均
一に加熱するとともに、一定程度乾燥させ、然る後、こ
の噴流層乾燥された被乾燥物を高温ガスを用いて移動層
で所望の滞留時間を以て乾燥させて所定の乾燥度とする
場合に、前記噴流層乾燥と、既に噴流層乾燥を終えた被
乾燥物の前記移動層乾燥とを同時に並行させて行なうよ
うにした。
[Means for Solving the Problems 1 To Achieve the Object 1] In the present invention, a granular material to be dried is uniformly heated in a short time using a high-temperature gas in a spouted bed, and is heated at a constant temperature. When drying the spouted bed-dried material to a predetermined degree of dryness by drying the spouted-bed-dried material for a desired residence time in a moving bed using high-temperature gas, the spouted-bed drying and the The moving bed drying of the dried material after spouted bed drying was carried out at the same time.

また、この方法を実施するための粒状物の乾燥装置とし
ては、容器の下部に逆截頭円錯頭状部をイ]した2つの
縦型容器を配管にて接続し、上部縦型容器の内部下方に
高温の熱媒体を流す伝熱管群を設けるとともに、この伝
熱管群の上方位置に被乾燥物の供給口とガス排出口を設
け、さらに、下部縦型容器の内部下方に高温ガスの吹込
管を設け。
In addition, as a drying device for granular materials to carry out this method, two vertical containers each having an inverted truncated round part at the lower part of the container are connected by piping, and the upper vertical container is connected by piping. A group of heat transfer tubes for flowing a high-temperature heat medium is provided in the lower part of the container, and a supply port and a gas outlet for the material to be dried are provided above the group of heat transfer tubes. Install a blow pipe.

前記縦型容器を噴流層乾燥部とし、後記縦型容器を移動
層乾燥器とした構成にした。
The vertical container was configured as a spouted bed drying section, and the vertical container described later was configured as a moving bed dryer.

[作用] 本発明における粒状物乾燥装置は、と段部に噴流層乾燥
器を、また下段部に移動層乾燥器を重ねて設けたもので
、粒状物の乾燥をする場合、内部水分を含有した粒状の
ナイロンチップ等の被乾燥物が、まず、噴流層乾燥器に
入り、ここで移動層乾燥器から上昇してきた高温のガス
で噴流化されて均一に加熱されるとともに所定の水分が
飛ばされて一定程度に比較的短時間に乾燥され2次に。
[Function] The granular material drying device of the present invention is provided with a spouted bed dryer in the upper stage and a moving bed dryer in the lower stage, and when drying the granular material, it is necessary to dry the granular material containing internal moisture. The material to be dried, such as granular nylon chips, first enters the spouted bed dryer, where it is turned into a jet by the high temperature gas rising from the moving bed dryer, and is uniformly heated and a predetermined amount of moisture is blown off. Secondary, it is dried to a certain extent in a relatively short time.

これにより乾燥された被乾燥物は、下段部分の移動層乾
燥器に既に噴流層乾燥器で一定程度乾燥された被乾燥物
が充填され、−旦充填された被乾燥物は移動層乾燥器間
部のロータリバルブより抜き出されるため移動層となり
、この移動層では容器下部のガス供給管を経由して分散
管から吹込まれる高温ガスが被乾燥物の各粒子間を通過
して被乾燥物が最終的に乾燥される。この移動層乾燥器
では充分な滞留時間をとって乾燥されるので、滞留時間
のバラツキを無くした状態で乾燥される0本装置におい
ては1粒状物の乾燥が噴流層乾燥器における予備乾燥と
、流動層乾燥器における本乾燥が同時に併行して行なわ
れるため、全体として比較的短時間で一定程度まで乾燥
される。噴流層乾燥器で前記のごとく所定時間の乾燥が
行なわれると、移動層乾燥器で乾燥された被乾燥物が容
器下部の被乾燥物排出口から所定量抜き出され、噴流層
乾燥器で一定程度乾燥された被乾燥物が、噴流層乾燥器
と移動層乾燥器間のスロート部を通って藷下し移動層乾
燥器に導かれる。同時に、容器上部の供給口から新たな
被乾燥物が噴流層乾燥器に所定高さまで投入されて、以
下同様な乾燥作用が行なわれる。
As a result, the drying material that has been dried to a certain extent in the spouted bed dryer is filled into the moving bed dryer in the lower stage, and the dried material that has been filled is placed between the moving bed dryer. It becomes a moving bed because it is extracted from the rotary valve at the bottom of the container, and in this moving bed, the high-temperature gas blown from the dispersion tube via the gas supply pipe at the bottom of the container passes between each particle of the material to be dried, is finally dried. In this moving bed dryer, sufficient residence time is allowed for drying, so drying is performed with no variation in residence time. Since the main drying in the fluidized bed dryer is carried out at the same time, the entire product can be dried to a certain degree in a relatively short time. When drying is carried out for a predetermined period of time in the spouted bed dryer as described above, a predetermined amount of the dried material dried in the moving bed dryer is extracted from the drying material outlet at the bottom of the container, and the material is dried at a constant rate in the spouted bed dryer. The material to be dried, which has been dried to a certain extent, passes through the throat section between the spouted bed dryer and the moving bed dryer, and is then drained and guided to the moving bed dryer. At the same time, new material to be dried is introduced into the spouted bed dryer from the supply port at the top of the container to a predetermined height, and the same drying operation is performed thereafter.

