JPH0137365B2 - - Google Patents

Info

Publication number
JPH0137365B2
JPH0137365B2 JP55008959A JP895980A JPH0137365B2 JP H0137365 B2 JPH0137365 B2 JP H0137365B2 JP 55008959 A JP55008959 A JP 55008959A JP 895980 A JP895980 A JP 895980A JP H0137365 B2 JPH0137365 B2 JP H0137365B2
Authority
JP
Japan
Prior art keywords
container
powder
volatile solvent
cosmetics
drying
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP55008959A
Other languages
Japanese (ja)
Other versions
JPS56108703A (en
Inventor
Hideo Nakamura
Tetsuyuki Oosawa
Masaaki Tobe
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shiseido Co Ltd
Original Assignee
Shiseido Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shiseido Co Ltd filed Critical Shiseido Co Ltd
Priority to JP895980A priority Critical patent/JPS56108703A/en
Publication of JPS56108703A publication Critical patent/JPS56108703A/en
Publication of JPH0137365B2 publication Critical patent/JPH0137365B2/ja
Granted legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/12Face or body powders for grooming, adorning or absorbing

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)

Description

【発明の詳細な説明】 本発明は、容器入り小型固形粉末化粧品に関す
るものである。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a compact solid powder cosmetic packaged in a container.

詳しくは、粉末化粧料を容器に充填・成型して
なる容器入り小型固形粉末化粧品、例えば固型白
粉、アイシヤドウ、頬紅、マスカラ等に関するも
のである。
Specifically, it relates to small-sized solid powder cosmetics in containers, such as solid white powder, eye shadow, blusher, mascara, etc., which are made by filling and molding powder cosmetics into containers.

従来、粉末化粧料を容器に充填・成型して容器
入り固形粉末化粧品とする場合には、粉末化粧料
を容器に充填し、各種成型機を用いて圧縮による
プレス成型を行つている。
BACKGROUND ART Conventionally, when filling and molding a powder cosmetic into a container to produce a container-packed solid powder cosmetic, the powder cosmetic is filled into a container and press-molded by compression using various molding machines.

しかしながら、一般に粉末化粧料は10〜25重量
%(以下、%は重量%を表す。)程度の油分しか
含有していないため流動性が劣ること並びに粉末
自体の付着性のために、約10g以下の小量、特に
0.05〜1g程度(因みに、アイシヤドウ等の試供
品は0.05g程度が充填されている。)の小量を定
量充填・成型することは著しく困難である。殊に
雲母等の板状形粉末を多く含む製品の場合には圧
縮によるプレス成型は極めて困難であり、10g以
上の通常の粉末化粧品の場合でも強く成型した場
合にはケーキングがし易くなり使用性の点におい
ても問題が生じる。
However, in general, powdered cosmetics contain only 10 to 25% by weight (hereinafter, % means weight%) of oil, resulting in poor fluidity and adhesion of the powder itself, making it less than about 10g. small amounts of, especially
It is extremely difficult to quantitatively fill and mold a small amount of about 0.05 to 1 g (incidentally, sample products such as Ishiyado are filled with about 0.05 g). Press molding by compression is extremely difficult especially in the case of products containing a large amount of plate-shaped powder such as mica, and even in the case of ordinary powder cosmetics weighing 10 g or more, caking becomes easier when molded strongly, making it easier to use. Problems also arise in this respect.

本発明者等は鋭意研究の結果、粉末化粧料に揮
発性溶剤を混合してスラリー状にし、該スラリー
状物を容器に充填した後乾燥し、揮発性溶剤を揮
散させることによつて粉末化粧料を固型化すると
いう技術手段を採れば、粉末化粧料を極めて短時
間に効率よく充填・成型し得、しかも充填・成型
後の固型粉末化粧品の使用性も、パフへのとれが
極めて良好で従来のケーキングの問題も解消され
ることを知つた。
As a result of intensive research, the present inventors have found that powder cosmetics can be made by mixing powder cosmetics with a volatile solvent to form a slurry, filling the slurry into a container, drying it, and volatilizing the volatile solvent. By adopting the technical means of solidifying the powder, powder cosmetics can be efficiently filled and molded in an extremely short period of time, and the usability of the solid powder cosmetics after filling and molding is also extremely high. I found that it works well and eliminates the problems of traditional caking.

