JP6690788B1 - ERW steel pipe, its manufacturing method, and steel pipe pile - Google Patents

Abstract

An electric resistance welded steel pipe having a base material portion and a welded portion in the axial direction of the pipe, wherein the component composition of the base material portion has a specific component composition and the plate thickness of the base material portion is t. In the steel structure at a position 1 / 4t deeper than the plate thickness t from the outer surface of the bainite, the area ratio of bainite is 60% or more, the average effective grain size of bainite is 20.0 μm or less in the average circle equivalent diameter, and The average aspect ratio is 0.1 to 0.8, the tensile strength in the tube axis direction is 590 MPa or more, the 0.2% proof stress is 450 MPa or more, and the yield ratio is 80 to 90%. Electric-resistance welded steel pipe having a Charpy absorbed energy of 70 J or more at −30 ° C. and a residual stress of 250 MPa or less in the axial direction of the outer surface of the steel pipe in the base material portion and a manufacturing method thereof, and a steel pipe Pile.

Description

  The present invention relates to an electric resistance welded steel pipe suitable for a steel pipe pile used as a foundation of a structure, a method for manufacturing the same, and a steel pipe pile. In particular, the present invention uses a hot-rolled steel sheet (hot-rolled steel strip) as a raw material, and improves the strength, toughness, and optimization of the yield ratio of an electric resistance welded steel pipe obtained by cold-roll forming the raw material into a pipe. , And the improvement of buckling resistance.

  In recent years, in response to large-scale earthquakes, there has been a strong demand for steel pipe piles used as the foundation of structures to have higher strength and improved deformation energy absorption capacity. Generally, in order to improve the deformation energy absorption capacity of a steel pipe, it is effective to use a steel material having high tensile strength and a low yield ratio. However, it is difficult for the steel pipe pile to excessively reduce the yield ratio in the pipe axial direction from the viewpoint of suppressing the deformation of the steel pipe during pile driving. Furthermore, high low temperature toughness is also required for steel pipe piles used especially in cold regions. In addition, high buckling resistance is required to withstand deformation such as an earthquake.

  Patent Document 1 describes a method for manufacturing an earthquake-resistant welded steel pipe having excellent local buckling resistance. In patent document 1, C: 0.03-0.15% and Mn: 1.0-2.0% are contained by weight%, Cu: 0.05-0.50%, Ni: 0.05. .About.0.50%, Cr: 0.05 to 0.50%, Mo: 0.05 to 0.50%, Nb: 0.005 to 0.10%, V: 0.005 to 0.10%, Ti: Steel containing at least one of 0.005 to 0.080% and having a composition of Pcm of 0.10 to 0.25 is hot-rolled, and after the rolling is finished, the temperature is 5 ° C / s up to 600 ° C or less. The steel sheet obtained by cooling at the above cooling rate is cold-formed into a steel pipe. As a result, it is possible to obtain a steel pipe having a work hardening index of 0.10 or more in a tensile test in the pipe axis direction and excellent in deformability, and the occurrence of local buckling due to an external force acting on the steel pipe laterally and brittleness caused by the occurrence of the local buckling. It is said that it can prevent the occurrence of specific cracks and fractures.

  Patent Document 2 contains C: 0.02 to 0.20%, Si: 0.02 to 0.50%, Mn: 0.50 to 2.00% by weight, and further Cu: 0. 1 or 2 selected from the group consisting of 10 to 1.5%, Ni: 0.10 to 0.50%, Nb: 0.005 to 0.10% and V: 0.005 to 0.10%. Hot-rolled steel sheet containing at least seeds and having a Ceq of 0.38 to 0.45 is hot-rolled such that the rolling reduction per pass in a temperature range of 900 ° C. or higher is 4% or less. And a method for manufacturing a steel pipe, wherein the hot rolled steel sheet is reheated to a two-phase temperature range of Ac1 point to Ac3 point and quenched from the two-phase temperature range, further tempered, and then pipe-formed. Is listed. The steel pipe thus obtained is a high-strength steel pipe having a low yield ratio of 0.2% proof stress: 440 MPa or more, a tensile strength: 590 to 700 MPa, and a yield ratio: 80% or less, and a steel structure such as a building, a bridge or a tank. It is said that it is suitable for use.

  In Patent Document 3, in producing a steel pipe having a composition including C: 0.10 to 0.18%, Si: 0.1 to 0.5%, and Mn: 1 to 2% by mass%, Ac3 point is set. The steps of heating and quenching after the above steps, the steps of heating in the two-phase temperature region of Ac1 point to Ac3 point and then air cooling, the step of cold forming into a tubular shape, and the step of reheating to 500 to 600 ° C. A method for producing a high-strength steel pipe for a building structure having a low yield ratio by sequentially performing it is described. As a result, it is said that a steel pipe for building structure having a tensile strength of 590 MPa or more can be manufactured without using an expensive alloy element.

  In Patent Document 4, C: 0.11 to 0.20%, Si: 0.05 to 0.50%, Mn: 1.00 to 2.00%, and P: 0.030% or less in mass%. , S: 0.010% or less, Al: 0.01 to 0.08%, and a ferrite phase as a main phase, and the second phase other than the main phase contains pearlite having an area ratio of 8 to 30% and And / or pseudo pearlite, having a structure in which the average grain size including the main phase and the second phase is 4.0 to 10 μm, and 0.2% proof stress YS: 450 MPa or more in the pipe circumferential direction and the pipe axial direction. , Tensile strength TS: 590 MPa or more and yield ratio: 90% or less, a low yield ratio high strength electric resistance welded steel pipe for steel pipe piles is described.

Japanese Patent Laid-Open No. 11-6032 Japanese Patent No. 2687841 JP, 2004-300461, A Japanese Patent No. 6123734

  However, in the steel pipe manufactured by the technique described in Patent Document 1, the yield ratio in the pipe axial direction is excessively reduced. Therefore, when the obtained steel pipe is applied as a steel pipe pile, there is a risk that buckling or the like may occur due to driving during pile driving.

  The technique described in Patent Document 2 requires a heat treatment step for tempering. In addition, the technique described in Patent Document 3 requires a large-sized heat treatment apparatus for pipes, and also needs a heat treatment step after pipe making. The techniques requiring these heat treatments have a problem that the yield ratio becomes too low. Further, there is a problem that the process becomes complicated and the productivity is lowered. In addition, the production cost increases, and it becomes difficult to provide it at low cost.

