JP6493564B2 - Friction stir welding method and apparatus - Google Patents

Friction stir welding method and apparatus Download PDF

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JP6493564B2
JP6493564B2 JP2017558591A JP2017558591A JP6493564B2 JP 6493564 B2 JP6493564 B2 JP 6493564B2 JP 2017558591 A JP2017558591 A JP 2017558591A JP 2017558591 A JP2017558591 A JP 2017558591A JP 6493564 B2 JP6493564 B2 JP 6493564B2
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heating
steel plate
stir welding
friction stir
joining
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JPWO2018070316A1 (en
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松下 宗生
宗生 松下
公一 谷口
公一 谷口
池田 倫正
倫正 池田
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JFE Steel Corp
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K20/00Non-electric welding by applying impact or other pressure, with or without the application of heat, e.g. cladding or plating
    • B23K20/12Non-electric welding by applying impact or other pressure, with or without the application of heat, e.g. cladding or plating the heat being generated by friction; Friction welding
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K20/00Non-electric welding by applying impact or other pressure, with or without the application of heat, e.g. cladding or plating
    • B23K20/26Auxiliary equipment

Description

本発明は、回転ツールを被加工材間の未接合部に挿入し回転させながら移動させ、この回転ツールとの摩擦熱による被加工材の軟化と、その軟化部を回転ツールが撹拌することにより生じる塑性流動と、を利用して、溶加材を添加することなく接合を行う摩擦撹拌接合方法および当該摩擦撹拌接合方法を実現する装置に関する。   According to the present invention, the rotary tool is inserted into an unjoined portion between the workpieces and moved while rotating, and the workpiece is softened by frictional heat with the rotary tool, and the softened portion is stirred by the rotary tool. The present invention relates to a friction stir welding method in which joining is performed without adding a filler material by using the generated plastic flow, and an apparatus for realizing the friction stir welding method.

摩擦溶接法として、特許文献1には、一対の金属材料の両方または片方を回転することにより、金属材料に摩擦熱を生じさせて軟化させながら、その軟化した部位を撹拌して塑性流動を起こすことによって、金属材料を接合する技術が開示されている。   As a friction welding method, in Patent Document 1, by rotating both or one of a pair of metal materials, the metal material generates frictional heat and softens, while the softened portion is stirred to cause plastic flow. Thus, a technique for joining metal materials is disclosed.

しかしながら、この技術は、接合対象とする金属材料を回転させるものであるから、接合する金属材料の形状や寸法に限界がある。   However, since this technique rotates the metal material to be joined, there is a limit to the shape and size of the metal material to be joined.

特許文献2には、被加工材よりも実質的に硬い材質からなるツールを被加工材の未接合部に挿入し、このツールを回転させながら移動させることにより、ツールと被加工材との間に生じる熱と塑性流動によって、被加工材を長手方向に連続的に接合する方法が開示されている。   In Patent Document 2, a tool made of a material that is substantially harder than a workpiece is inserted into an unjoined portion of the workpiece, and the tool is moved while being rotated. A method is disclosed in which workpieces are continuously joined in the longitudinal direction by heat and plastic flow.

特許文献1に記載された摩擦溶接法は、被加工材同士を回転させ、被加工材同士の摩擦熱によって溶接する方法である。特許文献2に開示された摩擦撹拌接合法は、接合部材を固定した状態で、ツールを回転させながら移動することにより接合する方法である。このように、摩擦撹拌接合法ではツールを移動させて接合するので溶接方向に対して実質的に無限に長い部材であっても、その長手方向に連続的に固相接合できる利点がある。また、ツールと接合部材との摩擦熱による金属の塑性流動を利用した固相接合であるので、接合部を溶融することなく接合できる。さらに、加熱温度が低いので接合後の変形が少なく、接合部は溶融されないので欠陥が少なく、加えて溶加材を必要としないなど多くの利点がある。   The friction welding method described in Patent Document 1 is a method in which workpieces are rotated and welded by frictional heat between workpieces. The friction stir welding method disclosed in Patent Document 2 is a method of joining by moving a tool while rotating a joining member in a fixed state. Thus, in the friction stir welding method, since the tool is moved and joined, even a member that is substantially infinitely long with respect to the welding direction has an advantage that it can be continuously solid-phase joined in the longitudinal direction. Moreover, since it is a solid-phase joining using the plastic flow of the metal by the frictional heat of a tool and a joining member, it can join, without melt | dissolving a junction part. Furthermore, since the heating temperature is low, deformation after joining is small, the joint is not melted, so there are few defects, and in addition, there are many advantages such as not requiring a filler material.

摩擦撹拌接合法は、アルミニウム合金やマグネシウム合金に代表される低融点金属材料の接合法として、航空機、船舶、鉄道車輌および自動車等の分野で利用が広がってきている。この理由としては、これらの低融点金属材料は、従来のアーク溶接法では接合部の満足な特性を得ることが難しく、摩擦撹拌接合法を適用することにより生産性が向上すると共に、品質の高い接合部を得ることができるからである。   The friction stir welding method is widely used in the fields of aircraft, ships, railway vehicles, automobiles and the like as a method of joining low melting point metal materials typified by aluminum alloys and magnesium alloys. The reason for this is that these low melting point metal materials are difficult to obtain satisfactory characteristics of the joints by conventional arc welding methods, and the productivity is improved and the quality is high by applying the friction stir welding method. It is because a junction can be obtained.