[実施例] 以下1本発明を図示の実施例に基づいて説明する。第1
図は本発明の粒状物乾燥装置の縦断面図、第2図は第1
図のII −IIからみた断面図、第3図は第2図のm
−■からみた本発明の粒状物乾燥装置のガス供給管と分
散管の断面図、第4図は第1図のV−Vからみた断面図
、第5図は被乾燥物(ナイロンチップ)の乾燥工程を示
すグラフである。第1図、R2図、第3図、第4図およ
び第5図を用いて本実施例を説明する。
[Example] The present invention will be explained below based on the illustrated example. 1st
The figure is a longitudinal sectional view of the granular material drying device of the present invention, and FIG.
A sectional view taken from II-II in the figure, Figure 3 is m in Figure 2.
- sectional view of the gas supply pipe and dispersion pipe of the granular material drying apparatus of the present invention seen from It is a graph showing a drying process. This embodiment will be explained using FIG. 1, FIG. R2, FIG. 3, FIG. 4, and FIG. 5.

粒状物乾燥装置lは、上段部が噴流層乾燥器2、下段部
が移動層乾燥器11として構成され、上段部の噴流層乾
燥器2をナイロンチップlOの予熱乾燥としての役割を
、さらに下段部の移動層乾燥器11においては主要乾燥
としての役割を有している。
The granular material drying device 1 is configured with a spouted bed dryer 2 in the upper stage and a moving bed dryer 11 in the lower stage. In the moving bed dryer 11 in the section, it plays the role of main drying.

まず、噴流層乾燥器2の構成について述べる。First, the configuration of the spouted bed dryer 2 will be described.

噴流層乾燥器2の最上部には上側に向いている截頭円錐
筒状部2c、中段部には円筒状直胴部2b、および最下
段には下側に向いている逆蓼頭円錐筒状部2aからなり
、さらに、原料供給ホッパ3とサイクロン4および伝熱
管群5等がそれぞれ組合わされて構成されている0図中
、白抜き矢印はガスの流れ方向を、また、黒ぬり矢印は
被乾燥物の粒子の流れ方向を示す、ここで、まず、噴流
層について簡単に述べる。噴流層は一般的に最下段の逆
截頭円錐筒状部2aのガス導入口であるスロート部6か
ら上向きに噴出して形成されるガスの通路であるスパウ
ト部Bと、最下段の逆截頭円錐筒状部2aよりすべりな
がら移動してきたナイロンチップ10原料が、−旦、前
記スパウト部Bでガスに同伴されて上部に移送され、移
動されたナイロンチップ1OJilは途中でガスから与
えられた連動エネルギを失って、ガス抵抗の少ない円筒
状直胴部2bとスパウト部B間のアニユラ部Aに落下す
る。落下したナイロンチップ10原料は、移動層状のア
ニユラ部Aを形成する。アニユラ部Aにあるナイロンチ
ップ10は、円筒状1な胴部2bと緑下段の逆截頭円錐
筒状部2aをすべって下方に移動し、最後にスパウト部
Bを通るガス中に排出されるとともに、ガス中に排出さ
れたナイロンチップ10原料は、スパウト部Bのガスの
上昇流に伴なって上部に同伴され、そこでエネルギを失
って、再度アニユラ部Aの界面に堆積されるといった粒
子の循環流れを生じた噴流層を形成している。こうした
噴流層を利用した噴流層乾燥器2において、噴流層乾燥
器2へ乾燥原料であるナイロンチップ10を供給するた
めに、原料供給ホッパ3の下部から円筒状直胴部2bに
向け、適宜な角度に傾斜させて配管3bを配設し、配管
3b途」−の適宜な位置に供給弁3aを取付け、原料供
給ホッパ3に供給した原料のナイロンチップ10を供給
弁3aを必要に応じて開閉することで噴流層乾燥器2に
供給できるようになっている。また、サイクロン4の入
口部が截頭円錐筒状部2Cと配管4aを介して接続され
、また、サイクロン4の下部が円筒状直胴部2bと配管
4bを介してそれぞれ接続され、噴流層乾燥器2の最上
部のガス排出口16から排出されるガスに同伴されたナ
イロンチップlOをサイクロン4で、ガスとナイロンチ
ップ10に分離される0分離されたナイロンチップ10
はサイクロン4下部より円筒状直胴部2bに配設された
配管4bを通って噴流層乾燥器2内に戻され、ガスはサ
イクロン4の頂部より配管4Cを通って図示しない次工
程に送られる0次工程においては、例えば、図示しない
バグフィルタやN2ガスを連続的に循環して使用するた
めに除湿装置に通して除湿し、再度、ブロワで加圧した
後、熱交換器で所定温度まで加熱し、最後に後述する移
動層乾燥器11のガス供給管9から層内へ吹き込まれる
ことになる。ここで、前記したガス排出口16からのガ
スに同伴されて排出されるナイロンチップ10の排出量
を抑制するために、噴流乾燥器2内のスパウト部Bの上
部域に陣笠7を設けた。これは、スパウト部Bでガスか
ら授与。
The spouted bed dryer 2 has a truncated conical cylinder part 2c facing upward at the top, a cylindrical straight body part 2b at the middle stage, and an inverted conical conical cylinder facing downward at the bottom stage. In the figure, the white arrows indicate the gas flow direction, and the black arrows indicate the gas flow direction. First, a brief description of the spouted bed, which indicates the flow direction of particles of the material to be dried, will be given. The spouted layer generally consists of a spout part B, which is a gas passage formed by spouting upward from a throat part 6, which is a gas inlet of the inverted truncated conical cylindrical part 2a at the lowest stage, and a spout part B, which is a gas passage formed by spouting upward from the throat part 6 which is the gas introduction port of the inverted truncated conical cylindrical part 2a at the lowest stage. The raw material of nylon chips 10, which had been slidingly moved from the conical cylindrical part 2a, was then transported to the upper part of the spout part B along with the gas, and the moved nylon chips 1OJil were given by the gas on the way. It loses interlocking energy and falls into the annular part A between the cylindrical straight body part 2b and the spout part B, where gas resistance is low. The fallen nylon chip 10 raw material forms an annular part A in the form of a moving layer. The nylon chip 10 in the annular part A slides through the cylindrical body part 2b and the inverted truncated conical cylindrical part 2a of the lower green tier, moves downward, and is finally discharged into the gas passing through the spout part B. At the same time, the nylon chip 10 raw material discharged into the gas is entrained in the upper part with the upward flow of gas in the spout part B, where it loses energy and is deposited again on the interface of the annular part A. A spouted bed with circulating flow is formed. In the spouted bed dryer 2 that utilizes such a spouted bed, in order to supply the nylon chips 10, which are dry raw materials, to the spouted bed dryer 2, an appropriate amount of air is supplied from the lower part of the raw material supply hopper 3 toward the cylindrical straight body portion 2b. The pipe 3b is arranged at an angle, and the supply valve 3a is installed at an appropriate position on the pipe 3b, and the nylon chips 10 of the raw material supplied to the raw material supply hopper 3 are opened and closed as necessary. By doing so, it can be supplied to the spouted bed dryer 2. Further, the inlet part of the cyclone 4 is connected to the truncated conical cylindrical part 2C via the pipe 4a, and the lower part of the cyclone 4 is connected to the cylindrical straight body part 2b via the pipe 4b. The nylon chips 1O entrained in the gas discharged from the gas outlet 16 at the top of the vessel 2 are separated into gas and nylon chips 10 by the cyclone 4.0 Separated nylon chips 10
The gas is returned to the spouted bed dryer 2 from the bottom of the cyclone 4 through a pipe 4b arranged in the cylindrical straight body part 2b, and the gas is sent from the top of the cyclone 4 through a pipe 4C to the next process (not shown). In the 0th step, for example, it is dehumidified by passing it through a bag filter (not shown) or a dehumidifier for continuous circulation of N2 gas, pressurized again with a blower, and then heated to a predetermined temperature with a heat exchanger. It is heated and finally blown into the layer from a gas supply pipe 9 of a moving bed dryer 11, which will be described later. Here, in order to suppress the amount of nylon chips 10 that are discharged together with the gas from the gas discharge port 16, a cap 7 is provided in the upper region of the spout part B in the jet dryer 2. This is awarded by the gas at spout part B.