  In the technique described in Patent Document 4, after the hot rolling, it is cooled from the finish rolling end temperature to a temperature range of 550 to 700 ° C. in 10 to 100 s to obtain a structure mainly composed of ferrite and pearlite. Organization has not been obtained. Further, equipment having an extremely long cooling zone is required, and it becomes difficult to provide an inexpensive high strength and high toughness electric resistance welded steel pipe for steel pipe piles.

  The present invention has been made in view of the above problems, has an optimal yield ratio and high buckling resistance, and further has high strength and high toughness, an electric resistance welded steel pipe and a method for manufacturing the same, and a steel pipe pile. The purpose is to provide.

  The present invention also provides an electric resistance welded steel pipe, a method for manufacturing the same, and a steel pipe pile, which can achieve the above-mentioned problems when a hot-rolled steel plate having a plate thickness of 16 mm or more is mainly used as a material.

  The term "high strength" as used herein means a case where 0.2% proof stress (YS): 450 MPa or more and tensile strength (TS): 590 MPa or more in the pipe axis direction in the base material portion of the electric resistance welded steel pipe. The term "high toughness" as used herein means a case where the Charpy absorbed energy at -30 ° C is 70 J or more, with the pipe axis direction in the base material portion of the electric resistance welded steel pipe being the longitudinal direction of the test piece, and the pipe of the electric resistance welded steel pipe. The above-mentioned high toughness is satisfied in both the circumferential direction and the pipe axis direction. The term "optimal yield ratio" as used herein means that the ratio of 0.2% proof stress to tensile strength (YR) is 80 to 90%. The "high buckling resistance" as used herein means a case where the residual stress in the pipe axial direction of the outer surface of the steel pipe in the base material portion of the electric resistance welded steel pipe is 250 MPa or less and the yield ratio is 90% or less.

  In order to achieve the above-mentioned object, the inventors diligently studied the influence of various alloying elements and manufacturing conditions on the yield ratio, 0.2% proof stress, tensile strength, and Charpy impact property. In addition, the buckling resistance of the obtained steel pipe (electric resistance welded steel pipe) was also earnestly studied. As a result, they have found that while maintaining a relatively low yield ratio, high strength and high toughness can both be achieved, and there is an appropriate component composition, steel structure and manufacturing conditions that have high buckling resistance.

  That is, the hot-rolled steel sheet manufactured by limiting the specific component composition and the hot rolling condition is subjected to the diameter-reducing rolling under the specific condition after welding in the cold roll forming step by the cold roll forming. As a result, bainite has an area ratio of 60% or more, and the average effective grain size of bainite is an average circle of the steel structure at a position 1/4 t deep from the steel pipe outer surface of the base material part of the electric resistance welded steel pipe. The equivalent diameter is 20.0 μm or less, and the average aspect ratio of bainite is 0.1 to 0.8. As a result, the 0.2% proof stress is relatively low at 450 MPa or higher, the tensile strength is high at 590 MPa or higher, the yield ratio is 80 to 90%, and the Charpy absorbed energy at -30 ° C is 70 J or higher. It has been found that an electric resistance welded steel pipe having a low yield ratio, a high yield strength, a high toughness, and a high buckling resistance, in which the residual stress of the outer surface of the steel pipe in the pipe portion in the pipe axial direction is 250 MPa or less, can be obtained.

The present invention has been completed by further studies based on such findings, and the gist of the present invention is as follows.
[1] An electric resistance welded steel pipe having a base material portion and a welded portion in the steel axial direction,
The component composition of the base material part is mass%,
C: 0.12 to 0.20%,
Si: 0.60% or less,
Mn: 0.50 to 1.70%,
P: 0.030% or less,
S: 0.015% or less,
Al: 0.010 to 0.060%,
Nb: 0.010 to 0.080%,
Ti: 0.010 to 0.050%,
N: 0.006% or less is contained, and the balance is Fe and inevitable impurities,
Assuming that the plate thickness of the base material portion is t, the steel structure at a depth position of ¼t from the outer surface of the electric resistance welded steel pipe is
Bainite has an area ratio of 60% or more,
The average effective particle size of the bainite is 20.0 μm or less in average circle equivalent diameter, and the average aspect ratio of the bainite is 0.1 to 0.8;
The tensile strength in the tube axis direction is 590 MPa or more, the 0.2% proof stress is 450 MPa or more, and the yield ratio is 80 to 90%.
Charpy absorbed energy at −30 ° C. in which the pipe axis direction in the base material portion is the longitudinal direction of the test piece is 70 J or more,
An electric resistance welded steel pipe having a residual stress of 250 MPa or less in the pipe axial direction on the outer surface of the steel pipe in the base material portion.
[2] The electric resistance welded steel pipe according to [1], which further contains B: 0.008% or less by mass% in addition to the component composition.
[3] In addition to the above component composition, further in mass%,
Cr: 0.01 to 1.0%,
V: 0.010 to 0.060%,
Mo: 0.01 to 1.0%,
Cu: 0.01 to 0.50%,
Ni: 0.01 to 1.0%,
Ca: 0.0005 to 0.010%
The electric resistance welded steel pipe according to [1] or [2], which contains one or more selected from the above.
[4] A method for producing an electric resistance welded steel pipe, in which a steel material is subjected to a hot rolling step and a cooling step in this order to obtain a hot rolled steel sheet, and the hot rolled steel sheet is subjected to a cold roll forming step to obtain an electric resistance welded steel tube. And
The steel material has a composition according to any one of [1] to [3],
In the hot rolling step, after heating the steel material to a heating temperature of 1100 to 1280 ° C., rough rolling end temperature: 850 to 1150 ° C., finish rolling end temperature: 750 to 850 ° C., and rough rolling and finish rolling. Total rolling reduction at 930 ° C. or less in the above: 65% or more rough rolling and finish rolling to give a hot rolled sheet,
The cooling step is a step of cooling the hot-rolled sheet at an average cooling rate from the start of cooling to a stop of cooling at a sheet thickness center temperature: 5 to 25 ° C./s, a cooling stop temperature: 450 to 650 ° C.,
In the cold roll forming step, a steel pipe material that has been subjected to roll forming processing is welded to the hot rolled steel plate, and a diameter reduction ratio of 0.2 to 0.5% is reduced with respect to the circumferential length of the outer surface of the steel pipe after welding. A method for manufacturing an electric resistance welded steel pipe that is diameter rolled.
[5] The steel structure having the component composition according to any one of [1] to [3] and assuming the plate thickness to be t, the steel structure at a depth position of ¼t from the outer surface is t A hot rolled steel sheet having an area ratio of bainite of 60% or more, an average effective particle diameter of bainite of 20.0 μm or less in an average circle equivalent diameter, and an average aspect ratio of bainite of 0.1 to 0.8. A method of manufacturing an electric resistance welded steel pipe, which comprises a cold roll forming step to obtain an electric resistance welded steel pipe,
In the cold roll forming step, a steel pipe material that has been subjected to roll forming processing is welded to the hot rolled steel plate, and a diameter reduction ratio of 0.2 to 0.5% is reduced with respect to the circumferential length of the outer surface of the steel pipe after welding. A method for manufacturing an electric resistance welded steel pipe that is diameter rolled.
[6] A steel pipe pile using the electric resistance welded steel pipe according to any one of [1] to [3].