即ち、本発明は、粉末化粧料を揮発性溶剤(沸
点200℃以下)と混合してスラリー状にし、該ス
ラリー状物を容器に充填し、次いで乾燥して前記
揮発性溶剤を揮散させることによつて前記粉末化
粧料を固型化することを特徴とする容器入り小型
固形粉末化粧品の製造方法である。
That is, the present invention mixes a powdered cosmetic with a volatile solvent (boiling point 200°C or lower) to form a slurry, fills a container with the slurry, and then dries it to volatilize the volatile solvent. Therefore, the present invention is a method for producing a small-sized solid powder cosmetic packaged in a container, which is characterized by solidifying the powder cosmetic material.

次に本発明の構成、効果を説明する。 Next, the configuration and effects of the present invention will be explained.

本発明に使用する揮発性溶剤は、沸点200℃以
下のものであるが、化粧品に使用し得るものが、
好ましい。例えば、エチルアルコール或はイツプ
ロピルアルコール等のような低沸点アルコール、
アイソパー等のような揮発性炭化水素等がある。
アイソパーは石油系炭化水素の合成油で、その主
成分はヘキサン或はイソパラフインであり、米国
のHumble Oil & Refining Company(ハンブ
ル オイル アンド リフアイニング カンパニ
ー)製造の商品名である。例えばアイソパーAの
沸点は66〜70℃、アイソパーEの沸点は116〜143
℃、アイソパーHの沸点は171〜193℃である。
The volatile solvent used in the present invention has a boiling point of 200°C or less, but those that can be used in cosmetics include
preferable. For example, low-boiling alcohols such as ethyl alcohol or ispropyl alcohol,
There are volatile hydrocarbons such as Isopar etc.
Isopar is a petroleum hydrocarbon synthetic oil whose main component is hexane or isoparaffin, and is a trade name manufactured by Humble Oil & Refining Company in the United States. For example, the boiling point of Isopar A is 66-70℃, and the boiling point of Isopar E is 116-143℃.
°C, the boiling point of Isopar H is 171-193 °C.

上記揮発性溶剤の添加量は対象とする粉末化粧
料の吸液量等によつて異なるが通常、粉末化粧料
に対し50〜150%添加される。50%以下である場
合には乾燥後にひび割れが発生し易く、150%以
上であると乾燥時間が長くなり、また、乾燥後の
中味の減量、耐衝撃性の低下等の問題が生じる。
The amount of the volatile solvent added varies depending on the liquid absorption amount of the target powder cosmetic, but it is usually added in an amount of 50 to 150% of the powder cosmetic. If it is less than 50%, cracks are likely to occur after drying, and if it is more than 150%, drying time becomes longer and problems such as loss of content after drying and reduction in impact resistance occur.

本発明による充填成型工程は、次の通りであ
る。
The filling and molding process according to the present invention is as follows.

粉末化粧料 揮発性溶剤―― 〔撹拌混合〕 ―― 〔脱気〕 ―― 〔充填〕 ―― 〔乾燥〕 揮発性溶剤 粉末化粧料に揮発性溶剤を添加し、において
プロペラ撹拌を行い脱気した後()、定量充填
機により充填し()、乾燥して揮発性溶剤を揮
散させる()。乾燥はエタノール、イソプロピ
ルアルコール、ヘキサン等の比較的低沸点溶剤の
場合には温風槽又はランプ照射により40〜70℃で
乾燥し、揮発性分岐炭化水素のような比較的高沸
点の溶剤の場合には減圧で乾燥する。
Powdered cosmetics Volatile solvent -- [Stirring and mixing] --- [Deaeration] --- [Filling] --- [Drying] Volatile solvent A volatile solvent was added to the powdered cosmetics and degassed by stirring with a propeller. After that (), it is filled with a quantitative filling machine () and dried to volatilize the volatile solvent (). Drying is performed at 40 to 70°C using a hot air bath or lamp irradiation in the case of relatively low boiling point solvents such as ethanol, isopropyl alcohol, and hexane, and in the case of relatively high boiling point solvents such as volatile branched hydrocarbons. Dry under reduced pressure.