されて上方に移送されるナイロンチップ10の慣性力を
利用して陣笠7に衝突させ、強制的に飛散量を防止する
役割を有している。ここで、噴流層乾燥器2底部の逆截
頭円錐筒状部2aのコーン角度は少なくともナイロンチ
ップIOの安息角以上にすることが望ましい、また、円
筒状直胴部2bと逆截頭円錐筒状部2aに亘り伝熱管群
5が設けられている。この伝熱管群5は第1図に示すよ
うに、アニュ、う部Aの上部から下部に向けて移動する
粒子群をガスによる加熱とは別に、強制的に水蒸気など
の熱媒体で加熱するために設けたものであって、アニユ
ラ部Aの外側、すなわち、円筒状直胴部2bと截頭円錐
筒状部2aの内部側壁と。
The inertial force of the nylon chip 10 that is moved upward is used to collide with the camp hat 7, and has the role of forcibly preventing the amount of scattering. Here, it is desirable that the cone angle of the inverted truncated conical cylindrical portion 2a at the bottom of the spouted bed dryer 2 is at least equal to or greater than the repose angle of the nylon chip IO. A heat exchanger tube group 5 is provided across the shaped portion 2a. As shown in Fig. 1, this heat transfer tube group 5 is used to forcibly heat the particle group moving from the upper part of the hollow part A toward the lower part with a heat medium such as steam, in addition to heating with gas. It is provided on the outside of the annular part A, that is, on the inner side wall of the cylindrical straight body part 2b and the truncated conical part 2a.

