JPH01123616A - Washing tower - Google Patents

Washing tower

Info

Publication number
JPH01123616A
JPH01123616A JP62280491A JP28049187A JPH01123616A JP H01123616 A JPH01123616 A JP H01123616A JP 62280491 A JP62280491 A JP 62280491A JP 28049187 A JP28049187 A JP 28049187A JP H01123616 A JPH01123616 A JP H01123616A
Authority
JP
Japan
Prior art keywords
cleaning
scrubbing
exhaust gas
tower
chambers
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP62280491A
Other languages
Japanese (ja)
Inventor
Kiyoshi Tominari
富成 清
Yukimasa Tamura
田村 行正
Shinichiro Suzuki
鈴木 愼一朗
Makoto Tanaka
誠 田中
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Japan Oxygen Co Ltd
Nippon Sanso Corp
International Business Machines Corp
Original Assignee
Japan Oxygen Co Ltd
Nippon Sanso Corp
International Business Machines Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Japan Oxygen Co Ltd, Nippon Sanso Corp, International Business Machines Corp filed Critical Japan Oxygen Co Ltd
Priority to JP62280491A priority Critical patent/JPH01123616A/en
Publication of JPH01123616A publication Critical patent/JPH01123616A/en
Pending legal-status Critical Current

Links

Abstract

PURPOSE: To eliminate the need for dilution of waste gases and to reduce the size of the apparatus by segmenting and forming the inside of a scrubbing column to plural scrubbing chambers and disposing scrubbing liquid introducing ports to the upper parts of the respective scrubbing chambers and waste gas introducing ports of respective semiconductor producing apparatus to the lower parts thereof. CONSTITUTION: The waste gases W from the respective semiconductor producing apparatus 14 are introduced from discharge ports 23 through the waste gas introducing ports 24 communicating therewith into the respective scrubbing chambers 13 and come into contact with the scrubbing liquids F introduced from the scrubbing liquid introducing ports 25, by which SiH4 , etc., are removed. The waste gases are then discharged from gas outlet pipes 19. The scrubbing liquids F are led out of piping 21 together with the scrubbing liquids from another scrubbing chambers 13 in scrubbing liquid paths 20 and are circulated by a pump 22. Since the scrubbing column 11 is segmented to the respective scrubbing chambers 13 by barriers 15, the waste gases W before the scrubbing are not mixed with the scrubbed waste gases and since there is no danger of combustion or explosion, the need for the dilution is eliminated and the size of the apparatus is reduced.

Description

【発明の詳細な説明】 〔産業上の利用分野〕 本発明は、複数台の半導体製造装置からそれぞれ別個に
排出される排ガスの除害を行う洗浄塔に関するものであ
る。
DETAILED DESCRIPTION OF THE INVENTION [Field of Industrial Application] The present invention relates to a cleaning tower that removes harmful substances from exhaust gas discharged separately from a plurality of semiconductor manufacturing apparatuses.

〔従来の技術〕[Conventional technology]

プラズマケミカルベーパーデポジット(P−CVD)等
の半導体製造装置から排出される排ガス中には、シラン
、ジボラン、アルシン、ホスフィン、ジクロルシラン、
トリクロルシラン等の有毒。
The exhaust gas emitted from semiconductor manufacturing equipment such as plasma chemical vapor deposition (P-CVD) contains silane, diborane, arsine, phosphine, dichlorosilane,
Toxic substances such as trichlorosilane.

自燃性のガスが含まれているため、大気放出前に除去す
る必要がある。この除去手段として、気液接触を行う洗
浄塔内で上記シラン等を含む排ガスをアルカリ水溶液と
接触させ、アルカリ水溶液との反応及び化学吸着により
シラン等の濃度を許容濃度以下にまで除害して排気する
ものが知られている。
Contains pyrophoric gases and must be removed before release into the atmosphere. As a means of removing this, the exhaust gas containing the silane, etc. is brought into contact with an alkaline aqueous solution in a cleaning tower that performs gas-liquid contact, and the concentration of the silane, etc. is reduced to below the permissible concentration by reaction with the alkaline aqueous solution and chemical adsorption. It is known what exhausts.