一方、建築物や船舶、重機、パイプライン、自動車といった構造物の素材として主に適用されている構造用鋼に対する摩擦撹拌接合法の適用は、従来の溶融溶接で課題となる凝固割れや水素割れを回避できるとともに、鋼材の組織変化をも抑制できるので、継手性能に優れることが期待できる。また、摩擦撹拌接合法では、回転ツールにより接合界面を撹拌することで清浄面を創出して清浄面同士を接触させるので、拡散接合のような前準備工程は不要であるという利点も期待できる。このように、構造用鋼に対する摩擦撹拌接合法の適用は、多くの利点が期待される。しかし、接合時における欠陥発生の抑制や接合速度の高速度化といった接合施工性に問題があることから、低融点金属材料と比較して構造用鋼では摩擦撹拌接合法の普及が進んでいない。   On the other hand, the application of friction stir welding to structural steel, which is mainly applied as a structural material such as buildings, ships, heavy machinery, pipelines, and automobiles, is subject to solidification cracking and hydrogen cracking, which are problems in conventional fusion welding. Can be avoided, and the structural change of the steel material can be suppressed, so that it can be expected that the joint performance is excellent. Further, in the friction stir welding method, a clean interface is created by stirring the bonding interface with a rotating tool and the clean surfaces are brought into contact with each other. Therefore, an advantage that a preparatory step such as diffusion bonding is unnecessary can be expected. Thus, the application of the friction stir welding method to structural steel is expected to have many advantages. However, since there is a problem in joining workability such as suppression of defect generation during joining and an increase in joining speed, the friction stir welding method has not been widely used in structural steel compared to low melting point metal materials.

構造用鋼の摩擦撹拌接合においては、特許文献3および特許文献4に記載されているように、回転ツールとして多結晶硼素窒化物(PCBN)や窒化珪素(Si)などの高耐磨耗性材料を用いている。これらのセラミックスは脆いので、回転ツールの破損を防止するために、接合する鋼板の板厚やその施工条件が著しく制限される。In friction stir welding of structural steel, as described in Patent Document 3 and Patent Document 4, high wear resistance such as polycrystalline boron nitride (PCBN) and silicon nitride (Si 3 N 4 ) is used as a rotating tool. Wearable material is used. Since these ceramics are brittle, the thickness of the steel plates to be joined and the construction conditions thereof are significantly limited in order to prevent damage to the rotary tool.

特許文献5および特許文献6には、接合施工性の向上を目的として、加熱手段を付加した接合方法が開示されている。   Patent Document 5 and Patent Document 6 disclose a joining method in which a heating means is added for the purpose of improving joining workability.

例えば、特許文献5には、誘導加熱装置を用いた加熱手段を有し、接合前後に被加工材の加熱を行うことで、接合速度の高速度化や接合部の割れの解消を図った摩擦撹拌接合法が開示されている。   For example, Patent Document 5 includes a heating unit using an induction heating device, and by heating the workpieces before and after joining, friction that increases the joining speed and eliminates cracks in the joined part. A stir welding method is disclosed.

特許文献6には、レーザ装置を用いた加熱手段を有し、接合直前に被加工材を部分的に加熱することで、予熱による加熱領域周辺のミクロ組織変化を抑制しつつ接合速度の高速度化を図った摩擦撹拌接合装置が開示されている。   Patent Document 6 has a heating means using a laser device, and the workpiece is partially heated immediately before joining, thereby suppressing the microstructure change around the heating region due to preheating and increasing the joining speed. A friction stir welding apparatus which is designed to be simplified is disclosed.

しかしながら、特許文献5および特許文献6の技術では、接合前の加熱による被加工材の加熱領域の表面温度や深さ等について考慮されておらず、そのため、十分な接合施工性が得られない。さらに、過剰加熱により加熱領域周辺のミクロ組織が変化し、接合継手特性、特に、接合継手強度に悪影響を及ぼす場合があった。   However, the techniques of Patent Document 5 and Patent Document 6 do not take into consideration the surface temperature, depth, and the like of the heated region of the workpieces by heating before bonding, and therefore, sufficient bonding workability cannot be obtained. Furthermore, the microstructure around the heating region may change due to overheating, which may adversely affect the properties of the joint joint, particularly the joint strength.

特許文献7には、接合直前に被加工材を部分的に加熱することに関して、加熱領域の位置、表面温度や深さ等について限定されており、十分な強度を得るとともに、接合施工性を向上させた摩擦撹拌接合方法が開示されている。しかしながら、被加工材の部分的な加熱の位置と、回転ツールの素材もしくは回転ツールの表面に被覆した素材と被接合材の間の動摩擦係数に支配される摩擦発熱との関係が接合施工性に及ぼす影響については何ら考慮されていない。   In Patent Document 7, the position of the heating region, the surface temperature, the depth, and the like are limited with respect to partially heating the workpieces immediately before bonding, and sufficient strength is obtained and the bonding workability is improved. A friction stir welding method is disclosed. However, the relationship between the position of partial heating of the workpiece and the frictional heat generated by the dynamic friction coefficient between the rotating tool material or the material coated on the surface of the rotating tool and the workpiece is effective for bonding workability. No influence is taken into account.

特開昭62−183979号公報JP 62-183979 A 特表平7−505090号公報JP 7-505090 Gazette 特表2003−532542号公報Special table 2003-532542 gazette 特表2003−532543号公報Japanese translation of PCT publication No. 2003-532543 特開2003−94175号公報JP 2003-94175 A 特開2005−288474号公報JP 2005-288474 A 国際公開第2015/045299号International Publication No. 2015/045299

本発明は、上記現状を鑑みてなされたもので、摩擦撹拌接合に際し、被加工材の加熱不足による塑性流動不良を解消して、十分な強度とともに、接合施工性の向上を図ることを目的とする。特に、被加工材の部分的な加熱の位置と、回転ツールの素材もしくは回転ツールの表面に被覆した素材と被接合材の間の動摩擦係数による摩擦発熱との関係が接合施工性に及ぼす影響を考慮し、予熱処理プロセス条件を厳密に精査した摩擦撹拌接合方法と当該摩擦撹拌接合方法を実現する装置を提供することを課題とする。   The present invention has been made in view of the above-mentioned present situation, and at the time of friction stir welding, an object of the present invention is to solve the plastic flow failure due to insufficient heating of work materials and to improve the joining workability with sufficient strength. To do. In particular, the relationship between the position of partial heating of the workpiece and the frictional heat generation due to the dynamic friction coefficient between the rotating tool material or the material coated on the surface of the rotating tool and the workpiece affects the workability. In view of this, it is an object of the present invention to provide a friction stir welding method in which the pre-heat treatment process conditions are closely scrutinized and an apparatus for realizing the friction stir welding method.