上記の通りの本発明における工程では、従来法
の如く成型機を用いる圧縮によるプレス工程を経
る必要がない。
In the process of the present invention as described above, there is no need to go through a press process using compression using a molding machine as in the conventional method.

従来の圧縮によるプレス工程を採る場合には、
例えば2gの容器入り固型粉末化粧品5万個を製
造するのに5日間要したものが1日で成型が可能
となり、極めて効率がよい。
When using the conventional compression press process,
For example, what used to take 5 days to produce 50,000 solid powder cosmetics in 2g containers can now be molded in one day, which is extremely efficient.

また、従来法に比較して中皿等を使用せずに容
器に直接充填が可能となる効果がある。
Moreover, compared to the conventional method, there is an effect that the container can be directly filled without using an inner plate or the like.

更に、本発明による場合には、容器内の固型粉
末化粧品は揮発性溶剤の揮散によつて多孔質とな
つており、このため使用時におけるパフや刷子、
チツプ等へのとれが極めて良好であり、またケー
キングの問題も生じないという利点がある。
Furthermore, in the case of the present invention, the solid powder cosmetic in the container becomes porous due to the volatilization of the volatile solvent, and therefore, it is difficult to use the powder with a puff or brush during use.
It has the advantage that it adheres extremely well to chips, etc., and does not cause any caking problems.

次に本発明を実施例によつて説明する。 Next, the present invention will be explained with reference to examples.

実施例 1 アイシヤドウ 重量部 雲母 59.3 パール剤 15.0 無機顔料 15.0 ラノリン 4.5 スクワラン 4.5 界面活性剤 1.0 防腐剤 0.5 香料 0.2 イソプロピルアルコール 100.0 上記〜の粉末部に〜の油分、界面活性
剤、防腐剤、香料を添加し、の揮発性溶剤を加
えて充分に撹拌し脱気してスラリー状物とする。
次に上記スラリー状物を定量充填機により容器1
個当り0.1g宛充填し、60℃の温風槽による乾燥
工程を経て、製品を得る。
Example 1 Eye shadow Part by weight Mica 59.3 Pearl agent 15.0 Inorganic pigment 15.0 Lanolin 4.5 Squalane 4.5 Surfactant 1.0 Preservative 0.5 Fragrance 0.2 Isopropyl alcohol 100.0 Add the oil, surfactant, preservative, and fragrance of ~ to the powder part of ~ above Then, add a volatile solvent, stir thoroughly, and degas to form a slurry.
Next, the slurry-like material is poured into a container 1 using a quantitative filling machine.
Fill each piece to 0.1g and go through a drying process in a hot air tank at 60°C to obtain the product.

なお、乾燥工程において充填品表面にひび割れ
が生じる場合には、必要に応じ、充填直後紙又は
樹脂等を充填品の表面に置き、中味と密着させた
後乾燥することもできる。
If cracks occur on the surface of the filled product during the drying process, if necessary, paper or resin may be placed on the surface of the filled product immediately after filling to bring it into close contact with the contents, followed by drying.

実施例 2 固型白粉 重量部 雲母 50.0 タルク 2.0 二酸化チタン 15.0 酸化鉄(赤黄) 20.4 ラノリン 3.0 イソプロピルミリステート 5.5 界面活性剤 3.7 防腐剤 0.1 香料 0.3 アイソパーH 50.0 実施例1と同様の工程を経て100mmHgで減圧
乾燥し、容器1個当り1g入りの製品を得る。
Example 2 Solid white powder Parts by weight Mica 50.0 Talc 2.0 Titanium dioxide 15.0 Iron oxide (red and yellow) 20.4 Lanolin 3.0 Isopropyl myristate 5.5 Surfactant 3.7 Preservative 0.1 Fragrance 0.3 Isopar H 50.0 100 mmHg through the same process as Example 1 Dry under reduced pressure to obtain a product containing 1 g per container.