アニユラ部Aの内側、すなわち、スパウト部B間を上下
方向に折り返えされて連続する伝熱管群5が設けられ、
内部に前記した高温の熱媒体として高温の蒸気が流れて
いる。ここで、伝熱管群5の先端部位置は、例えば、ア
ニユラ部Aの投影断面積の2/3までとするのがよい、
これは、伝熱管群5の先端部位置を伝熱管群5からナイ
ロンチップ】0への伝熱量を増やすために、アニユラ部
Aとスパウト部Bの境界域まで延長して配設すれば、ス
パウト部を上昇するガスとナイロンチップlOの混相涼
の影響を受けてナイロンチップ10が伝熱管群5に衝突
する割合が増え、これによってナイロンチップ10が変
形したり、割れたりしてナイロンチップIOの粉化や製
品の品質低下の原因になる。逆に、伝熱管群5の先端部
位置を噴流層乾燥器2の内壁寄りに配設すると、スパウ
ト部Bからの影響を受けない代わりに、伝熱管群5の伝
熱部活が小さくなり、熱媒体としての蒸気温度を変えな
い限り結果として伝熱管群5からナイロンチップ10へ
の伝熱量が減少して伝熱管群5の噴流層乾燥器2への配
設の意味が薄れてしまうことになる。
A heat exchanger tube group 5 is provided inside the annular part A, that is, between the spout parts B, and is folded back in the vertical direction and continuous.
High-temperature steam flows inside as the aforementioned high-temperature heat medium. Here, the position of the tip of the heat exchanger tube group 5 is preferably set to, for example, up to 2/3 of the projected cross-sectional area of the annular part A.
This can be done by extending the tip of the heat transfer tube group 5 to the boundary area between the annulus part A and the spout part B in order to increase the amount of heat transferred from the heat transfer tube group 5 to the nylon chip 0. Under the influence of the mixed phase cooling of the gas rising in the area and the nylon chip IO, the rate at which the nylon chip 10 collides with the heat transfer tube group 5 increases, which deforms or cracks the nylon chip 10, causing the nylon chip IO to collide with the heat exchanger tube group 5. This may cause powdering and deterioration of product quality. Conversely, if the tip of the heat exchanger tube group 5 is placed closer to the inner wall of the spouted bed dryer 2, it will not be affected by the spout portion B, but the heat transfer activity of the heat exchanger tube group 5 will be reduced, and the heat Unless the temperature of the steam as a medium is changed, the amount of heat transferred from the heat exchanger tube group 5 to the nylon chip 10 will decrease, and the meaning of arranging the heat exchanger tube group 5 in the spouted bed dryer 2 will diminish. .

また、噴流層乾燥器2の最下段の逆截頭円錐筒状部2a
と移動層乾燥器11の最上段部に設けられた截頭円錐筒
状部11c間に適宜な径を有したスロート部6を設けて
おり、噴流層乾燥器2で予め所望の水分値まで乾燥した
ナイロンチップ10を、次工程の移動層乾燥器11に送
るための接続管の役目を有するとともに、移動層乾燥器
11に送入された乾燥用ガス、例えば、N2ガスが移動
層乾燥器ll内を0 、1〜0 、2m/seaで上昇
し、さらに、スロー)・部6で8〜10 m/seeに
アップされる。このように、スロート部6における平均
ガス速度は、ナイロンチップの平均径、比重や形状によ
って変わるものであり、少なくともナイロンチップ10
がスロート部6のガス流速の抵抗に打勝って噴流層乾燥
器2から移動層乾燥器11に落下しない程度のガス速度
を有していることが必要である。これは、噴流層乾燥器
z内に原料供給ホッパ3から供給されたナイロンチップ
1、0が、一定の滞留時間内にガスの保有したエンタル
ピによって乾燥され、ナイロンチップ10のイアした水
分量を所定の保有含水率にまで低下させることが必要な
ためである。
In addition, the lowermost inverted truncated conical cylindrical portion 2a of the spouted bed dryer 2
A throat portion 6 having an appropriate diameter is provided between the truncated conical cylindrical portion 11c provided at the top of the moving bed dryer 11, and the spouted bed dryer 2 is used to dry the fluid to a desired moisture level in advance. It serves as a connecting pipe for sending the dried nylon chips 10 to the moving bed dryer 11 in the next step, and the drying gas, such as N2 gas, sent to the moving bed dryer 11 is transferred to the moving bed dryer II. It rises at 0, 1~0, 2m/sea in the inner part, and further increases to 8~10m/sea in the slow part 6. As described above, the average gas velocity at the throat portion 6 changes depending on the average diameter, specific gravity, and shape of the nylon tip.
It is necessary that the gas velocity be such that it overcomes the resistance of the gas flow velocity in the throat portion 6 and does not fall from the spouted bed dryer 2 to the moving bed dryer 11. This is because the nylon chips 1 and 0 supplied from the raw material supply hopper 3 into the spouted bed dryer z are dried by the enthalpy held by the gas within a certain residence time, and the amount of water in the nylon chips 10 is reduced to a predetermined level. This is because it is necessary to reduce the retained moisture content to .

一方、移動層乾燥器11は、前記した噴流層乾燥器2と
同様に、最上部には截頭円錐筒状部11C1中段部には
円筒状直胴部11b、および最下段には逆截頭円錐筒状
部11aから構成され、円筒状直胴部11bの下方にナ
イロンチップ10を乾燥させるために、ガスを供給する
ためのガス供給管9から分岐して、複数本の分岐管12
が所定のピッチで円筒状直胴部11bを貫通した後、容
器11bを横断して円筒状直胴部11bと略直角方向に
配設されている。また、それぞれのガス供給管9は図示
しないガスヘシダに接続され、さらにガスヘッダには高
温のN2ガス供給源(図示せず)が接続されている。第
2図に示すように。
On the other hand, the moving bed dryer 11, like the spouted bed dryer 2 described above, has a truncated conical cylindrical part 11C at the top, a cylindrical straight body part 11b at the middle part, and a reverse truncated cylindrical part 11b at the bottom. It is composed of a conical cylindrical part 11a, and in order to dry the nylon chip 10 below the cylindrical straight body part 11b, a plurality of branch pipes 12 are branched from the gas supply pipe 9 for supplying gas.
passes through the cylindrical straight body part 11b at a predetermined pitch, and then traverses the container 11b and is disposed in a direction substantially perpendicular to the cylindrical straight body part 11b. Further, each gas supply pipe 9 is connected to a gas header (not shown), and a high temperature N2 gas supply source (not shown) is further connected to the gas header. As shown in Figure 2.