発明者らは、上記課題を解決すべく鋭意検討を重ねた結果、下記知見を得た。
a)通常の摩擦撹拌接合では、接合のために必要な熱源が、回転ツールと被加工材との間で発生する摩擦熱のみである。そのため、構造用鋼を摩擦撹拌接合法により接合する場合には、被加工材である構造用鋼を軟化させるために必要な熱量を十分に確保できない。その結果、接合部において十分な塑性流動が得られず、接合速度の低下や接合欠陥の発生などの接合施工性の劣化が懸念される。
The inventors obtained the following knowledge as a result of intensive studies to solve the above problems.
a) In ordinary friction stir welding, the only heat source required for welding is frictional heat generated between the rotary tool and the workpiece. Therefore, when the structural steel is joined by the friction stir welding method, the amount of heat necessary to soften the structural steel that is the workpiece cannot be secured. As a result, a sufficient plastic flow cannot be obtained at the joint, and there is a concern about the deterioration of joining workability such as a reduction in joining speed and the occurrence of joining defects.

上記技術を工業化する上で非常に重要となる接合施工性の劣化を回避するには、摩擦撹拌接合前の予熱処理プロセスが有効であると考えられる。
b)しかしながら、摩擦撹拌接合前の予熱処理プロセスを行う際に、予熱熱量が過剰になると、加熱領域周辺のミクロ組織が変化する問題が生じる。特に、マルテンサイト組織により強化された高張力鋼板の場合は、加熱領域周辺が、フェライト−オーステナイト変態温度以下での加熱であっても、マルテンサイトが焼き戻されることで軟化が生じ、接合継手強度を著しく低下させる。
In order to avoid the deterioration of joining workability, which is very important in industrializing the above technology, it is considered that a pre-heat treatment process before friction stir welding is effective.
b) However, when the preheating heat amount before the friction stir welding is performed, if the amount of preheating heat is excessive, there arises a problem that the microstructure around the heating region changes. In particular, in the case of a high-tensile steel sheet strengthened with a martensite structure, even when the periphery of the heating region is heated below the ferrite-austenite transformation temperature, softening occurs due to tempering of the martensite, and the joint joint strength Is significantly reduced.

そこで、発明者らは、摩擦撹拌接合前の予熱処理プロセス条件について種々検討した。   Therefore, the inventors examined various preheat treatment process conditions before friction stir welding.

その結果、
c)レーザなどのエネルギー密度の高い熱源を用いることで、予熱処理プロセスでの加熱領域の表面温度、面積、位置を厳密に制御し、また必要に応じて加熱領域の厚さ方向における温度についても適正に制御する。それにより、接合継手強度等の接合継手特性の劣化を招くことなく、接合施工性を向上できるとの知見を得た。
d)特に、上記の被加工材の部分的な加熱の位置に関しては、回転ツールの素材もしくは回転ツールの表面に被覆した素材と被接合材の間の動摩擦係数に支配される摩擦発熱との関係により、接合施工性を向上する効果が生じる領域が変化するとの知見を得た。
e)通常の摩擦撹拌接合では、接合完了後、接合部が自然放冷状態となるので、鋼材製造時の圧延プロセスで行われているような熱履歴管理によるミクロ組織制御を適用できないという問題があった。しかし、接合完了直後に、接合部に対し、加熱処理や冷却処理を組み合わせたプロセスを実施することで、接合継手特性をさらに向上できるとの知見を得た。
as a result,
c) By using a heat source with a high energy density such as a laser, the surface temperature, area, and position of the heating region in the pre-heat treatment process are strictly controlled, and the temperature in the thickness direction of the heating region is also adjusted as necessary. Control appropriately. As a result, it has been found that the joining workability can be improved without causing deterioration of the jointed joint properties such as the jointed joint strength.
d) In particular, with respect to the position of partial heating of the workpiece, the relationship between the frictional heating controlled by the dynamic friction coefficient between the workpiece of the rotary tool or the material coated on the surface of the rotary tool and the workpiece. Thus, the knowledge that the region where the effect of improving the bonding workability is generated is obtained.
e) In normal friction stir welding, since the joint is naturally cooled after the completion of joining, there is a problem that the microstructure control by thermal history management that is performed in the rolling process at the time of steel production cannot be applied. there were. However, immediately after the completion of the joining, it was found that the joint joint characteristics can be further improved by performing a process that combines heat treatment and cooling treatment on the joint.

本発明は、上記知見に立脚するものであり、特に、摩擦撹拌接合方法を構造用鋼の接合に適用した場合に懸念される、被加工材の加熱不足による塑性流動不良を解消して、十分な強度と共に、接合施工性の向上を図るものである。   The present invention is based on the above knowledge, and in particular, when the friction stir welding method is applied to the joining of structural steel, the plastic flow failure due to insufficient heating of the work material is solved, and sufficient In addition to high strength, it is intended to improve the joining workability.