実施例 3 マスカラ 重量部 酸化鉄(黒) 30.0 カオリン 20.0 タルク 38.3 ラノリン 5.0 ワセリン 4.0 界面活性剤 2.0 防腐剤 0.5 香料 0.2 エチルアルコール 150.0 実施例1と同様の工程を経て、容器1個当り2
g入りの製品を得る。
Example 3 Mascara Weight parts Iron oxide (black) 30.0 Kaolin 20.0 Talc 38.3 Lanolin 5.0 Vaseline 4.0 Surfactant 2.0 Preservative 0.5 Fragrance 0.2 Ethyl alcohol 150.0 Through the same process as in Example 1, 2 per container
Obtain a product containing g.

実施例 4 頬 紅 重量部 タルク 51.7 雲母 15.0 パール剤 15.0 無機顔料 10.0 ラノリン 1.0 流動パラフイン 6.0 界面活性剤 0.7 防腐剤 0.1 香料 0.5 アイソパーA 100.0 実施例1と同様の工程を経て容器1個当り0.5
g入りの製品を得る。
Example 4 Cheek blush Parts by weight Talc 51.7 Mica 15.0 Pearl agent 15.0 Inorganic pigment 10.0 Lanolin 1.0 Liquid paraffin 6.0 Surfactant 0.7 Preservative 0.1 Fragrance 0.5 Isopar A 100.0 0.5 per container through the same process as Example 1
Obtain a product containing g.

Claims (1)

【特許請求の範囲】[Claims] 1 2g以下の粉末化粧料を該化粧料の50〜150
重量%の揮発性溶剤(沸点200℃以下)と混合し
てスラリー状にし、脱気して容器に充填し、次い
で乾燥して前記揮発性溶剤を揮散させることを特
徴とする容器入り小型固形粉末化粧品。
1 2g or less of powdered cosmetics
Small solid powder packed in a container, characterized in that it is mixed with % by weight of a volatile solvent (boiling point 200°C or less) to form a slurry, deaerated and filled into a container, and then dried to volatilize the volatile solvent. cosmetics.
JP895980A 1980-01-29 1980-01-29 Production of caked powder cosmetic in vessel Granted JPS56108703A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP895980A JPS56108703A (en) 1980-01-29 1980-01-29 Production of caked powder cosmetic in vessel

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP895980A JPS56108703A (en) 1980-01-29 1980-01-29 Production of caked powder cosmetic in vessel

Publications (2)

Publication Number Publication Date
JPS56108703A JPS56108703A (en) 1981-08-28
JPH0137365B2 true JPH0137365B2 (en) 1989-08-07

Family

ID=11707202

Family Applications (1)

Application Number Title Priority Date Filing Date
JP895980A Granted JPS56108703A (en) 1980-01-29 1980-01-29 Production of caked powder cosmetic in vessel

Country Status (1)

Country Link
JP (1) JPS56108703A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007209676A (en) * 2006-02-13 2007-08-23 Key Tranding Co Ltd Cosmetic container