  According to the present invention, there is provided an electric resistance welded steel pipe suitably used as a steel pipe pile, having an optimum yield ratio and a high buckling resistance, and having high strength and high toughness, a method for producing the same, and a steel pipe pile. can do. The electric resistance welded steel pipe of the present invention can be easily manufactured and has a remarkable industrial effect.

  Hereinafter, the present invention will be described in detail.

  First, the reasons for limiting the component composition of the electric resistance welded steel pipe of the present invention will be described. Hereinafter, "mass%" in the component composition is simply described as "%" unless otherwise specified.

  The electric resistance welded steel pipe of the present invention has a base material portion and a welded portion, and the base material portion has C: 0.12 to 0.20%, Si: 0.6% or less, and Mn: 0.50 to 1.70. %, P: 0.030% or less, S: 0.015% or less, Al: 0.010 to 0.060%, Nb: 0.010 to 0.080%, Ti: 0.010 to 0.050% , N: 0.006% or less, with the balance being Fe and inevitable impurities.

  The electric resistance welded steel pipe of the present invention has a welded portion in the pipe axis direction. The “hot rolled steel sheet” described later includes hot rolled steel sheet and hot rolled steel strip.

C: 0.12 to 0.20%
C is an element that increases the strength of a steel pipe (electric resistance welded steel pipe) by solid solution strengthening and is involved in the formation of a steel structure such as bainite. C is an element effective in optimizing the yield ratio. Since a steel pipe having a relatively large plate thickness (for example, a steel pipe having a plate thickness of 16 mm or more) has a large difference between the outer diameter and the inner diameter, the workability in manufacturing the steel pipe is large and the yield ratio is likely to increase. Therefore, it is necessary to contain a large amount of C. Therefore, in order to obtain the above effects, it is necessary to contain 0.12% or more of C. On the other hand, when the content of C exceeds 0.20%, martensite is likely to be formed, and the steel structure targeted by the present invention cannot be obtained. As a result, it becomes impossible to secure the high toughness targeted by the present invention. Therefore, C is 0.12 to 0.20%. C is preferably 0.13% or more, and more preferably 0.14% or more. C is preferably 0.19% or less, more preferably 0.18% or less.

Si: 0.60% or less Si is an element that acts as a deoxidizer and can increase the strength of the steel pipe. However, if Si is contained excessively, the toughness decreases. Therefore, Si is set to 0.60% or less. Si is preferably 0.50% or less, more preferably 0.45% or less. The lower limit of Si is not particularly specified, but is preferably 0.01% or more from the viewpoint of electric resistance weldability. More preferably, it is 0.02% or more.

Mn: 0.50 to 1.70%
Mn is an element that increases the strength of the steel pipe through solid solution strengthening. In order to obtain such an effect and ensure the high strength targeted by the present invention, it is necessary to contain 0.50% or more of Mn. On the other hand, if the Mn content exceeds 1.70%, the steel structure becomes finer and the yield strength becomes higher, so that the yield ratio targeted by the present invention cannot be secured. Therefore, Mn is set to 0.50 to 1.70%. Mn is preferably 0.55% or more, more preferably 0.60% or more. Mn is preferably 1.65% or less, more preferably 1.60% or less.

P: 0.030% or less P is an element that segregates at the crystal grain boundaries and reduces toughness, and it is desirable to reduce it as an impurity as much as possible, but in the present invention, up to 0.030% is acceptable. Therefore, P is 0.030% or less. P is preferably 0.025% or less, more preferably 0.020% or less. However, excessive reduction of P causes an increase in refining cost, so P is preferably 0.002% or more. More preferably, it is 0.003% or more.

S: 0.015% or less S is present as MnS in steel when producing a hot-rolled steel sheet that is a raw material of a steel pipe, and is thinly drawn in the hot rolling step, which adversely affects the ductility and toughness of the steel pipe. Exert. Therefore, in the present invention, it is desirable to reduce S as an impurity as much as possible, but the content of S can be allowed up to 0.015%. Therefore, S is set to 0.015% or less. S is preferably 0.010% or less, more preferably 0.008% or less. However, excessive reduction of S causes a rise in refining cost, so S is preferably 0.0002% or more. More preferably, it is 0.001% or more.

Al: 0.010 to 0.060%
Al acts as a deoxidizing agent, combines with N to form AlN, and contributes to refinement of crystal grains. In order to obtain such an effect, it is necessary to contain 0.010% or more of Al. On the other hand, the inclusion of a large amount of Al exceeding 0.060% reduces the cleanliness of the steel material (hot rolled steel sheet that is the raw material of the steel pipe), and reduces the ductility and toughness of the steel pipe. Therefore, Al is set to 0.010 to 0.060%. Al is preferably 0.015% or more, more preferably 0.020% or more. The Al content is preferably 0.055% or less, and more preferably 0.050% or less.

Nb: 0.010 to 0.080%
Nb combines with carbon and nitrogen to form fine precipitates, and increases the strength of the steel pipe by precipitation strengthening. In order to obtain such an effect, it is necessary to contain Nb in an amount of 0.010% or more. On the other hand, when Nb is contained in excess of 0.080%, it becomes difficult to form a solid solution by heating in the hot rolling step when manufacturing a hot rolled steel sheet which is a raw material of a steel pipe. As a result, coarse precipitates remain and the toughness decreases. Therefore, Nb is set to 0.010 to 0.080%. Nb is preferably 0.015% or more, more preferably 0.020% or more. Nb is preferably 0.075% or less, more preferably 0.070% or less.