すなわち、本発明の要旨構成は次のとおりである。
[1]肩部と、該肩部に配され、該肩部と回転軸を共有するピン部と、を含み、前記肩部および前記ピン部が被加工材である鋼板よりも硬い材質からなる回転ツールを、鋼板間の未接合部に挿入して回転させながら接合方向に移動させ、前記回転ツールと前記鋼板との摩擦熱により前記鋼板を軟化させつつ、その軟化した部位を前記回転ツールで撹拌することにより塑性流動を生じさせて鋼板同士を接合する摩擦撹拌接合方法であって、前記回転ツールの素材、もしくは前記回転ツールの表面に被覆された素材と前記鋼板との動摩擦係数がは0.6以下であり、前記回転ツールの接合方向前方に設けられた加熱手段により加熱された前記鋼板の表面の温度T(℃)が下記式(1)を満足する領域を加熱領域としたとき、前記加熱領域と前記回転ツールとの最小距離は、前記回転ツールの肩部の直径以下であり、前記加熱領域の面積は、前記回転ツールのピン部の最大径部の面積以下であり、前記加熱領域の面積の65%以上は、前記鋼板の表面における前記回転ツールの回転軸を通り接合方向に平行な直線である接合中央線と、該接合中央線に平行で、かつリトリーティングサイドへ前記回転ツールのピン部の最大半径と同じ距離だけ隔てた直線と、の間に位置する摩擦撹拌接合方法。
≧0.8×TA1・・・(1)
A1は、下記式(2)で示される温度である。
A1(℃)=723−10.7[%Mn]−16.9[%Ni]+29.1[%Si]+16.9[%Cr]+290[%As]+6.38[%W]・・・(2)
上記[%M]は、被加工材である鋼板におけるM元素の含有量(質量%)であり、含有しない場合は0とする。
[2]前記加熱領域の厚さ方向の温度T(℃)が下記式(3)を満足する領域における前記鋼板の表面からの最大深さを加熱領域の深さDとしたとき、前記加熱領域の深さDは、前記鋼板の厚さの30%以上である請求項1に記載の摩擦撹拌接合方法。
≧0.8×TA1・・・(3)
[3]前記加熱手段は、レーザ加熱装置である[1]または[2]に記載の摩擦撹拌接合方法。
[4]前記回転ツールの接合方向後方には後方加熱手段が設けられており、該後方加熱手段は、前記鋼板の接合部を加熱する[1]から[3]のいずれか1つに記載の摩擦撹拌接合方法。
[5]前記後方加熱手段の接合方向後方には冷却手段が設けられており、該冷却手段は、前記後方加熱手段により加熱された前記接合部を冷却する[4]に記載の摩擦撹拌接合方法。
[6]前記回転ツールの接合方向後方には冷却手段が設けられており、該冷却手段は、前記鋼板の接合部を冷却する[1]から[3]のいずれか1つに記載の摩擦撹拌接合方法。
[7]前記冷却手段の接合方向後方には後方加熱手段が設けられており、該後方加熱手段は、前記冷却手段により冷却された前記接合部を加熱する[6]に記載の摩擦撹拌接合方法。
[8]被加工材である鋼板間の未接合部を接合する摩擦撹拌接合装置であって、肩部と、該肩部に配され、該肩部と回転軸を共有するピン部と、を含み、前記肩部および前記ピン部は、前記鋼板よりも硬い材質からなり、前記鋼板間の未接合部に挿入された状態で回転しながら接合方向に移動することで、摩擦熱により前記鋼板を軟化させつつ、その軟化した部位を撹拌することにより塑性流動を生じさせる回転ツールと、該回転ツールの接合方向前方に設けられ、前記鋼板を加熱する加熱手段と、下記状態1を実現するように前記回転ツール及び前記加熱手段を制御する制御手段と、を有し、前記回転ツールの素材、もしくは前記回転ツールの表面に被覆した素材と前記鋼板との動摩擦係数は0.6以下である摩擦撹拌接合装置。
(状態1)
前記加熱手段により加熱された前記鋼板の表面の温度T(℃)が下記式(1)を満足する領域を加熱領域としたとき、前記加熱領域と前記回転ツールとの最小距離は、前記回転ツールの肩部の直径以下であり、前記加熱領域の面積は、前記回転ツールのピン部の最大径部の面積以下であり、前記加熱領域の面積の65%以上は、前記鋼板の表面における前記回転ツールの回転軸を通り接合方向に平行な直線である接合中央線と、該接合中央線に平行で、かつリトリーティングサイドへ前記回転ツールのピン部の最大半径と同じ距離だけ隔てた直線と、の間に位置する。
≧0.8×TA1・・・(1)
A1は、下記式(2)で示される温度である。
A1(℃)=723−10.7[%Mn]−16.9[%Ni]+29.1[%Si]+16.9[%Cr]+290[%As]+6.38[%W]・・・(2)
上記[%M]は、被加工材である鋼板におけるM元素の含有量(質量%)であり、含有しない場合は0とする。
[9]前記制御手段は、以下の状態2を実現するように前記回転ツール及び前記加熱手段を制御する[8]に記載の摩擦撹拌接合装置。
(状態2)
前記加熱領域の厚さ方向の温度T(℃)が下記式(3)を満足する領域における前記鋼板の表面からの最大深さを加熱領域の深さDとしたとき、前記加熱領域の深さDがは、前記鋼板の厚さの30%以上である。
≧0.8×TA1・・・(3)
[10]前記加熱手段は、レーザ加熱装置である[8]または[9]に記載の摩擦撹拌接合装置。
[11]前記鋼板の接合部を加熱する後方加熱手段をさらに有し、該後方加熱手段は、前記回転ツールの接合方向後方に設けられる[8]から[10]のいずれか1つに記載の摩擦撹拌接合装置。
[12]前記接合部を冷却する冷却手段をさらに有し、該冷却手段は、前記後方加熱手段の接合方向後方に設けられる[11]に記載の摩擦撹拌接合装置。
[13]前記鋼板の接合部を冷却する冷却手段をさらに有し、該冷却手段は、前記回転ツールの接合方向後方に設けられる[8]から[10]のいずれか1つに記載の摩擦撹拌接合装置。
[14]前記接合部を加熱する後方加熱手段をさらに有し、該後方加熱手段は、前記冷却手段の接合方向後方に設けられる[13]に記載の摩擦撹拌接合装置。
That is, the gist configuration of the present invention is as follows.
[1] A shoulder portion and a pin portion that is arranged on the shoulder portion and shares the rotation axis with the shoulder portion, and the shoulder portion and the pin portion are made of a material harder than a steel plate that is a workpiece. The rotating tool is inserted into an unjoined portion between the steel plates and rotated to move in the joining direction, and the softened portion is softened by the frictional heat between the rotating tool and the steel plate while the softened part is moved with the rotating tool. A friction stir welding method in which steel plates are joined to each other by causing plastic flow by stirring, and the dynamic friction coefficient between the material of the rotating tool or the material coated on the surface of the rotating tool and the steel plate is 0. .6 or less, and a region where the surface temperature T S (° C.) of the steel sheet heated by the heating means provided in front of the rotating tool in the joining direction satisfies the following formula (1) is defined as a heating region. The heating area and the front The minimum distance to the rotating tool is not more than the diameter of the shoulder of the rotating tool, the area of the heating region is not more than the area of the maximum diameter portion of the pin portion of the rotating tool, and is 65% of the area of the heating region. % Of the surface of the steel plate is a straight line that passes through the rotation axis of the rotary tool and is parallel to the welding direction, and is parallel to the welding center line and to the retreating side of the pin portion of the rotary tool. A friction stir welding method located between a straight line separated by the same distance as the maximum radius.
T S ≧ 0.8 × T A1 (1)
T A1 is a temperature represented by the following formula (2).
T A1 (° C.) = 723-10.7 [% Mn] −16.9 [% Ni] +29.1 [% Si] +16.9 [% Cr] +290 [% As] +6.38 [% W] · (2)
Said [% M] is content (mass%) of M element in the steel plate which is a workpiece, and is set to 0 when not containing.
[2] When the maximum depth from the surface of the steel sheet in the region where the temperature T D (° C.) in the thickness direction of the heating region satisfies the following formula (3) is the depth D of the heating region, the heating The friction stir welding method according to claim 1, wherein the depth D of the region is 30% or more of the thickness of the steel plate.