ガス供給管9には所定ピッチで分散管12が導通して多
数配列され、分散管12の上方部13に設けられた無数
の小孔から高温のN2ガスが吹き出されるようになって
いる。すなわち、分散管12の断面において上方部13
は屋根型の尖った形状になっており、この屋根部(斜面
部)は1例えばパンチングメタル等の無数の小孔が穿設
された部材から形成され、その小孔の直径は例えばim
m程度とされる。また、このように分散管12の上方部
13を屋根型の尖った形状とすることにより。
A large number of dispersion pipes 12 are connected to the gas supply pipe 9 and arranged at a predetermined pitch, and high-temperature N2 gas is blown out from numerous small holes provided in the upper part 13 of the dispersion pipes 12. That is, in the cross section of the dispersion tube 12, the upper part 13
has a pointed roof-like shape, and this roof part (slope part) is formed from a member such as punched metal in which countless small holes are bored, and the diameter of the small holes is, for example, im.
It is said to be about m. Moreover, by making the upper part 13 of the dispersion pipe 12 into a roof-like pointed shape as described above.

内部に収容されたナイロンチップ10が抜かれる時に、
ナイロンチップ10が分散管12の上方部13に残って
高温度にさらされて黄変などして変色しないように構成
されている(第2図参照)。
When the nylon chip 10 housed inside is pulled out,
The structure is such that the nylon chip 10 remains in the upper part 13 of the dispersion tube 12 and does not change color due to yellowing or the like when exposed to high temperatures (see FIG. 2).

また、移動層乾燥器11に吹き込まれるガスは、このガ
ス供給配管9から分散管12を経由して。
Further, gas is blown into the moving bed dryer 11 from this gas supply pipe 9 via a dispersion pipe 12.

分散管12の上方部13に穿設され無数の小孔からN2
ガスが移動層乾燥器11の内部に収容されたナイロンチ
ップを流動化しない量が吹き込まれる。さらに、移動層
乾燥器11の最下部の逆截頭円錐筒状部11aの下端に
は、円錐状に縮径した、乾燥されたナイロンチップ10
用の被乾燥物排出口14が設けられ、その内部には、容
器itb内の被乾燥物を容器断面から均一に引き出すた
めの円錐状のバックル15が取付けられている。また、
前記ナイロンチップlO用の被乾燥物排出口14の下端
には、例えば、ロータリバルブ17を取付けて、移動層
乾燥器11に吹き込まれた乾燥用ガスのシールを行ない
ながらナイロンチップlOのみ連続的に排出できるよう
になっている。このため、移動層乾燥器11内に堆積さ
れたナイロンチップ10は、上部は噴流層乾燥器2かも
落下してくる被乾燥物と、下部には排出弁としてのロー
タリバルブ17を介して排出されるために、ナイロンチ
ップ10のフローパターンは移動層の状態を呈する。ま
た、この移動層乾燥器11の断面形状が円形に形成され
ているので、被乾燥物の排出時に下降する被乾燥物の流
れがスムースであり、角部での滞留がない。
N2 from countless small holes drilled in the upper part 13 of the dispersion pipe 12.
Gas is blown in an amount that does not fluidize the nylon chips contained within the moving bed dryer 11. Further, at the lower end of the inverted truncated conical cylindrical part 11a at the lowest part of the moving bed dryer 11, a dried nylon chip 10 with a reduced diameter in a conical shape is provided.
A conical buckle 15 is attached to the inside of the outlet 14 for the dried material to uniformly draw out the dried material in the container itb from the cross section of the container. Also,
For example, a rotary valve 17 is attached to the lower end of the drying material outlet 14 for the nylon chips 1O, and while sealing the drying gas blown into the moving bed dryer 11, only the nylon chips 1O are continuously removed. It can be discharged. For this reason, the nylon chips 10 deposited in the moving bed dryer 11 are discharged through the upper part of the spouted bed dryer 2 and the falling material to be dried, and the lower part through the rotary valve 17 as a discharge valve. Because of this, the flow pattern of the nylon chip 10 exhibits the state of a moving layer. Further, since the moving bed dryer 11 has a circular cross-sectional shape, the flow of the dried material descending when the dried material is discharged is smooth, and there is no accumulation at the corners.

このように構成された粒状物乾燥装置は次のように作動
する。
The thus constructed granular material drying apparatus operates as follows.

まず、噴流層乾燥器2に付随した原料供給ホッパ3下部
の供給弁3aを開き、アニユラ部Aの層高を所定の高さ
まで被乾燥物Tある例えばサイズが2.5mmφX2.
5mm文で、水分を例えば1%含有したナイロンチップ
10を投入した後、供給弁3aを閉じる。なお、このよ
うにナイロンチップ10の投入を開始する時点では、移
動層乾燥器11には既に噴流層乾燥を終えたナイロンチ
ップ10が充填されている。
First, the supply valve 3a at the bottom of the raw material supply hopper 3 attached to the spouted bed dryer 2 is opened, and the layer height of the annular part A is raised to a predetermined height.
After inserting the nylon chip 10 containing, for example, 1% water to a depth of 5 mm, the supply valve 3a is closed. Incidentally, at the time when the introduction of the nylon chips 10 is started in this manner, the moving bed dryer 11 is already filled with nylon chips 10 that have been subjected to spouted bed drying.