第4図及び第5図は、複数台の半導体製造装置から排出
される排ガスの除害処理を行う従来の洗浄塔を示すもの
である。
FIGS. 4 and 5 show a conventional cleaning tower that performs detoxification treatment on exhaust gas discharged from a plurality of semiconductor manufacturing apparatuses.

洗浄塔1は、内部に充填された充填剤2の下方から排ガ
スWを導入するとともに、上方から洗浄液Fを導入して
両者を充填剤2中で接触させ、排ガスW中の有害物質を
除去するもので、洗浄液Fは、所定量が洗浄塔1の底部
に貯留されてポンプ3により循環している。一方複数台
の半導体製造装置から排出された排ガスWは、第4図に
示すように、ヘッダー管4で集合した後に洗浄塔1に導
入されるか、あるいは第5図に示すように、それぞれ独
立した配管5,5で洗浄塔1の下部に導入され、洗浄液
Fにより除害されて洗浄塔1の上部から排出される。
The cleaning tower 1 introduces the exhaust gas W from below the filler 2 filled inside, and also introduces the cleaning liquid F from above to bring them into contact in the filler 2, thereby removing harmful substances in the exhaust gas W. A predetermined amount of the cleaning liquid F is stored at the bottom of the cleaning tower 1 and circulated by a pump 3. On the other hand, exhaust gases W discharged from multiple semiconductor manufacturing devices are either collected in a header pipe 4 and then introduced into the cleaning tower 1, as shown in FIG. 4, or are collected independently, as shown in FIG. The water is introduced into the lower part of the cleaning tower 1 through pipes 5, 5, which are removed by the cleaning liquid F, and discharged from the upper part of the cleaning tower 1.

〔発明が解決しようとする問題点〕[Problem that the invention seeks to solve]

しかしながら、上述のものでは、運転時間や使用ガスの
異なる複数台の半導体製造装置からの排ガスを洗浄前に
混合するため、ある装置で有毒性。
However, in the above-mentioned method, exhaust gases from multiple semiconductor manufacturing equipment with different operating times and gas usage are mixed before cleaning, so some equipment may be toxic.

自燃性ガス(シランSL 84等)を使用中に、他の装
置からの空気あるいは酸素ガスを含むガスが導入すると
、両者の混合により燃焼、爆発の危険性がある。さらに
他の装置で水素ガスを使用している場合には、大爆発の
危険性も考慮しなければならない。このような危険を回
避するために、窒素ガス等の不活性ガスで排ガスを希釈
することが考えられているが、爆発下限界にまで希釈す
るには大量の不活性ガスが必要であり、また希釈により
排ガスの総置が増すため、極端に大きな洗浄塔が必要と
なる。
If a gas containing air or oxygen gas from another device is introduced while a self-combustible gas (such as Silane SL 84) is in use, there is a risk of combustion or explosion due to the mixture of the two. Furthermore, if hydrogen gas is used in other equipment, the risk of a large explosion must be considered. In order to avoid such dangers, diluting the exhaust gas with inert gas such as nitrogen gas has been considered, but diluting the exhaust gas to the lower explosive limit requires a large amount of inert gas, and Dilution increases the total amount of exhaust gas, requiring an extremely large scrubbing tower.

そこで本発明は、大量の不活性ガスによる希釈を必要と
せずに上記爆発の危険性をなくし、さらに小型に形成す
ることのできる洗浄塔を提供することを目的としている
SUMMARY OF THE INVENTION Therefore, an object of the present invention is to provide a cleaning tower that eliminates the risk of explosion without requiring dilution with a large amount of inert gas, and that can be made smaller.