T D ≧ 0.8 × T A1 (3)
[3] The friction stir welding method according to [1] or [2], wherein the heating means is a laser heating device.
[4] Back heating means is provided at the rear of the rotating tool in the joining direction, and the rear heating means heats the joining portion of the steel sheet according to any one of [1] to [3]. Friction stir welding method.
[5] A friction stir welding method according to [4], wherein a cooling means is provided behind the rear heating means in the joining direction, and the cooling means cools the joint heated by the rear heating means. .
[6] A cooling means is provided behind the rotating tool in the joining direction, and the cooling means cools the joining portion of the steel sheet. Friction stirring according to any one of [1] to [3] Joining method.
[7] A friction stir welding method according to [6], wherein a rear heating unit is provided behind the cooling unit in the joining direction, and the rear heating unit heats the joint cooled by the cooling unit. .
[8] A friction stir welding apparatus for joining unjoined portions between steel plates as workpieces, comprising a shoulder portion and a pin portion arranged on the shoulder portion and sharing the rotation axis with the shoulder portion. The shoulder portion and the pin portion are made of a material harder than the steel plate, and move in the joining direction while rotating in a state where the shoulder portion and the pin portion are inserted in the unjoined portion between the steel plates, so that the steel plate is caused by frictional heat. A rotating tool that causes plastic flow by stirring the softened portion while being softened, a heating unit that is provided in front of the rotating tool in the joining direction, and that heats the steel sheet, and realizes the following state 1 A friction stir that has a dynamic friction coefficient of 0.6 or less between the material of the rotary tool or the material coated on the surface of the rotary tool and the steel plate. Joining device.
(State 1)
When a region where the surface temperature T S (° C.) of the steel sheet heated by the heating unit satisfies the following formula (1) is a heating region, the minimum distance between the heating region and the rotating tool is the rotation It is not more than the diameter of the shoulder portion of the tool, the area of the heating region is not more than the area of the maximum diameter portion of the pin portion of the rotating tool, and 65% or more of the area of the heating region is the surface of the steel plate A joint center line that is a straight line that passes through the rotation axis of the rotary tool and is parallel to the joint direction, and a straight line that is parallel to the joint center line and separated from the retreating side by the same distance as the maximum radius of the pin portion of the rotary tool. , Located between.
T S ≧ 0.8 × T A1 (1)
T A1 is a temperature represented by the following formula (2).
T A1 (° C.) = 723-10.7 [% Mn] −16.9 [% Ni] +29.1 [% Si] +16.9 [% Cr] +290 [% As] +6.38 [% W] · (2)
Said [% M] is content (mass%) of M element in the steel plate which is a workpiece, and is set to 0 when not containing.
[9] The friction stir welding apparatus according to [8], wherein the control unit controls the rotating tool and the heating unit so as to realize the following state 2.
(State 2)
When the maximum depth from the surface of the steel sheet in the region where the temperature T D (° C.) in the thickness direction of the heating region satisfies the following formula (3) is the depth D of the heating region, the depth of the heating region The thickness D is 30% or more of the thickness of the steel plate.
T D ≧ 0.8 × T A1 (3)
[10] The friction stir welding apparatus according to [8] or [9], wherein the heating means is a laser heating apparatus.
[11] The apparatus according to any one of [8] to [10], further including a rear heating unit that heats the joint portion of the steel plates, the rear heating unit provided at a rear side in the joining direction of the rotary tool. Friction stir welding device.
[12] The friction stir welding apparatus according to [11], further including a cooling unit that cools the joint, and the cooling unit is provided behind the rear heating unit in the joining direction.
[13] The friction stirrer according to any one of [8] to [10], further including a cooling unit that cools a bonded portion of the steel plates, the cooling unit being provided at the rear in the bonding direction of the rotary tool. Joining device.
[14] The friction stir welding apparatus according to [13], further including a rear heating unit that heats the joint, and the rear heating unit is provided behind the cooling unit in the joining direction.