そして、移動層乾燥器1部下部城に配設された分散管1
2の多数の小孔から例えば温度が130°Cの高温のN
2ガスを噴出させ、移動層乾燥器11に充填されたナイ
ロンチップ10間の間隙を通って上方に流れ、これらの
N2ガスはスa −4部にてスピードアラプレで噴流層
を形成させて噴流層乾燥器2内のナイロンチップ10を
予熱乾燥させる。
Then, the dispersion pipe 1 installed in the lower part of the moving bed dryer 1
For example, high-temperature N of 130°C is released from the large number of small holes in
N2 gas is spouted out and flows upward through the gap between the nylon chips 10 filled in the moving bed dryer 11, and these N2 gases are formed into a spouted bed at a speed in section A-4. The nylon chips 10 in the spouted bed dryer 2 are preheated and dried.

そして、所定時間1例えば20分間程度、このような噴
流層乾燥して噴流層乾燥器2で所定温度まで均一に加熱
すると同時に、一定程度まで乾燥する1次に、移動層乾
燥器11に送入するN2ガス琶を減少させてスロート部
6でのガス速度を一旦減少させれば、噴流層乾燥器2内
で、循環しながら滞留しているナイロンチップlOが、
スロート部6のガス速度による抗力に打勝って移動層乾
燥器11に落下し、噴流層乾燥器2内のナイロンチップ
lOの保有状態を示す圧力損失は小さくなる。一定の圧
力損失値まで低下すれば、移動層乾燥器11へ吹き込む
ガス量を再度元の状態まで増大させた後、原料供給ホッ
パ3下部の供給弁3aを開いて噴流層乾燥器2内の圧力
損失が一定になるまでナイロンチップ10を供給する。
Then, it is dried in the spouted bed for a predetermined period of time (for example, about 20 minutes), heated uniformly to a predetermined temperature in the spouted bed dryer 2, and at the same time dried to a certain degree. Once the gas velocity at the throat portion 6 is reduced by reducing the N2 gas flow, the nylon chips 1O circulating and staying in the spouted bed dryer 2 will be
The nylon chips fall into the moving bed dryer 11 by overcoming the drag force due to the gas velocity in the throat portion 6, and the pressure loss indicating the state of retention of the nylon chips 1O in the spouted bed dryer 2 becomes small. When the pressure loss has decreased to a certain value, the amount of gas blown into the moving bed dryer 11 is increased again to the original state, and the supply valve 3a at the bottom of the raw material supply hopper 3 is opened to reduce the pressure inside the spouted bed dryer 2. Nylon chips 10 are fed until the loss becomes constant.

以」−の操作を行なう場合、噴流層乾燥器2内の圧力損
失値と移動層乾燥器11へのNZガスの流入星との相関
関係を裏面に調べておけば、これを利用してカスケード
制御による操作も可能であり、さらに供給弁3を電気的
に開閉可能にし、噴流層乾燥器2内の圧力損失が低下す
れば、供給弁3が開き、逆に、前記圧力損失が所定の値
になると閉じるようにカスケード制御することも容易に
可能である。
When performing the following operation, if you check the correlation between the pressure loss value in the spouted bed dryer 2 and the inflow of NZ gas into the moving bed dryer 11 on the back page, you can use this to perform the cascade Operation by control is also possible, and the supply valve 3 can be opened and closed electrically, so that when the pressure loss in the spouted bed dryer 2 decreases, the supply valve 3 opens, and conversely, the pressure loss decreases to a predetermined value. It is also easily possible to carry out cascade control so that it closes when the

次に、被乾燥物排出口14の排出弁であるロータリパル
プ17を所定の回転数に回転させながら、所望の値まで
乾燥の終了したナイロンチップ10を系外に排出できる
8なお、この場合、移動層乾燥′J:Allへ複数本の
分散管12より層内へ供給されたN2ガスは、分散管1
2上部の無数の小孔から噴出されてナイロンチップ10
の各々の粒子の間を通過して上昇する高温のN2ガスで
充分な滞留時間をとって乾燥される。
Next, while rotating the rotary pulp 17, which is the discharge valve of the drying material discharge port 14, to a predetermined rotation speed, the nylon chips 10 that have been dried to a desired value can be discharged from the system. Moving bed drying'J: The N2 gas supplied into the layer from multiple dispersion tubes 12 to All is transferred to the dispersion tube 1
2 Nylon chips 10 are ejected from the numerous small holes on the top.
The high-temperature N2 gas that passes through and rises between each particle allows sufficient residence time for drying.

このようなナイロンチップ10の乾燥工程は、第5図に
示すような過程をたどる。これにより。
The drying process of the nylon chip 10 follows the steps shown in FIG. Due to this.

ナイロンチップ10の各々の粒子は滞留時間のバラツキ
がない状態で乾燥される。なお、この噴流層乾燥器2で
の乾燥作用と移動層乾燥器11での乾燥作用は同時に併
行して行なわれている。また、噴流層乾燥器2内には整
流板がないため、該層内にナイロンチップ10が残留す
ることもなくさらに、高温ガスに何度もさらされて変色
、変質して品質が低下することがない、このことは、移
動層乾燥器11にもいえることであり5分散管12の上
方部13は屋根型をしているため、、t*層内における
残留ナイロンチップ10は見受けられない。
Each particle of the nylon chip 10 is dried with no variation in residence time. Note that the drying action in the spouted bed dryer 2 and the drying action in the moving bed dryer 11 are performed simultaneously. In addition, since there is no rectifying plate in the spouted bed dryer 2, the nylon chips 10 do not remain in the layer, and furthermore, there is no possibility that the nylon chips 10 will be exposed to high temperature gas many times and the quality will deteriorate due to discoloration and deterioration. This also applies to the moving bed dryer 11, and since the upper part 13 of the 5-distribution tube 12 is roof-shaped, no residual nylon chips 10 in the T* layer can be seen.