Ti: 0.010 to 0.050%
Ti combines with carbon and nitrogen to form fine precipitates, and increases the strength of the steel pipe by precipitation strengthening. To obtain such an effect, it is necessary to contain Ti in an amount of 0.010% or more. On the other hand, if the Ti content exceeds 0.050%, the precipitates become coarse and the toughness decreases. Therefore, Ti is set to 0.010 to 0.050%. Ti is preferably 0.012% or more, more preferably 0.015% or more. The Ti content is preferably 0.045% or less, more preferably 0.040% or less.

N: 0.006% or less N has the effect of increasing the strength of the steel pipe if it is in a trace amount, but if it is contained in a large amount, it forms coarse precipitates at high temperatures and reduces toughness. Therefore, N is 0.006% or less. Excessive reduction of N causes an increase in refining cost, so the content is preferably 0.001% or more, and more preferably 0.002% or more. N is preferably 0.005% or less, more preferably 0.004% or less.

  The balance is Fe and inevitable impurities. In addition, as long as the effect of the present invention is not impaired, the content of O: 0.0050% or less can be allowed as an unavoidable impurity.

  The above-mentioned components are the basic component compositions of the electric resistance welded steel pipe in the present invention. Although the above-mentioned essential elements can provide the characteristics desired in the present invention, in addition to the basic component composition, the following elements can be further contained, if necessary.

B: 0.008% or less B is an element that contributes to the refinement of the steel structure by lowering the ferrite transformation start temperature, and can be contained if necessary. However, if the content of B exceeds 0.008%, segregation tends to occur at the grain boundaries, and the toughness may decrease. Therefore, when B is contained, B is preferably 0.008% or less. It is more preferably 0.006% or less. In addition, B is preferably 0.0003% or more.

Cr: 0.01-1.0%, V: 0.010-0.060%, Mo: 0.01-1.0%, Cu: 0.01-0.50%, Ni: 0.01- 1.0%, one or more selected from Ca: 0.0005 to 0.010% Cr: 0.01 to 1.0%
Cr is an element that increases the strength of the steel pipe by increasing the hardenability, and can be contained if necessary. In order to obtain such effects, it is preferable to contain Cr in an amount of 0.01% or more. On the other hand, if Cr is contained in excess of 1.0%, the toughness and weldability may be deteriorated, so the content is preferably 1.0% or less. Therefore, when Cr is contained, Cr is preferably 0.01 to 1.0%. Cr is more preferably 0.02% or more, still more preferably 0.03% or more. Cr is more preferably 0.8% or less, and even more preferably 0.6% or less.

V: 0.010 to 0.060%
V is an element that combines with carbon or nitrogen to form fine precipitates and increases the strength of the steel pipe by precipitation strengthening, and can be contained as necessary. In order to obtain such an effect, it is necessary to contain V by 0.010% or more. On the other hand, if V is contained in excess of 0.060%, the precipitates become coarse and the above-mentioned effect is easily saturated. Therefore, V is set to 0.010 to 0.060%. V is preferably 0.012% or more, more preferably 0.015% or more. V is preferably 0.055% or less, and more preferably 0.050% or less.

Mo: 0.01-1.0%
Mo is an element that increases the strength of the steel pipe by increasing the hardenability, and can be contained if necessary. In order to obtain such effects, it is preferable to contain Mo in an amount of 0.01% or more. On the other hand, if Mo is contained in excess of 1.0%, the toughness may be reduced, so 1.0% or less is preferable. Therefore, when Mo is contained, it is preferable to set Mo to 0.01 to 1.0%. Mo is more preferably 0.02% or more, still more preferably 0.03% or more. Mo is more preferably 0.8% or less, and even more preferably 0.6% or less.

Cu: 0.01 to 0.50%
Cu is an element that increases the strength of the steel pipe by solid solution strengthening, and can be contained if necessary. In order to obtain such an effect, it is preferable to contain Cu in an amount of 0.01% or more. On the other hand, if Cu is contained in excess of 0.50%, the toughness may be reduced, so 0.50% or less is preferable. Therefore, when Cu is contained, the content of Cu is preferably 0.01 to 0.50%. Cu is more preferably 0.02% or more, still more preferably 0.03% or more. Cu is more preferably 0.45% or less, and even more preferably 0.40% or less.

Ni: 0.01-1.0%
Ni is an element that increases the strength of the steel pipe by solid solution strengthening, and can be contained if necessary. In order to obtain such effects, it is preferable to contain Ni in an amount of 0.01% or more. On the other hand, if Ni is contained in excess of 1.0%, the toughness may be reduced, so the content is preferably 1.0% or less. Therefore, when Ni is contained, the Ni content is preferably 0.01 to 1.0%. The Ni content is more preferably 0.02% or more, still more preferably 0.03% or more. The Ni content is more preferably 0.8% or less, and even more preferably 0.6% or less.

Ca: 0.0005 to 0.010%
Ca is an element that contributes to the improvement of the toughness of steel by spheroidizing sulfides such as MnS that are thinly drawn in the hot rolling step when producing a hot rolled steel sheet that is a material for steel pipes, and is necessary. Can be included accordingly. In order to obtain such an effect, when Ca is contained, it is preferably contained in 0.0005% or more. However, if the Ca content exceeds 0.010%, Ca oxide clusters are formed in the steel, and the toughness may deteriorate. Therefore, when Ca is contained, it is preferable that the content of Ca be 0.0005% to 0.010%. Ca is more preferably 0.0010% or more, and further preferably 0.0015% or more. Ca is more preferably 0.005% or less, and even more preferably 0.004% or less.

  Next, the reason for limiting the steel structure of the electric resistance welded steel pipe of the present invention will be described.

  In the electric resistance welded steel pipe of the present invention, when the plate thickness of the base material portion is t, the steel structure at a depth position of 1/4 t of the plate thickness t from the outer surface of the electric resistance welded steel pipe has bainite at an area ratio of 60% or more. That is, the steel has a steel structure in which the average effective grain size of bainite is 20.0 μm or less in average circle equivalent diameter, and the average aspect ratio of bainite is 0.1 to 0.8.