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JPS56127305A (en) * 1980-02-22 1981-10-06 Yoshida Kogyo Kk <Ykk> Filling and solidifying method of cosmetic
US4337859A (en) * 1980-04-21 1982-07-06 Kolmar Laboratories Inc. Method of producing a cosmetic product containing a powder cake
JPS58203908A (en) * 1982-05-24 1983-11-28 Shiseido Co Ltd Solid cosmetic
JPS6067405A (en) * 1983-09-26 1985-04-17 Shiseido Co Ltd Production of multicolor solid powder cosmetic
JPS6067408A (en) * 1983-09-26 1985-04-17 Shiseido Co Ltd Production of multicolor solid powder cosmetic
JPS60172917A (en) * 1984-02-16 1985-09-06 Shiseido Co Ltd Production of solid powdery cosmetic
JPS60243006A (en) * 1984-05-17 1985-12-03 Asanuma Sogyo Kk Production of powdery solid cosmetic
GB2184587A (en) * 1985-10-28 1987-06-24 Ritz Group Ltd Charles Apparatus and method for display and sampling of solid cosmetics
US5566693A (en) * 1986-06-17 1996-10-22 Color Prelude, Inc. Fragrance sampler
US5690130A (en) * 1986-06-17 1997-11-25 Color Prelude Inc. Cosmetic sampler with integral applicator
US4751934A (en) * 1986-06-17 1988-06-21 Alford Industries, Inc. Cosmetic sampler
US5192386A (en) * 1986-06-17 1993-03-09 Alford Industries Inc. Method of making a cosmetic sampler
US5799675A (en) * 1997-03-03 1998-09-01 Color Prelude, Inc. Screen printed product sampler in hermetically sealed package
US6190730B1 (en) 1998-05-22 2001-02-20 Color Prelude, Inc. Cosmetic sampler with sample screen printed on film
US6006916A (en) * 1998-06-12 1999-12-28 Color Prelude, Inc. Cosmetic sampler with applicator backing
TW513309B (en) 1998-07-01 2002-12-11 Kao Corp Powder-based solid cosmetic composition and preparation process thereof
JP3850612B2 (en) 1999-12-28 2006-11-29 花王株式会社 Solid powder cosmetic
KR20030008373A (en) * 2001-06-11 2003-01-29 (주)피티엘 Method for preparation of binder-free pressed powder and cosmetic compositions made thereby
KR100416343B1 (en) * 2002-03-25 2004-01-31 한국화장품주식회사 Multi-colored granule pressed powder make-up cosmetic composition and method of producing the same
JP3752187B2 (en) * 2002-03-25 2006-03-08 株式会社コーセー Solid powder cosmetic
JP4484649B2 (en) * 2004-09-24 2010-06-16 株式会社資生堂 Method for producing solid powder makeup cosmetics
JP5110916B2 (en) * 2007-03-05 2012-12-26 花王株式会社 Method for producing solid powder cosmetic
KR100894058B1 (en) 2007-08-20 2009-04-21 주식회사 엘지생활건강 Method for manufacturing powder cake and apparatus thereof
JP5558061B2 (en) * 2009-09-18 2014-07-23 日本メナード化粧品株式会社 Solid powder cosmetic
JP5588658B2 (en) * 2009-11-12 2014-09-10 紀伊産業株式会社 Method for producing solid powder cosmetic
JP2012149005A (en) * 2011-01-19 2012-08-09 Shiseido Co Ltd Makeup cosmetic
JP2012184211A (en) * 2011-03-08 2012-09-27 Fujifilm Corp Foundation cosmetic and method for producing the same
JP2012214420A (en) * 2011-03-31 2012-11-08 Naris Cosmetics Co Ltd Powder solid cosmetic
FR2998781B1 (en) * 2012-12-04 2014-11-21 Oreal SOLID COSMETIC COMPOSITION IN THE FORM OF POWDER PRESSED
JP6199984B2 (en) 2012-12-04 2017-09-20 ロレアル Solid powdery cosmetic composition

Citations (1)

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Publication number Priority date Publication date Assignee Title
JPS54163831A (en) * 1978-06-16 1979-12-26 Shiseido Co Ltd Powdery makeeup cosmetics

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS54163831A (en) * 1978-06-16 1979-12-26 Shiseido Co Ltd Powdery makeeup cosmetics

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007209676A (en) * 2006-02-13 2007-08-23 Key Tranding Co Ltd Cosmetic container

Also Published As

Publication number Publication date
JPS56108703A (en) 1981-08-28

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