また、被乾燥物排出口14の上方中心部には円錐形のバ
ッフル15が設けられているので、移動層乾燥器11で
乾燥されたナイロンチップ10が容器から一様に抜き出
される。このため、部分的に滞留してその部分のナイロ
ンチップlOが乾燥され過ぎたりして品質が低下するこ
ともない。
Further, since a conical baffle 15 is provided at the upper center of the drying material outlet 14, the nylon chips 10 dried in the moving bed dryer 11 are uniformly extracted from the container. For this reason, there is no possibility that the nylon chips 10 in that part will become too dry due to partial retention and that the quality will deteriorate.

このような乾燥方法を採用した実験結果によれば、被乾
燥物の酸化劣化を起こさないことを条件として、N2ガ
ス温度を130℃とし、ナイロンチップの水分を1.0
%から0.05%にするのに乾燥時間は合計で約7hr
であり、従来の流動層乾燥装置だけで乾燥させる場合と
ほぼ同じ所要時間の短い乾燥時間である。しかもこの場
合、被乾燥物の滞留時間のバラツキがなく、各粒子が均
一でバラツキがなく一定の乾燥度の製品を得ることがで
きた。また、勿論、N2ガスを使用することにより酸化
劣化は起こらなかった。
According to the experimental results using such a drying method, the N2 gas temperature was set at 130°C and the moisture content of the nylon chips was set at 1.0°C, provided that the drying material did not undergo oxidative deterioration.
Total drying time is about 7 hours to change from % to 0.05%
This is a short drying time that is approximately the same as drying using a conventional fluidized bed dryer alone. Moreover, in this case, there was no variation in the residence time of the material to be dried, and it was possible to obtain a product in which each particle was uniform and had a constant degree of dryness. Moreover, of course, no oxidative deterioration occurred due to the use of N2 gas.

さらに、被乾燥物の切り替え時、内部の水洗を容易に行
なうことができた。
Furthermore, when changing the items to be dried, the inside could be easily washed with water.

なお、本実施例の場合、下段の移動層乾燥器11の充填
容積を噴流層乾燥器2での乾燥処理量よりも数倍から数
十倍大きくとることにより、移動層で一層均等に乾燥さ
せることができ、バラツキの少ない乾燥度の製品が得ら
れる。
In the case of this embodiment, by setting the filling volume of the lower moving bed dryer 11 to be several times to several tens of times larger than the drying capacity of the spouted bed dryer 2, the moving bed can dry more evenly. It is possible to obtain a product with a dryness with little variation.

さらに、以上の本実施例では移動層乾燥器11内を移動
層による乾燥とした場合を説明したが、例えば、容器の
下部被乾燥物排出目14に取付けたロータリバルブ17
を間欠的に駆動すれば、運転中に徐々に充填層を下降さ
せることなく固定層乾燥器としも良い、この場合、より
バラツキの少ない乾燥度とすることができる。
Furthermore, in the present embodiment described above, the case where the inside of the moving bed dryer 11 is dried by the moving layer has been explained, but for example, the rotary valve 17 attached to the lower part of the container to be dried is discharged 14
If it is driven intermittently, it can be used as a fixed bed dryer without gradually lowering the packed bed during operation, and in this case, dryness can be achieved with less variation.

なお、被乾燥物としてナイロンチップ10を用いて説明
したが、他の粒状物の乾燥物であっても使用し、得るこ
とはもちろんである。
Although the description has been made using the nylon chips 10 as the material to be dried, it goes without saying that other dried granular materials can also be used and obtained.

[発明の効果] 以上詳述したように、本発明における粒状物の乾燥方法
では、被乾燥物の全体的な乾燥時間が短かく、かつ、全
体的に熱ガス供給のための所要動力を減少することがで
き、さらに、均一でバラツキの小さい一定の乾燥度の製
品を得ることができる。また、噴流層乾燥器においてア
ニユラ部に伝熱管群を配設したため、噴出ガスによる乾
燥とは別に被乾燥物を加熱乾燥できるため、内部水分を
包含していて乾燥が困難な被乾燥物に対しても短時間で
確実かつ容易に所定の乾燥度に乾燥できる。
[Effects of the Invention] As detailed above, in the method for drying granular materials of the present invention, the overall drying time of the material to be dried is shortened, and the overall power required for supplying hot gas is reduced. Furthermore, it is possible to obtain a product with a uniform dryness and a constant degree of dryness with little variation. In addition, since a group of heat exchanger tubes is installed in the annular part of the spouted bed dryer, the material to be dried can be heated and dried separately from the drying by the jet gas. It can be reliably and easily dried to a predetermined degree of dryness in a short period of time.

