JP7680434B2 - 流動層プロパン脱水素化反応器排出物から触媒を除去するための燃料油洗浄の使用方法 - Google Patents

流動層プロパン脱水素化反応器排出物から触媒を除去するための燃料油洗浄の使用方法 Download PDF

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JP7680434B2
JP7680434B2 JP2022516243A JP2022516243A JP7680434B2 JP 7680434 B2 JP7680434 B2 JP 7680434B2 JP 2022516243 A JP2022516243 A JP 2022516243A JP 2022516243 A JP2022516243 A JP 2022516243A JP 7680434 B2 JP7680434 B2 JP 7680434B2
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catalyst
oil
exhaust gas
filter
fuel oil
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JP2022547708A5 (https=
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ライアン ライナカ
ホセ マニュエル ウルキアガ
トリュック ヴー
ジェフリー ドナルド ケイトン
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ケロッグ ブラウン アンド ルート エルエルシー
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/90—Regeneration or reactivation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/02—Heat treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B01J38/12—Treating with free oxygen-containing gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/005—Separating solid material from the gas/liquid stream
    • B01J8/006—Separating solid material from the gas/liquid stream by filtration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0278—Feeding reactive fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1836—Heating and cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/02—Alkenes
    • C07C11/06—Propene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/32—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with formation of free hydrogen
    • C07C5/321—Catalytic processes
    • C07C5/322—Catalytic processes with metal oxides or metal sulfides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/32—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by dehydrogenation with formation of free hydrogen
    • C07C5/327—Formation of non-aromatic carbon-to-carbon double bonds only
    • C07C5/333—Catalytic processes
    • C07C5/3332—Catalytic processes with metal oxides or metal sulfides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/11—Purification; Separation; Use of additives by absorption, i.e. purification or separation of gaseous hydrocarbons with the aid of liquids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G31/00—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for
    • C10G31/09—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for by filtration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2247/00—Details relating to the separation of dispersed particles from gases, air or vapours by liquid as separating agent
    • B01D2247/04—Regenerating the washing fluid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D47/00—Separating dispersed particles from gases, air or vapours by liquid as separating agent
    • B01D47/14—Packed scrubbers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00761—Discharging
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00769—Details of feeding or discharging
    • B01J2208/00787—Bringing the solid in the form of a slurry before feeding it to the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00946—Features relating to the reactants or products
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00991—Disengagement zone in fluidised-bed reactors
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/70—Catalyst aspects
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/584—Recycling of catalysts

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Combustion & Propulsion (AREA)
  • Physics & Mathematics (AREA)
  • Water Supply & Treatment (AREA)
  • Thermal Sciences (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Filtration Of Liquid (AREA)
  • Catalysts (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
JP2022516243A 2019-09-13 2020-09-10 流動層プロパン脱水素化反応器排出物から触媒を除去するための燃料油洗浄の使用方法 Active JP7680434B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US16/570,029 2019-09-13
US16/570,029 US11117108B2 (en) 2019-09-13 2019-09-13 Use of a fuel oil wash to remove catalyst from a fluidized-bed propane dehydrogenation reactor effluent
PCT/US2020/050052 WO2021050631A1 (en) 2019-09-13 2020-09-10 Use of a fuel oil wash to remove catalyst from a fluidized-bed propane dehydrogenation reactor effluent

Publications (3)

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JP2022547708A JP2022547708A (ja) 2022-11-15
JP2022547708A5 JP2022547708A5 (https=) 2023-09-19
JP7680434B2 true JP7680434B2 (ja) 2025-05-20

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US (1) US11117108B2 (https=)
EP (1) EP4028154A4 (https=)
JP (1) JP7680434B2 (https=)
KR (1) KR20220087435A (https=)
CN (1) CN114364455A (https=)
MY (1) MY209056A (https=)
SA (1) SA522431929B1 (https=)
WO (1) WO2021050631A1 (https=)
ZA (1) ZA202202993B (https=)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11725153B2 (en) 2020-04-17 2023-08-15 Uop Llc Process and apparatus for recovering catalyst from a product stream
KR102841719B1 (ko) 2022-11-17 2025-08-04 한국에너지기술연구원 가압 기포유동층 촉매 재생시스템 및 그 운전방법