本発明によれば、被加工材の加熱不足による塑性流動不良を解消して、摩擦撹拌接合の接合施工性の向上を図ることができる。さらには、加熱領域周辺のミクロ組織の変化も抑制して、接合部において高い継手強度を得ることができる。   ADVANTAGE OF THE INVENTION According to this invention, the plastic flow failure by underheating of a workpiece can be eliminated, and the joining workability of friction stir welding can be improved. Furthermore, a change in the microstructure around the heating region is also suppressed, and a high joint strength can be obtained at the joint.

図1は、本実施形態に係る摩擦撹拌接合方法を説明する概略図である。FIG. 1 is a schematic diagram illustrating a friction stir welding method according to the present embodiment. 図2は、予熱プロセスにおける加熱領域、接合後に行ったプロセスにおける冷却領域および再加熱領域の一例を示す図(上面図およびA−A断面図)である。FIG. 2 is a diagram (top view and AA sectional view) showing an example of a heating region in a preheating process, a cooling region and a reheating region in a process performed after bonding. 図3は、本実施形態に係る摩擦撹拌接合方法で接合する鋼板の温度と引張強さの関係を示す図である。FIG. 3 is a diagram showing the relationship between the temperature and tensile strength of the steel plates to be joined by the friction stir welding method according to this embodiment. 図4は、回転ツールの断面寸法を示す図である。FIG. 4 is a diagram showing a cross-sectional dimension of the rotary tool.

以下、本発明を本発明の実施形態を通じて具体的に説明する。図1は、本実施形態に係る摩擦撹拌接合方法および摩擦撹拌接合装置を説明する概略図である。本実施形態に係る擦撹拌接合方法では、図1に示すように、回転ツールを、鋼板間の未接合部に挿入して回転させながら接合方向に移動させ、回転ツールと鋼板との摩擦熱により該鋼板を軟化させつつ、その軟化した部位を回転ツールで撹拌することにより塑性流動を生じさせて、鋼板同士を接合する。ここで、回転ツールは、肩部と、この肩部に配され、この肩部と回転軸を共有するピン部と、を含み、少なくとも肩部およびピン部は被加工材である鋼板よりも硬い材質により形成される。 Hereinafter, the present invention will be specifically described through embodiments of the present invention. FIG. 1 is a schematic diagram illustrating a friction stir welding method and a friction stir welding apparatus according to the present embodiment. The friction stir welding method according to the present embodiment, as shown in FIG. 1, the rotary tool is moved in the welding direction while rotating and inserted to the unwelded portion between the steel plate, the frictional heat between the rotational tool and the steel sheet While the steel plates are softened by the above, the softened portion is stirred with a rotating tool to cause plastic flow, thereby joining the steel plates together. Here, the rotating tool includes a shoulder portion and a pin portion that is arranged on the shoulder portion and shares the rotation axis with the shoulder portion, and at least the shoulder portion and the pin portion are harder than the steel plate that is the workpiece. It is formed by the material.

図1中、符号1は回転ツールであり、2は回転軸であり、3は鋼板であり、4は接合部であり、5は加熱手段であり、6は冷却手段であり、7は後方加熱手段であり、8は回転ツールの肩部であり、9は回転ツールのピン部であり、15は制御手段である。αは回転ツールの傾斜角度を示す。「AS」は、アドバンシングサイドを示し、「RS」は、リトリーティングサイドを示す。ここで、アドバンシングサイドとは、ツール回転方向と接合方向が一致する側であり、リトリーティングサイドとは、ツール回転方向と接合方向が反対となる側であるとそれぞれ定義する。   In FIG. 1, reference numeral 1 is a rotary tool, 2 is a rotating shaft, 3 is a steel plate, 4 is a joint, 5 is a heating means, 6 is a cooling means, and 7 is backward heating. Means 8, a shoulder of the rotary tool, 9 a pin part of the rotary tool, and 15 a control means. α indicates the tilt angle of the rotating tool. “AS” indicates an advancing side, and “RS” indicates a retreating side. Here, the advancing side is defined as the side where the tool rotation direction and the joining direction coincide with each other, and the retreating side is defined as the side where the tool rotation direction and the joining direction are opposite to each other.

本実施形態では、鋼板3を突き合わせただけで未だ接合されていない状態にある突き合わせ部分を「未接合部」と記載し、塑性流動により接合されて一体化された部分を「接合部」と記載する。   In the present embodiment, the butted portion that is not yet joined just by butting the steel plates 3 is described as “unjoined portion”, and the portion joined and integrated by plastic flow is described as “joined portion”. To do.

本実施形態の摩擦撹拌接合方法では、接合方向へ移動する回転ツール1の前方に設けた加熱手段5により鋼板3を加熱する予熱処理プロセスが重要である。以下、この予熱処理プロセスの条件を、図2を参照しながら説明する。   In the friction stir welding method of this embodiment, a preheat treatment process in which the steel plate 3 is heated by the heating means 5 provided in front of the rotary tool 1 moving in the joining direction is important. Hereinafter, the conditions of the pre-heat treatment process will be described with reference to FIG.