また、噴流層乾燥器および移動層乾燥内部に被乾燥物の
残留する個所がないため、長時間高温ガスにさらされて
変質や変色して品質が低下することがない。
In addition, since there are no places in the spouted bed dryer or moving bed dryer where the material to be dried remains, there is no deterioration in quality due to deterioration or discoloration due to long-term exposure to high-temperature gas.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図は本発明の粒状物乾燥装置の縦断面図、第2図は
第1図のII −IIからみた断面図、第3図は第2図
の■−■からみた本発明の粒状物乾燥装置のガス供給管
と分散管の断面図、第4図は第1図のV−■からみた断
面図、P、5図は被乾燥物(ナイロンチップ)の乾燥工
程を示すグラフ、第6図は従来技術の粒状物乾燥器の断
面図である。 1・・・粒状物乾燥装置、  2・・・噴流層乾燥器、
3・・・原料供給ホツノ々、   4・・・サイクロン
、5・・・伝熱管群、     6・・・スロート部7
・・・陣笠、        9・・・ガス供給管、1
0・・・MUI物(ナイロンチップ)。 11・・・移動層乾燥器、   12・・・分散管、1
4・・・被乾燥物排出口、  15・・・/<ツフル。 16・・・ガス排出口、     A・・・アニユラ部
。 B・・・スパウト部。 特許出願人  宇部興産株式会社 第2図 j 4 コ n
FIG. 1 is a longitudinal sectional view of the granular material drying apparatus of the present invention, FIG. 2 is a sectional view taken from II-II in FIG. 1, and FIG. 3 is a sectional view of the granular material of the present invention seen from II-II in FIG. 4 is a sectional view of the gas supply pipe and dispersion pipe of the drying device, FIG. 4 is a sectional view taken from V-■ in FIG. The figure is a cross-sectional view of a prior art granule dryer. 1... Granular material dryer, 2... Spouted bed dryer,
3... Raw material supply hotspots, 4... Cyclone, 5... Heat exchanger tube group, 6... Throat part 7
...jinkasa, 9...gas supply pipe, 1
0...MUI product (nylon tip). 11... Moving bed dryer, 12... Dispersion tube, 1
4...Dried material discharge port, 15.../<Tuffle. 16... Gas discharge port, A... Annular part. B... Spout part. Patent applicant: Ube Industries, Ltd. Figure 2 j 4 Conn

Claims (2)

【特許請求の範囲】[Claims] (1)粒状物である被乾燥物を高温ガスを用いて、噴流
層で短かい時間で均一に加熱するとともに、一定程度乾
燥させ、然る後、この噴流層乾燥された被乾燥物を高温
ガスを用いて移動層で所望の滞留時間を以て乾燥させて
所定の乾燥度とする場合に、前記噴流層乾燥と、既に噴
流層乾燥を終えた被乾燥物の前記移動層乾燥とを同時に
並行させて行なわせることを特徴とする粒状物の乾燥方
法。
(1) The material to be dried, which is a granular material, is heated uniformly in a spouted bed for a short period of time using high-temperature gas, and dried to a certain extent, and then the material to be dried, which has been dried in the spouted bed, is When drying with gas for a desired residence time in a moving bed to achieve a predetermined degree of dryness, the spouted bed drying and the moving bed drying of the material to be dried that has already been spouted bed drying are performed simultaneously in parallel. A method for drying granular materials, characterized by:
(2)容器の下部に逆截頭円錐頭状部を有した2つの縦
型容器を配管にて接続し、上部縦型容器の内部下方に高
温の熱媒体を流す伝熱管群を設けるとともに、この伝熱
管群の上方位置に被乾燥物の供給口とガス排出口を設け
、さらに、下部縦型容器の内部下方に高温ガスの吹込管
を設け、前記縦型容器を噴流層乾燥部とし、後記縦型容
器を移動層乾燥器としたことを特徴とする粒状物乾燥装
置。
(2) Two vertical containers each having an inverted truncated conical head at the bottom of the container are connected by piping, and a group of heat transfer tubes is provided to flow a high temperature heat medium downward inside the upper vertical container. A supply port and a gas discharge port for the material to be dried are provided above the group of heat transfer tubes, and a high temperature gas blowing pipe is provided in the lower part of the lower vertical container, and the vertical container is used as a spouted bed drying section; A granular material drying device characterized in that a vertical container described later is used as a moving bed dryer.
JP3609389A 1989-02-17 1989-02-17 Method and device for drying granular body Pending JPH02217777A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP3609389A JPH02217777A (en) 1989-02-17 1989-02-17 Method and device for drying granular body

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP3609389A JPH02217777A (en) 1989-02-17 1989-02-17 Method and device for drying granular body

Publications (1)

Publication Number Publication Date
JPH02217777A true JPH02217777A (en) 1990-08-30

Family

ID=12460140

Family Applications (1)

Application Number Title Priority Date Filing Date
JP3609389A Pending JPH02217777A (en) 1989-02-17 1989-02-17 Method and device for drying granular body

Country Status (1)

Country Link
JP (1) JPH02217777A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPWO2009028568A1 (en) * 2007-08-28 2010-12-02 株式会社日本触媒 Method for producing water absorbent resin
JP2012180999A (en) * 2011-03-03 2012-09-20 Kawata Mfg Co Ltd Drying system and drying method
JP2015102255A (en) * 2013-11-22 2015-06-04 株式会社Ihi Hydrate solid drying device
JP2021505839A (en) * 2017-12-07 2021-02-18 ポール ワース エス.アー. Milling and drying plant containing drying hoppers and such

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPWO2009028568A1 (en) * 2007-08-28 2010-12-02 株式会社日本触媒 Method for producing water absorbent resin
JP5405304B2 (en) * 2007-08-28 2014-02-05 株式会社日本触媒 Method for producing water absorbent resin
JP2012180999A (en) * 2011-03-03 2012-09-20 Kawata Mfg Co Ltd Drying system and drying method
JP2015102255A (en) * 2013-11-22 2015-06-04 株式会社Ihi Hydrate solid drying device
JP2021505839A (en) * 2017-12-07 2021-02-18 ポール ワース エス.アー. Milling and drying plant containing drying hoppers and such
TWI803544B (en) * 2017-12-07 2023-06-01 盧森堡商保羅伍斯股份有限公司 Drying hopper and use of the drying hopper, as well as grinding and drying plant comprising such

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