  Here, the 1 / 4t depth position of the plate thickness t means that the cooling rate in the hot rolling step when manufacturing a hot rolled steel sheet, which is a raw material of a steel pipe, is the most important in controlling the steel structure. It is a position intermediate between the outermost surface layer and the 1 / 2t depth position that is the smallest. In the present invention, a cross section parallel to the rolling direction at the 1/4 W position of the strip width W in hot rolling is used as the evaluation surface of the steel structure. In the present invention, since heat treatment or the like is not performed after hot rolling, the structure of the hot rolled steel plate and the structure of the steel pipe (base material portion) are the same.

Area ratio of bainite: 60% or more In the present invention, in order to achieve both high strength and high toughness, it is important to contain bainite in an area ratio of 60% or more. When the bainite content is less than 60%, it becomes difficult to obtain the strength intended in the present invention. Therefore, the steel structure at the 1 / 4t depth position of the plate thickness t from the outer surface of the steel pipe has bainite in an area ratio of 60% or more. It is preferably at least 65%. If the area ratio of bainite is excessive, the yield ratio becomes too high. Therefore, the area ratio of bainite is preferably 98% or less. It is more preferably 95% or less.

  As the structure (residual structure) other than bainite, ferrite, pearlite, martensite, austenite, etc. can be considered. If the total area ratio of these structures is 40% or more with respect to the entire steel structure, the strength and toughness are insufficient, and the yield ratio is increased or excessively decreased. Therefore, it is preferably less than 40%. It is more preferably less than 35%. In consideration of obtaining the yield ratio targeted in the present invention, the lower limit of the total area ratio of the remaining structure is preferably more than 2%, more preferably more than 5%.

  In the present invention, the area ratio of each tissue described above can be measured by the method described in Examples below.

Average effective particle size of bainite: average circle equivalent diameter of 20.0 μm or less In the present invention, in order to achieve both high strength and high toughness, the average effective equivalent particle diameter of bainite may be 20.0 μm or less. is important. When the average effective particle size of bainite exceeds 20.0 μm in average equivalent circle diameter, the toughness targeted by the present invention cannot be obtained. In addition, the desired strength cannot be obtained in the present invention. It is preferably 15.0 μm or less. If the bainite becomes too fine, the yield ratio becomes too high. Therefore, it is preferable that the average equivalent circle diameter of the average effective particle diameter of bainite is 1.0 μm or more, and more preferably 2.0 μm or more. .

  Here, when the difference in orientation between adjacent crystals is obtained and the region surrounded by the boundary where the difference in orientation between adjacent crystals (crystal orientation difference) is 15 ° or more is defined as a crystal grain, the area of the circle is equal to that of the crystal grain. The diameter was defined as the effective particle size of bainite. The arithmetic mean of the particle diameters was calculated from the obtained effective particle diameters to obtain the average equivalent circle diameter (average effective particle diameter). In the present invention, the crystal orientation difference, the effective grain size, and the average equivalent circle diameter can be measured by the methods described in Examples described later.

Bainite average aspect ratio: 0.1-0.8
In the present invention, in order to control the yield ratio in the tube axis direction to 80 to 90%, it is necessary to set the average aspect ratio of bainite to 0.1 to 0.8. Here, in the above-mentioned bainite crystal grains, (average length in the plate thickness direction) / (average length in the tube axis direction) was calculated and used as the average aspect ratio of bainite. When the average aspect ratio of bainite exceeds 0.8, the plastic deformability in the pipe axis direction decreases, and the yield ratio easily exceeds 90%. On the other hand, when the average aspect ratio of bainite is less than 0.1, the strength in the tube axis direction decreases, and the strength intended by the present invention cannot be obtained.

  In the present invention, the average length in the plate thickness direction and the average length in the rolling direction of the bainite crystal grains can be measured by the method described in Examples below.

  Next, a method for manufacturing an electric resistance welded steel pipe according to an embodiment of the present invention will be described.

  The electric resistance welded steel pipe of the present invention is, for example, a hot rolled steel sheet obtained by subjecting a steel material having the above-described composition to a hot rolling step, a cooling step and a winding step in this order, and further, cold rolling the hot rolled steel sheet. Roll-formed process is applied to make ERW steel pipe.

  In the following description of the manufacturing method, “° C.” regarding temperature is the surface temperature of a steel material or a steel plate (hot rolled steel plate) unless otherwise specified. These surface temperatures can be measured with a radiation thermometer or the like. The temperature at the center of the steel plate thickness can be obtained by calculating the temperature distribution in the steel plate cross section by heat transfer analysis and correcting the result according to the surface temperature of the steel plate. The "hot rolled steel sheet" includes hot rolled steel sheet and hot rolled steel strip.

  In the present invention, the method for melting the steel material (steel slab) is not particularly limited. Molten steel having the above-described component composition, a converter, an electric furnace, a melting process by a conventional melting method such as a vacuum melting furnace, and a slab or the like slab by a conventional casting method such as a continuous casting method, It is preferable from the viewpoint of quality and productivity. It should be noted that there is no problem even if the ingot-bulk rolling method is applied instead of the continuous casting method. The molten steel may be further subjected to secondary refining such as ladle refining.

  Then, the obtained steel material (steel slab) is subjected to a hot rolling step. In the hot rolling process, after heating the steel material to a heating temperature of 1100 to 1280 ° C., rough rolling to a rough rolling end temperature of 850 to 1150 ° C. is performed, and a finish rolling to a finish rolling end temperature of 750 to 850 ° C. And a hot rolling at which the total rolling reduction at 930 ° C. or less in rough rolling and finish rolling: 65% or more is performed to obtain a hot rolled sheet.

Heating temperature: 1100-1280 ° C
If the heating temperature is lower than 1100 ° C, coarse carbides existing in the steel material produced during casting cannot be dissolved. As a result, the effect of the contained carbide forming element cannot be sufficiently obtained. On the other hand, when the heating temperature is higher than 1280 ° C. and becomes high temperature, the crystal grains are remarkably coarsened and the structure of the hot-rolled steel sheet, which is a raw material of the steel tube, is coarsened, and it becomes difficult to secure the target characteristics of the present invention. . Therefore, the heating temperature of the steel material needs to be 1100 to 1280 ° C. It is preferably 1120 to 1230 ° C. Note that this temperature is the temperature set in the furnace of the heating furnace.