〔問題点を解決するための手段〕[Means for solving problems]

上記した目的を達成するために本発明は、複数台の半導
体製造装置から排出される排ガスの除害を行う洗浄塔に
おいて、該洗浄塔内を、複数の洗浄室に区画形成すると
ともに、各洗浄室の上部に排ガスの除害を行う洗浄液を
導入する洗浄隋導入口を、また各洗浄室の下部に各半導
体製造装置の排ガスの排出口にそれぞれ連通する排ガス
導入口を設けたことを特徴とする。
In order to achieve the above object, the present invention provides a cleaning tower for detoxifying exhaust gas discharged from a plurality of semiconductor manufacturing equipment, in which the interior of the cleaning tower is divided into a plurality of cleaning chambers, and each cleaning The cleaning chamber is characterized by having a cleaning inlet in the upper part of the chamber for introducing a cleaning liquid for removing harmful substances from the exhaust gas, and an exhaust gas inlet in the lower part of each cleaning chamber to communicate with the exhaust gas outlet of each semiconductor manufacturing equipment. do.

〔作 用〕[For production]

従って、各半導体製造装置から排出された排ガスは、そ
れぞれ別の洗浄室に導入されて洗浄されるので、排ガス
の混合による爆発の危険性を回避することができる。
Therefore, the exhaust gas discharged from each semiconductor manufacturing device is introduced into separate cleaning chambers and cleaned, thereby avoiding the risk of explosion due to mixture of exhaust gases.

〔実施例〕〔Example〕

以下、本発明の一実施例を図面に基づいて説明する。 Hereinafter, one embodiment of the present invention will be described based on the drawings.

第1図は洗浄塔の断面正面図、第2図は洗浄塔及び半導
体製造装置を示す平面図、第3図は洗浄塔の側面図であ
って、洗浄塔11内には、充填剤12が充填された複数
の洗浄室13.13が形成されている。
FIG. 1 is a cross-sectional front view of the cleaning tower, FIG. 2 is a plan view showing the cleaning tower and semiconductor manufacturing equipment, and FIG. 3 is a side view of the cleaning tower. A plurality of filled cleaning chambers 13.13 are formed.

上記洗浄室13は、半導体製造装置14.14の台数に
応じて形成されるもので、垂直方向に設けられた隔壁1
5.15により区画形成されている。
The cleaning chamber 13 is formed according to the number of semiconductor manufacturing apparatuses 14, 14, and has partition walls 1 provided in the vertical direction.
5.15.

この隔壁15は、上下両端部を洗浄塔11の天板16及
び底板17と離間して設けられており、天板16と隔壁
15の上端との間を除害されたガスを排出するためのガ
ス流路18とし、天板16の中央部に設けられたガス出
口管19から除害されたガスを排出している。また底板
17と隔壁15の下端との間は、洗浄液Fのみを連通さ
せる洗浄液流路20としており、各洗浄室13の底部に
溜る洗浄液Fを、洗浄塔11の一側に設けられた配管2
1からポンプ22を介して洗浄塔11の上部に圧送し、
各洗浄室13内に循環させている。
This partition wall 15 is provided with its upper and lower ends separated from the top plate 16 and bottom plate 17 of the cleaning tower 11, and is used to discharge the detoxified gas between the top plate 16 and the upper end of the partition wall 15. The detoxified gas is discharged from a gas flow path 18 and a gas outlet pipe 19 provided at the center of the top plate 16. Also, between the bottom plate 17 and the lower end of the partition wall 15 is a cleaning liquid passage 20 that allows only the cleaning liquid F to communicate, and the cleaning liquid F accumulated at the bottom of each cleaning chamber 13 is transferred to a pipe 2 provided on one side of the cleaning tower 11.
1 to the upper part of the washing tower 11 via the pump 22,
It is circulated within each cleaning chamber 13.