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5073249A (en) 1989-11-21 1991-12-17 Mobil Oil Corporation Heavy oil catalytic cracking process and apparatus
JP2004131736A (ja) 2002-10-10 2004-04-30 Kellogg Brawn & Root Inc 軽質オレフィンｆｃｃ流出物からの触媒回収
JP2008260713A (ja) 2007-04-12 2008-10-30 Sumitomo Chemical Co Ltd ろ過方法

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GB1107432A (en) * 1964-09-01 1968-03-27 Lummus Co Dehydrogenation process
US4312779A (en) * 1980-09-25 1982-01-26 Uop Inc. Recovery of catalysts
AU555438B2 (en) * 1984-01-04 1986-09-25 Mobil Oil Corp. Fcc process
US7356606B2 (en) 2004-03-12 2008-04-08 Kagi Corporation Dynamic web storefront technology
US7329790B2 (en) * 2004-04-15 2008-02-12 Uop Llc Wet scrubbing and recycle of effluent-contaminating catalyst particles in an oxygenate-to-olefin process
US7935650B2 (en) 2006-12-18 2011-05-03 Uop Llc Neutralization of quench stream in a process for handling catalyst from an oxygenate-to-olefin reaction
US20090325783A1 (en) 2008-06-30 2009-12-31 Myers Daniel N Oto quench tower catalyst recovery system utilizing a low temperature fluidized drying chamber
US8927799B2 (en) 2010-11-01 2015-01-06 Uop Llc Propane dehydrogenation process utilizing fluidized catalyst system
US9834496B2 (en) 2011-07-13 2017-12-05 Dow Global Technologies Llc Reactivating propane dehydrogenation catalyst
US9446364B2 (en) * 2012-02-23 2016-09-20 Kellogg Brown & Root Llc Surge drum mixing system
CN102921470B (zh) * 2012-10-23 2014-04-02 南京理工大学 聚四氟乙烯粒子回收含氟催化剂的方法
KR101653457B1 (ko) * 2014-11-26 2016-09-02 주식회사 효성 탈수소화 공정에서의 촉매 재생 방법
US10059645B2 (en) * 2015-07-02 2018-08-28 Saudi Arabian Oil Company Systems and methods for producing propylene
CN109791018A (zh) * 2016-08-25 2019-05-21 沙特基础工业全球技术公司 用于丙烷脱氢反应器流出物的低温以上的分离方法
AR111992A1 (es) * 2017-06-19 2019-09-11 Dow Global Technologies Llc Sistemas de reactor que comprenden el reciclado de fluidos
WO2020191190A1 (en) * 2019-03-21 2020-09-24 Kellogg Brown & Root Llc System and method for catalyst removal from mto effluent
SG11202110419TA (en) 2019-03-21 2021-10-28 Kellogg Brown & Root Llc Processes for catalytic paraffin dehydrogenation and catalyst recovery

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5073249A (en) 1989-11-21 1991-12-17 Mobil Oil Corporation Heavy oil catalytic cracking process and apparatus
JP2004131736A (ja) 2002-10-10 2004-04-30 Kellogg Brawn & Root Inc 軽質オレフィンｆｃｃ流出物からの触媒回収
JP2008260713A (ja) 2007-04-12 2008-10-30 Sumitomo Chemical Co Ltd ろ過方法

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Publication number Publication date
WO2021050631A1 (en) 2021-03-18
CN114364455A (zh) 2022-04-15
KR20220087435A (ko) 2022-06-24
ZA202202993B (en) 2022-11-30
US11117108B2 (en) 2021-09-14
MY209056A (en) 2025-06-18
JP2022547708A (ja) 2022-11-15
SA522431929B1 (ar) 2024-04-24
EP4028154A4 (en) 2023-09-20
US20210077967A1 (en) 2021-03-18
EP4028154A1 (en) 2022-07-20

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