Rough rolling end temperature: 850 to 1150 ° C
When the rough rolling end temperature is lower than 850 ° C., the recovery of the structure during hot rolling does not occur and crystal grains excessively elongated in the rolling direction are likely to be generated. As a result, the average aspect ratio of bainite tends to be less than 0.1. On the other hand, when the rough rolling finish temperature exceeds 1150 ° C., the amount of reduction in the austenite unrecrystallized temperature range is insufficient, and fine austenite grains cannot be obtained. As a result, the average effective grain size of bainite aimed at by the present invention is obtained. It becomes difficult to secure the diameter. Therefore, the rough rolling end temperature is set to 850 to 1150 ° C. The temperature is preferably 860 to 1000 ° C.

Finish rolling finish temperature: 750-850 ° C
When the finish rolling end temperature is lower than 750 ° C., the recovery of the structure during hot rolling does not occur and crystal grains excessively elongated in the rolling direction are likely to be generated. As a result, the average aspect ratio of bainite tends to be less than 0.1. On the other hand, when the finish rolling finish temperature exceeds 850 ° C., the amount of reduction in the austenite unrecrystallized temperature region is insufficient, and fine austenite grains cannot be obtained, and as a result, the average effective grain size of bainite intended in the present invention is obtained. It becomes difficult to secure the diameter. Therefore, the finish rolling end temperature is set to 750 to 850 ° C. The temperature is preferably 770 to 830 ° C.

Total rolling reduction at 930 ° C. or less in rough rolling and finish rolling: 65% or more In the present invention, by refining austenite in the hot rolling step, bainite and the balance structure produced in the subsequent cooling step and winding step are formed. It is possible to obtain a hot-rolled steel sheet which is miniaturized and which has strength and toughness targeted in the present invention and which is suitable as a material for an electric resistance welded steel pipe. In order to refine the austenite in the hot rolling step, it is necessary to increase the rolling reduction in the austenite non-recrystallization temperature range and to introduce a sufficient processing strain. In order to obtain this effect, in the present invention, the total reduction ratio in the temperature range of 930 ° C. or lower to the finish rolling end temperature is set to 65% or more. Here, the total reduction rate refers to the total reduction rate of each rolling pass in the temperature range up to 930 ° C. or lower until the finish rolling end temperature.

  If the total reduction ratio in the temperature range up to the finish rolling finish temperature of 930 ° C. or lower is less than 65%, sufficient working strain cannot be introduced in the hot rolling process, and therefore the average effective grain size of bainite that is the object of the present invention. A steel structure having a diameter cannot be obtained. The total reduction ratio in the temperature range up to 930 ° C or lower until the finish rolling end temperature is more preferably 70% or more. The upper limit is not particularly specified, but if it exceeds 80%, the effect of improving the toughness with respect to the increase in the rolling reduction becomes small, and only the equipment load increases. Therefore, the total reduction ratio in the temperature range up to 930 ° C. or lower until the finish rolling end temperature is preferably 80% or less. It is more preferably 75% or less.

  In the present invention, the reason why the temperature is 930 ° C. or lower is that if the temperature exceeds 930 ° C., austenite is recrystallized in the hot rolling step, dislocations introduced by rolling disappear, and fine austenite cannot be obtained.

  In the present invention, when the steel material is hot-rolled, it may be hot-rolled in which both the rough rolling and the finish rolling described above have a total reduction ratio of 65% or more up to the finish rolling end temperature of 930 ° C. or less. Alternatively, the hot rolling may be performed by finishing rolling only to a total reduction ratio of 65% or more up to a finishing rolling finishing temperature of 930 ° C. or less. In the latter case, if the total rolling reduction up to the finish rolling end temperature of 930 ° C. or less cannot be set to 65% or more only by finish rolling, the slab is cooled during the rough rolling to a temperature of 930 ° C. or less. The total reduction ratio up to the finish rolling end temperature of 930 ° C. or less in both rough rolling and finish rolling may be 65% or more.

  Then, the hot rolled sheet after the hot rolling step is subjected to a cooling step. In the cooling step, the hot-rolled sheet is cooled at the center temperature of the sheet thickness at an average cooling rate from the start of cooling to a stop of cooling: 5 to 25 ° C / s and a cooling stop temperature: 450 to 650 ° C.

Average cooling rate from start of cooling to stop of cooling: 5 to 25 ° C / s
At the plate thickness center temperature of the hot rolled sheet, if the average cooling rate in the temperature range from the start of cooling to the cooling stop temperature described below is less than 5 ° C./s, the area ratio of bainite decreases due to the formation of ferrite, and in the present invention, The desired strength cannot be obtained. On the other hand, when the average cooling rate exceeds 25 ° C / s, the average aspect ratio of bainite exceeds 0.8. As a result, the yield ratio tends to exceed 90%. The average cooling rate is preferably 10 ° C./s or more, and preferably 20 ° C./s or less.

  In the present invention, unless otherwise specified, the average cooling rate is a value obtained by ((center temperature of hot-rolled sheet before cooling-center temperature of hot-rolled sheet after cooling) / cooling time) The average of (cooling rate). Examples of the cooling method include water cooling in which water is sprayed from a nozzle, cooling by spraying cooling gas, and the like. In the present invention, it is preferable to perform a cooling operation (treatment) on both sides of the hot rolled sheet so that both sides of the hot rolled sheet are cooled under the same conditions.

Cooling stop temperature: 450-650 ° C
When the cooling stop temperature is less than 450 ° C. at the plate thickness center temperature of the hot-rolled sheet, the average aspect ratio of bainite exceeds 0.8, and as a result, the yield ratio easily exceeds 90%. On the other hand, when the cooling stop temperature exceeds 650 ° C, the bainite transformation start temperature is exceeded, and therefore the bainite area ratio cannot be set to 60% or more. The cooling stop temperature is preferably 480 ° C. or higher, and preferably 620 ° C. or lower.

  Then, the hot-rolled steel sheet after the cooling step is wound, and then a winding step of allowing to cool is performed.

  In the winding step, it is preferable to wind at a winding temperature of 450 to 650 ° C. from the viewpoint of the steel sheet structure of the hot rolled steel sheet that is the material of the steel pipe. If the winding temperature is lower than 450 ° C, the average aspect ratio of bainite exceeds 0.8, and as a result, the yield ratio may exceed 90%. On the other hand, if the coiling temperature exceeds 650 ° C., the bainite transformation start temperature may be exceeded and the bainite area ratio may not be 60% or more. The coiling temperature is more preferably 480 to 620 ° C.