図2は、予熱プロセスにおける加熱領域、接合後に行ったプロセスにおける冷却領域および再加熱領域の一例を示す図(上面図およびA−A断面図)である。図2中、接合中央線10は、鋼板3の表面における回転ツール1の回転軸2を通り接合方向に平行な直線を示す。RS線11は、接合中央線10に平行で、かつリトリーティングサイドへ回転ツールのピン部9の最大半径と同じ距離だけ隔てた直線であり、12は加熱領域であり、13は冷却領域であり、14は再加熱領域である。aは回転ツールの肩部8の直径を示し、bは回転ツールのピン部9の最大径を示し、Xは加熱領域12と回転ツール1との最小距離を示し、Dは加熱領域12の深さを示し、tは鋼板3の厚さを示す。   FIG. 2 is a diagram (top view and AA sectional view) showing an example of a heating region in a preheating process, a cooling region and a reheating region in a process performed after bonding. In FIG. 2, the joining center line 10 indicates a straight line passing through the rotation axis 2 of the rotary tool 1 on the surface of the steel plate 3 and parallel to the joining direction. The RS line 11 is a straight line parallel to the joining center line 10 and separated to the retreating side by the same distance as the maximum radius of the pin portion 9 of the rotary tool, 12 is a heating area, and 13 is a cooling area. , 14 is a reheating region. a indicates the diameter of the shoulder 8 of the rotary tool, b indicates the maximum diameter of the pin portion 9 of the rotary tool, X indicates the minimum distance between the heating region 12 and the rotary tool 1, and D indicates the depth of the heating region 12. T indicates the thickness of the steel plate 3.

加熱領域における鋼板の表面温度T:T≧0.8×TA1
図3は、本実施形態に係る摩擦撹拌接合方法で接合する鋼板の温度と引張強さの関係を示す図である。本実施形態の摩擦撹拌接合方法で接合する鋼板3は、図3に示すように、通常、鋼の変態温度であるTA1の80%程度の温度では、常温時の強度の30%程度の強度となる。また、この温度より高くなると、銅板3の強度はさらに低下する。よって、鋼板3の表面温度Tが0.8×TA1℃以上を満足するように鋼板3を予め軟化させ、当該鋼板3を撹拌し、塑性流動を促進する。これにより、回転ツール1にかかる負荷が低減され、接合速度を高速度化できる。このため、本実施形態における摩擦撹拌接合方法では、鋼板3の表面温度Tが下記式(1)を満足する領域を加熱領域12とする。
Surface temperature T S of steel plate in heating region: T S ≧ 0.8 × T A1
FIG. 3 is a diagram showing the relationship between the temperature and tensile strength of the steel plates to be joined by the friction stir welding method according to this embodiment. As shown in FIG. 3, the steel plate 3 to be joined by the friction stir welding method of the present embodiment is generally about 30% strength at room temperature at a temperature of about 80% of TA1 , which is the transformation temperature of steel. It becomes. Moreover, when it becomes higher than this temperature, the intensity | strength of the copper plate 3 will fall further. Therefore, the steel plate 3 is previously softened so that the surface temperature T S of the steel plate 3 satisfy the above 0.8 × T A1 ° C., and stirred the steel plate 3, to promote plastic flow. Thereby, the load concerning the rotary tool 1 is reduced and the joining speed can be increased. Therefore, in the friction stir welding method in this embodiment, the surface temperature T S of the steel plate 3 is the heating region 12 a region which satisfies the following formula (1).

≧0.8×TA1・・・(1)
鋼の変態温度TA1(℃)は、下記式(2)により求めることができる。
T S ≧ 0.8 × T A1 (1)
The transformation temperature T A1 (° C.) of steel can be obtained by the following formula (2).

A1(℃)=723−10.7[%Mn]−16.9[%Ni]+29.1[%Si]+16.9[%Cr]+290[%As]+6.38[%W]・・・(2)
上記[%M]は、被加工材である鋼板3におけるM元素の含有量(質量%)であり、含有しない場合は0とする。
T A1 (° C.) = 723-10.7 [% Mn] −16.9 [% Ni] +29.1 [% Si] +16.9 [% Cr] +290 [% As] +6.38 [% W] · (2)
Said [% M] is content (mass%) of M element in the steel plate 3 which is a workpiece, and is set to 0 when not containing.

0.8×TA1℃超では温度の上昇と共に鋼板3の強度が低下する傾向があるので、加熱領域12における鋼板3の表面温度Tが上昇し過ぎないように調節することが好ましい。具体的に、厚さ方向へ加熱領域12を確保するには加熱領域12の表面に温度勾配(表面における温度のばらつき)が存在しても良いが、その場合、加熱領域12において鋼板3の最も高い表面温度は1.5×T℃以下であることが好ましい。さらに、加熱領域12における鋼板3の表面温度を、加熱領域12を通過する回転ツール1と接触するまでにT℃未満にすることが好ましい。これにより、接合部4の温度が過度に上昇することによる回転ツール1の損傷や、加熱領域12の周辺のミクロ組織の変質を避けることができる。TM(℃)は被加工材である鋼板3の融点である。If the temperature exceeds 0.8 × T A1 ° C., the strength of the steel plate 3 tends to decrease as the temperature increases. Therefore, it is preferable to adjust so that the surface temperature T S of the steel plate 3 in the heating region 12 does not increase excessively. Specifically, in order to secure the heating region 12 in the thickness direction, a temperature gradient (temperature variation on the surface) may exist on the surface of the heating region 12. The high surface temperature is preferably 1.5 × T M ° C. or less. Furthermore, it is preferable that the surface temperature of the steel plate 3 in the heating region 12 is less than T M ° C. before contacting the rotary tool 1 that passes through the heating region 12. Thereby, the damage of the rotary tool 1 and the alteration of the microstructure around the heating region 12 due to an excessive increase in the temperature of the joint 4 can be avoided. T M (° C.) is the melting point of the steel plate 3 as the workpiece.