そして各洗浄室13の下部には、各半導体製造装置14
の排ガスWの排出口23にそれぞれ連通する排ガス導入
口24が設けられており、また各洗浄室13の上部には
、排ガスWの除害を行う洗浄液E′4i−導入する洗浄
液導入口25が設けられている。
In the lower part of each cleaning chamber 13, each semiconductor manufacturing device 14 is provided.
An exhaust gas inlet 24 is provided which communicates with the exhaust outlet 23 of the exhaust gas W, and in the upper part of each cleaning chamber 13, a cleaning liquid inlet 25 for introducing the cleaning liquid E'4i which removes harmful substances from the exhaust gas W is provided. It is provided.

各半導体製造装置14から排出された排ガスWは、それ
ぞれの排出口23から、それぞれ連通している排ガス導
入口24を通って各洗浄室13内に尋人され、洗浄室1
3内を上昇して上方から流下してくる洗浄液Fと接触し
、除害された後にガス流路18で他の洗浄室13で除害
されたガスと共にガス出口管19から排出される。
Exhaust gas W discharged from each semiconductor manufacturing device 14 is discharged from each exhaust port 23 into each cleaning chamber 13 through an exhaust gas inlet 24 that communicates with the cleaning chamber 1.
3 and comes into contact with the cleaning liquid F flowing down from above, and after being detoxified, it is discharged from the gas outlet pipe 19 along with the gas detoxified in the other cleaning chambers 13 through the gas flow path 18.

また各洗浄室13を流下する洗浄液Fは、洗浄液流路2
0で他の洗浄室13を流下した洗浄液Fと共に配管21
から導出され、ポンプ22で上方に圧送され、各洗浄室
13内に分岐して洗浄液導入口25から導入される。
Further, the cleaning liquid F flowing down each cleaning chamber 13 is connected to the cleaning liquid flow path 2.
The pipe 21 along with the cleaning liquid F that flowed down the other cleaning chamber 13 at 0
The cleaning liquid is drawn out from the cleaning chamber 13, is forced upward by the pump 22, is branched into each cleaning chamber 13, and is introduced from the cleaning liquid inlet 25.

このように各半導体製造装置14から排出される排ガス
Wをそれぞれ別の洗浄室13に導入して洗浄し、排ガス
Wの除害を行うので洗浄前の排ガスWが混合することが
なく、燃焼や爆発の虞がない。また排ガスWを大量の不
活性ガスで希釈する必要がないので、洗浄塔11に導入
される排ガスWのIaffiが多くなることがなく、洗
浄塔11を小型に形成することができる。
In this way, the exhaust gases W discharged from each semiconductor manufacturing equipment 14 are introduced into separate cleaning chambers 13 and cleaned, and the exhaust gases W are detoxified. Therefore, the exhaust gases W before cleaning are not mixed, and combustion and combustion are prevented. There is no risk of explosion. Further, since there is no need to dilute the exhaust gas W with a large amount of inert gas, the Iaffi of the exhaust gas W introduced into the cleaning tower 11 does not increase, and the cleaning tower 11 can be formed in a small size.

さらに各半導体!Fj造装置に個別に洗浄塔を設けるの
に比べて洗浄液を圧送するポンプが1台でよく、除害さ
れた後に排出されるガスの配管も1本でよいため、装置
のコストダウンが図れ、装置を小型に形成することで洗
浄液の量も少なくてよく、運転コストも低減できる。
More semiconductors! Compared to installing a separate cleaning tower in the FJ manufacturing equipment, only one pump is required to forcefully pump the cleaning liquid, and only one pipe is required for the gas that is discharged after detoxification, reducing the cost of the equipment. By making the device smaller, the amount of cleaning liquid can be reduced, and operating costs can also be reduced.

尚、洗浄塔の形状等は、円筒形等信の形状に形成するこ
ともできる。
Note that the shape of the washing tower can also be formed into a cylindrical shape or the like.

実験例 洗浄塔 外形寸法(WxDxHim) 1200x500x1940 反応部  4分割(4室)300m111角材    
質    PVC 洗浄液  20%苛性ソーダ水溶液 流徴  80 J / tm* 排カス流11140ノ/+nim p −cv。
Experimental example Washing tower external dimensions (WxDxHim) 1200x500x1940 Reaction section 4 divisions (4 chambers) 300m 111 square pieces
Quality PVC Cleaning liquid 20% caustic soda aqueous solution Flow rate 80 J/tm* Waste flow 11140 min/+nim p-cv.