  Then, the hot rolled steel sheet after the winding step is subjected to a cold roll forming step. In the cold roll forming process, the hot-rolled steel sheet is cold rolled to form a cylindrical open pipe, and both ends of the steel pipe material (that is, the abutting parts of the open pipe) are electric resistance welded and after welding. Diameter reduction rolling is performed at a diameter reduction rate of 0.2 to 0.5% with respect to the peripheral length of the outer surface of the round steel pipe.

Diameter reduction ratio in diameter reduction rolling: 0.2 to 0.5%
When the diameter reduction ratio in the diameter reduction rolling is less than 0.2%, the reduction of the residual stress due to plastic deformation becomes insufficient in the above-described steel material of the steel pipe of the present invention. As a result, the residual stress in the pipe axial direction on the outer surface of the steel pipe exceeds 250 MPa. Further, the yield ratio becomes less than 80% due to insufficient workability. On the other hand, if the diameter reduction ratio in the diameter reduction rolling exceeds 0.5%, the yield ratio exceeds 90% due to work hardening. As a result, desired plastic deformability, that is, buckling resistance cannot be obtained. Further, even if the above-mentioned residual stress exceeds 250 MPa, the buckling resistance is deteriorated.

  As described above, the electric resistance welded steel pipe of the present invention is manufactured. According to the present invention, the tensile strength in the longitudinal direction of the pipe is 590 MPa or more, the 0.2% proof stress is 450 MPa or more, the yield ratio is 80 to 90%, the Charpy absorbed energy at -30 ° C is 70 J or more, and the steel pipe is An electric resistance welded steel pipe having a residual stress of 250 MPa or less on the outer surface in the pipe axis direction can be obtained. This makes it possible to easily manufacture an electric resistance welded steel pipe having high strength, high toughness, an optimum yield ratio and excellent buckling resistance. Since this electric resistance welded steel pipe can be suitably used particularly for a steel pipe pile used as a foundation of a structure, it has a remarkable industrial effect.

  Next, the steel pipe pile of the present invention will be described.

  The steel pipe pile of the present invention has a plate thickness of 16 mm or more, an outer diameter of 300 mm or more and 700 mm or less, and is made of an electric resistance welded steel pipe having the above-described composition and steel structure. By defining the component composition and the steel structure of the electric resistance welded steel pipe as described above, the tensile strength in the pipe longitudinal direction is 590 MPa or more, the 0.2% proof stress is 450 MPa or more, and the yield ratio is 80 to 90%. A steel pipe pile having a Charpy absorbed energy at 70 ° C. or higher and a residual stress of 250 MPa or less on the outer surface of the steel pipe in the pipe axis direction can be obtained. The steel pipe pile of the present invention is driven into the ground, and if necessary, the steel pipe piles may be welded or connected by connecting means such as a screw joint during the driving to be constructed on-site into a long pile. Become. According to the steel pipe pile of the present invention, since it has the above characteristics, it is possible to reduce the risk of causing problems such as buckling when driving the pile.

  Hereinafter, the present invention will be described in more detail based on examples. The present invention is not limited to the examples below.

  Molten steel having the chemical composition shown in Table 1 was melted in a converter and made into a slab (steel material: wall thickness 250 mm) by a continuous casting method. The obtained slab is subjected to a hot rolling step, a cooling step, a winding step, and a cold roll forming step under the manufacturing conditions shown in Tables 2-1 and 2-2, and then the tables 2-1 and 2-2. ERW steel pipes having outer diameters and plate thicknesses shown in were produced. Also, in the cold roll forming process, the butt portion of the open pipe was electric resistance welded.

  Test pieces were taken from the obtained electric resistance welded steel pipe, and the structure observation, tensile test, Charpy impact test, residual stress measurement, and member compression test were carried out by the following methods.

[Tissue observation]
The test piece for observing the structure was prepared so that the cross section in the tube axis direction at the position of 90 ° in the circumferential direction was the observation surface when the electric resistance welded portion was 0 °, and was polished and then subjected to nital corrosion. The structure is observed with an optical microscope (magnification: 1000 times) or a scanning electron microscope (SEM, magnification: 1000 times) from the outer surface of the electric resistance welded steel pipe to observe the structure at a depth position of 1/4 t of the plate thickness t. Then, the image was taken. The area ratio of bainite was determined from the obtained optical microscope image and SEM image. The area ratio of bainite was calculated by observing in 5 or more visual fields and averaging the values obtained in each visual field.

  Moreover, the average effective particle diameter (average equivalent circle diameter) of bainite was measured using the SEM / EBSD method. The effective grain size is obtained by determining the orientation difference between adjacent crystal grains, and assuming that the region surrounded by the boundary where the orientation difference is 15 ° or more is the effective grain, the diameter of a circle having the same area as that of the effective grain is calculated. The effective particle size of bainite was used. The arithmetic mean of the obtained effective particle diameters was calculated and made the average equivalent circle diameter. The measurement area was 500 μm × 500 μm, and the measurement step size was 0.5 μm. In the crystal grain size analysis, those having an effective grain size of 2.0 μm or less were excluded from the analysis target as measurement noise.

  Further, the average aspect ratio of bainite was obtained by measuring the length in the plate thickness direction and the length in the tube axis direction of each effective crystal grain measured by the above method, and calculating the respective averages. The length in the plate thickness direction and the length in the pipe axis direction were the maximum lengths in the plate thickness direction and the pipe axis direction in each effective crystal grain.

[Tensile test]
In the tensile test, when the electric resistance welded portion of the obtained electric resistance welded steel pipe was set at 0 °, a JIS 5 tensile test piece was sampled at a position of 90 ° in the circumferential direction so that the tensile direction was parallel to the pipe axis direction. did. A tensile test was carried out in accordance with JIS Z 2241. The 0.2% proof stress (yield strength YS) and the tensile strength TS were measured, and the yield ratio defined by (0.2% proof stress) / (tensile strength) was calculated.