型  式  多室型(4室) 使用ガス  SL Ha ・H2 p−cvoの各室と洗浄塔の各室をそれぞれ別配管によ
り接続するとともに、各P−CVDからの排ガスを窒素
ガスで希釈し、SLH++1度を5%以下として洗浄塔
の洗浄室に導入して洗浄・除害を行った。
Model Multi-chamber type (4 chambers) Gas used SL Ha ・H2 Each p-cvo chamber and each cleaning tower chamber are connected through separate piping, and the exhaust gas from each P-CVD is diluted with nitrogen gas. The SLH++1 degree was set to 5% or less and introduced into the cleaning chamber of the cleaning tower for cleaning and detoxification.

洗浄塔の出口部における排ガス中のSL 84濃度を測
定した結果、25 ppm以下に減少しており、ガス出
口管で排ガスが混合してもSL H4による燃焼、爆発
の危険性のないことが確認された。
As a result of measuring the SL 84 concentration in the exhaust gas at the outlet of the cleaning tower, it was found to have decreased to 25 ppm or less, confirming that there is no danger of combustion or explosion due to SL H4 even if the exhaust gas is mixed at the gas outlet pipe. It was done.

(発明の効果) 本発明は以上説明したように、洗浄塔内を複数の洗浄室
に区画形成し、各洗浄室にそれぞれ洗浄液導入口と排ガ
ス導入口を設けたから、洗浄前の排ガスが混合すること
がなくなり、燃焼や爆発の危険性がなくなる。これによ
り排ガスを人聞の不活性ガスで希釈する必要がなくなり
、排ガスの総量が多くなることがないので、洗浄塔を小
型に形成することができ、洗浄塔の建設コスト及び運転
コストの低減を図ることができる。
(Effects of the Invention) As explained above, in the present invention, the interior of the cleaning tower is divided into a plurality of cleaning chambers, and each cleaning chamber is provided with a cleaning liquid inlet and an exhaust gas inlet, so that the exhaust gas before cleaning is mixed. This eliminates the risk of combustion or explosion. This eliminates the need to dilute the flue gas with inert gas and does not increase the total amount of flue gas, allowing the cleaning tower to be made smaller and reducing the construction and operating costs of the cleaning tower. can be achieved.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図乃至第3図は本発明の一実施例を示すもので、第
1図は洗浄塔の断面正面図、第2図は洗浄塔及び半導体
製造装置を示す平面図、第3図は洗浄塔の側面図、第4
図及び第5図はそれぞれ従来の洗浄塔を示す説明図であ
る。 11・・・洗、浄塔  13・・・洗浄室  14・・
・半導体製造装fat   15・・・隔壁  18・
・・ガス流路19・・・ガス出口管  20・・・洗浄
液流路  22・・・ポンプ  24・・・排ガス導入
口  25・・・洗浄液導入口  F・・・洗浄液  
W・・・排ガス特 許 出 願 人 日本酸素株式会社
同        インターナショナルビジネス マシ
ーンズ コーポレーション
1 to 3 show one embodiment of the present invention, in which FIG. 1 is a cross-sectional front view of a cleaning tower, FIG. 2 is a plan view showing a cleaning tower and semiconductor manufacturing equipment, and FIG. 3 is a cleaning tower. Side view of the tower, No. 4
FIG. 5 and FIG. 5 are explanatory diagrams showing conventional cleaning towers, respectively. 11...Washing, purification tower 13...Washing room 14...
・Semiconductor manufacturing equipment fat 15...Partition wall 18・
...Gas flow path 19...Gas outlet pipe 20...Cleaning liquid flow path 22...Pump 24...Exhaust gas inlet 25...Cleaning liquid inlet F...Cleaning liquid
W...Exhaust gas patent applicant Nippon Sanso Co., Ltd. International Business Machines Corporation

Claims (1)

【特許請求の範囲】 1、複数台の半導体製造装置から排出される排ガスの除
害を行う洗浄塔において、該洗浄塔内を、複数の洗浄室
に区画形成するとともに、各洗浄室の上部に排ガスの除
害を行う洗浄液を導入する洗浄液導入口を、また各洗浄
室の下部に各半導体製造装置の排ガスの排出口にそれぞ
れ連通する排ガス導入口を設けたことを特徴とする洗浄
塔。 2、前記洗浄室は、洗浄塔内に垂直に設けられた複数の
隔壁により形成されるとともに、前記洗浄液導入口より
上方に、隣接する洗浄室と連通するガス流路を、また前
記排ガス導入口より下方に、各洗浄室内の底部に溜る洗
浄液のみを連通させる洗浄液流路を設けたことを特徴と
する特許請求の範囲第1項記載の洗浄塔。
[Claims] 1. In a cleaning tower that removes harmful substances from exhaust gas discharged from a plurality of semiconductor manufacturing equipment, the inside of the cleaning tower is divided into a plurality of cleaning chambers, and the upper part of each cleaning chamber is A cleaning tower characterized in that a cleaning liquid inlet for introducing a cleaning liquid for removing harmful substances from exhaust gas is provided, and an exhaust gas inlet is provided in the lower part of each cleaning chamber to communicate with the exhaust gas outlet of each semiconductor manufacturing device. 2. The cleaning chamber is formed by a plurality of partition walls installed vertically in the cleaning tower, and has a gas flow path communicating with the adjacent cleaning chamber above the cleaning liquid inlet, and also has a gas flow path connected to the exhaust gas inlet. 2. The cleaning tower according to claim 1, further comprising a cleaning liquid flow path that communicates only the cleaning liquid accumulated at the bottom of each cleaning chamber at a lower portion.
JP62280491A 1987-11-06 1987-11-06 Washing tower Pending JPH01123616A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP62280491A JPH01123616A (en) 1987-11-06 1987-11-06 Washing tower

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP62280491A JPH01123616A (en) 1987-11-06 1987-11-06 Washing tower

Publications (1)

Publication Number Publication Date
JPH01123616A true JPH01123616A (en) 1989-05-16

Family

ID=17625821

Family Applications (1)

Application Number Title Priority Date Filing Date
JP62280491A Pending JPH01123616A (en) 1987-11-06 1987-11-06 Washing tower

Country Status (1)

Country Link
JP (1) JPH01123616A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014178882A1 (en) * 2013-05-03 2014-11-06 Fluor Technologies Corporation Systems and methods for multi-celled gas processing
CN105311956A (en) * 2015-11-13 2016-02-10 中国化学工程第六建设有限公司 Packing-type catalytic desulfurization tower with reinforced concrete structure
US9333456B2 (en) 2013-05-03 2016-05-10 Fluor Technologies Corporation Systems and methods for multi-celled gas processing

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014178882A1 (en) * 2013-05-03 2014-11-06 Fluor Technologies Corporation Systems and methods for multi-celled gas processing
CN105392547A (en) * 2013-05-03 2016-03-09 氟石科技公司 Systems and methods for multi-celled gas processing
US9333456B2 (en) 2013-05-03 2016-05-10 Fluor Technologies Corporation Systems and methods for multi-celled gas processing
AU2013388102B2 (en) * 2013-05-03 2016-07-21 Fluor Technologies Corporation Systems and methods for multi-celled gas processing
US9975083B2 (en) 2013-05-03 2018-05-22 Fluor Technologies Corporation Systems and methods for multi-celled gas processing
CN105392547B (en) * 2013-05-03 2020-05-12 氟石科技公司 System and method for multi-unit gas processing
CN105311956A (en) * 2015-11-13 2016-02-10 中国化学工程第六建设有限公司 Packing-type catalytic desulfurization tower with reinforced concrete structure

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