[Charpy impact test]
In the Charpy impact test, when the electric resistance welded portion of the obtained electric resistance welded steel pipe is set at 0 °, the longitudinal direction of the test piece becomes parallel to the pipe axis direction from the plate thickness t / 2 position at the position of 90 ° in the circumferential direction. As described above, a V-notch test piece was taken. According to JIS Z 2242, a Charpy impact test was conducted at a test temperature of −30 ° C. to obtain absorbed energy (J). The number of test pieces was 3, and the average value was calculated to obtain the absorbed energy (J).

[Measurement of residual stress]
The residual stress was measured by the X-ray diffraction cos α method using μ-X360 manufactured by Pulstec. The residual stress was measured at three positions: 90 ° position, 180 ° position, and 270 ° position when the electric resistance welded portion was set at 0 ° on the outer surface of the obtained electric resistance welded steel pipe. The average value of the measured values at the three obtained points was taken as the residual stress. The stress measurement direction was the tube axis direction.

[Member compression test]
In the present invention, in order to evaluate the performance as a steel pipe pile, a member compression test is performed, and the buckling strength ratio σcr
/ σy (where σcr is the buckling stress and σy is the material yield strength). If the buckling strength ratio is greater than the reduction coefficient R = 0.8 + 2.5 × t / r (where t is the plate thickness and r is the radius), then the buckling strength, which is important for the performance of the steel pipe pile, is sufficient. I can judge.

  The obtained results are shown in Table 3-1 and Table 3-2, respectively.

  As shown in Tables 1 to 3-2, all the electric resistance welded steel pipes within the scope of the present invention have a tensile strength in the axial direction of 590 MPa or more, a 0.2% proof stress of 450 MPa or more, and a yield ratio of 80 to 90. %, The Charpy absorbed energy at −30 ° C. was 70 J or more, and the residual stress in the tube axial direction on the outer surface of the tube was 250 MPa or less. It was also found that the electric resistance welded steel pipe having these characteristics has sufficient buckling strength, which is important for the performance of the steel pipe pile.

  On the other hand, the steel pipes whose composition, steel structure and manufacturing conditions are out of the scope of the present invention include tensile strength in the longitudinal direction of the pipe, 0.2% proof stress, yield ratio, Charpy absorbed energy at -30 ° C, pipes on the outer surface of the pipe. Among the residual stresses in the axial direction, the value targeted by the present invention could not be obtained with any one or more.

  From the above, the composition of the electric resistance welded steel pipe, steel structure, and by making the manufacturing conditions within the scope of the present invention, suitable for steel pipe piles, having an optimum yield ratio and high buckling resistance, Furthermore, an electric resistance welded steel pipe having both high strength and high toughness can be provided.

Claims (6)

An electric resistance welded steel pipe having a base material portion and a welded portion in the pipe axial direction,
The component composition of the base material part is mass%,
C: 0.12 to 0.20%,
Si: 0.60% or less,
Mn: 0.50 to 1.70%,
P: 0.030% or less,
S: 0.015% or less,
Al: 0.010 to 0.060%,
Nb: 0.010 to 0.080%,
Ti: 0.010 to 0.050%,
N: 0.006% or less is contained, and the balance is Fe and inevitable impurities,
Assuming that the plate thickness of the base material portion is t, the steel structure at a depth position of ¼t from the outer surface of the electric resistance welded steel pipe is
Bainite has an area ratio of 60% or more,
The average effective particle size of the bainite is 20.0 μm or less in average circle equivalent diameter, and the average aspect ratio of the bainite is 0.1 to 0.8;
The tensile strength in the tube axis direction is 590 MPa or more, the 0.2% proof stress is 450 MPa or more, and the yield ratio is 80 to 90%.
Charpy absorbed energy at −30 ° C. in which the pipe axis direction in the base material portion is the longitudinal direction of the test piece is 70 J or more,
An electric resistance welded steel pipe having a residual stress of 250 MPa or less in the pipe axial direction on the outer surface of the steel pipe in the base material portion.   The electric resistance welded steel pipe according to claim 1, further comprising B: 0.008% or less by mass% in addition to the component composition. In addition to the above component composition, further in mass%,
Cr: 0.01 to 1.0%,
V: 0.010 to 0.060%,
Mo: 0.01 to 1.0%,
Cu: 0.01 to 0.50%,
Ni: 0.01 to 1.0%,
Ca: 0.0005 to 0.010%
The electric resistance welded steel pipe according to claim 1 or 2, containing one or more selected from the above. The hot rolling process and the cooling process are performed on the steel material in this order to obtain a hot rolled steel sheet, and the hot rolled steel sheet is subjected to a cold roll forming step to obtain a hot rolled steel sheet . A method of manufacturing an electric resistance welded steel pipe, which is an electric resistance welded steel pipe,
The steel material has a composition according to any one of claims 1 to 3,
In the hot rolling step, after heating the steel material to a heating temperature of 1100 to 1280 ° C., finish rolling temperature: 850 to 1150 ° C., finish rolling finish temperature: 750 to 850 ° C., and rough rolling and finish rolling. Total rolling reduction at 930 ° C. or lower: 65% or higher rough rolling and finish rolling to obtain a hot rolled sheet,
The cooling step is a step of cooling the hot-rolled sheet at a plate thickness center temperature at an average cooling rate from cooling start to cooling stop: 5 to 25 ° C / s, cooling stop temperature: 450 to 650 ° C.
In the cold roll forming step, the hot rolled steel sheet is subjected to roll forming by welding a steel pipe material, and a diameter reduction ratio of 0.2 to 0.5% is reduced with respect to the circumferential length of the outer surface of the steel pipe after welding. A method for manufacturing an electric resistance welded steel pipe that is diameter rolled. It has the composition of any one of claims 1 to 3, and when the plate thickness is t, the steel structure at a 1 / 4t depth position of the plate thickness t from the outer surface is bainite in area ratio. Cold roll forming step for a hot-rolled steel sheet having an average effective particle size of 60% or more, an average equivalent particle diameter of the bainite of 20.0 μm or less, and an average aspect ratio of the bainite of 0.1 to 0.8. A method of manufacturing an electric resistance welded steel pipe, which comprises:
In the cold roll forming step, the hot rolled steel sheet is subjected to roll forming by welding a steel pipe material, and a diameter reduction ratio of 0.2 to 0.5% is reduced with respect to the circumferential length of the outer surface of the steel pipe after welding. A method for manufacturing an electric resistance welded steel pipe that is diameter rolled.   A steel pipe pile using the electric resistance welded steel pipe according to claim 1.