鋼板の表面における加熱領域と回転ツールとの最小距離X:回転ツールの肩部の直径以下
鋼板3の表面における加熱領域12と回転ツール1との最小距離Xが大きくなり過ぎると、接合前に加熱領域12における温度が低下し、予熱による効果が十分に得られない。このため、本実施形態に係る摩擦撹拌接合方法において、鋼板3の表面における加熱領域12と接合方向へ移動する回転ツール1との最小距離Xは、回転ツールの肩部8の直径以下である。
Minimum distance X between the heating region on the surface of the steel plate and the rotating tool: less than the diameter of the shoulder of the rotating tool If the minimum distance X between the heating region 12 on the surface of the steel plate 3 and the rotating tool 1 becomes too large, heating is performed before joining. The temperature in the region 12 is lowered and the effect of preheating is not sufficiently obtained. For this reason, in the friction stir welding method according to the present embodiment, the minimum distance X between the heating region 12 on the surface of the steel plate 3 and the rotary tool 1 moving in the joining direction is equal to or less than the diameter of the shoulder 8 of the rotary tool.

ただし、加熱領域12と回転ツール1との最小距離Xが小さくなり過ぎると、回転ツール1が加熱手段5による熱で損傷する恐れがあるので、鋼板3の表面における加熱領域12と接合方向へ移動する回転ツール1との最小距離Xは、回転ツールの肩部8の直径の0.1倍以上であることが好ましい。本実施形態における回転ツールの肩部8の直径は、例えば、8〜60mm程度である。予熱による効果を十分に得るために、回転ツール1の移動速度は、200mm/min以上3000mm/min以下であることが好ましい。   However, if the minimum distance X between the heating region 12 and the rotating tool 1 becomes too small, the rotating tool 1 may be damaged by the heat of the heating means 5, so that it moves in the joining direction with the heating region 12 on the surface of the steel plate 3. The minimum distance X to the rotating tool 1 is preferably 0.1 times or more the diameter of the shoulder 8 of the rotating tool. The diameter of the shoulder 8 of the rotary tool in this embodiment is, for example, about 8 to 60 mm. In order to sufficiently obtain the effect of preheating, the moving speed of the rotary tool 1 is preferably 200 mm / min or more and 3000 mm / min or less.

鋼板の表面における加熱領域の面積:回転ツールのピン部の最大径部の面積以下
加熱領域12が大きくなり過ぎると加熱領域12およびその周辺領域のミクロ組織が変化する。特に、マルテンサイト組織により強化された高張力鋼板の場合は、フェライト−オーステナイト変態温度以下での加熱であっても、マルテンサイトが焼き戻されることで軟化を生じ、接合継手強度を大幅に低下させる。このため、本実施形態に係る摩擦撹拌接合方法において、鋼板3の表面における加熱領域12の面積は、回転ツールのピン部9の最大径部の面積以下である。
The area of the heating region on the surface of the steel sheet: not more than the area of the maximum diameter portion of the pin portion of the rotating tool When the heating region 12 becomes too large, the microstructure of the heating region 12 and its peripheral region changes. In particular, in the case of a high-tensile steel sheet strengthened by a martensite structure, even when heating at a temperature below the ferrite-austenite transformation temperature, the martensite is tempered to cause softening and greatly reduce the joint strength. . For this reason, in the friction stir welding method according to the present embodiment, the area of the heating region 12 on the surface of the steel plate 3 is equal to or less than the area of the maximum diameter portion of the pin portion 9 of the rotary tool.

一方、加熱領域12の面積が小さくなりすぎると、予熱による効果が十分に得られなくなる。よって、鋼板3の表面における加熱領域12の面積は、回転ツールのピン部9における最大径部の面積の0.1倍以上であることが好ましい。   On the other hand, if the area of the heating region 12 becomes too small, the effect of preheating cannot be sufficiently obtained. Therefore, the area of the heating region 12 on the surface of the steel plate 3 is preferably 0.1 times or more the area of the maximum diameter portion in the pin portion 9 of the rotary tool.

本実施形態における回転ツールのピン部9の最大径は、例えば、2〜50mm程度である。回転ツールのピン部9の最大径は、1つのピン部を軸線方向と垂直な断面で切断した際の切断面で得られる直径のうち最大のものである。   The maximum diameter of the pin portion 9 of the rotary tool in the present embodiment is, for example, about 2 to 50 mm. The maximum diameter of the pin portion 9 of the rotary tool is the maximum diameter among the diameters obtained at the cut surface when one pin portion is cut in a cross section perpendicular to the axial direction.

図4は、回転ツールの断面寸法を示す図である。図4に示すように、回転ツールのピン部9の直径が軸線方向に沿って変わらない場合には、回転ツールのピン部9の上面の直径(図では4mm)を回転ツールのピン部9の最大径としてよい。回転ツールのピン部9がテーパ形状等を有し、軸線方向の位置によってピン径が異なる場合には、最も大きい直径を回転ツールのピン部9の最大径としてよい。図4の符号cは、プローブ長さを示し、プローブ長さとは、回転ツールのピン部9の先端部と、回転ツールの肩部8の最も高い位置との間の高さの差で算出される長さである。   FIG. 4 is a diagram showing a cross-sectional dimension of the rotary tool. As shown in FIG. 4, when the diameter of the pin portion 9 of the rotary tool does not change along the axial direction, the diameter (4 mm in the figure) of the pin portion 9 of the rotary tool is set to the diameter of the pin portion 9 of the rotary tool. The maximum diameter may be used. When the pin portion 9 of the rotating tool has a taper shape or the like and the pin diameter varies depending on the position in the axial direction, the largest diameter may be the maximum diameter of the pin portion 9 of the rotating tool. 4 indicates the probe length, and the probe length is calculated by the difference in height between the tip portion of the pin portion 9 of the rotary tool and the highest position of the shoulder portion 8 of the rotary tool. Length.

加熱領域12の形状は、円形、楕円形、矩形など任意の形状であってよい。回転ツールのピン部9の最大径部の形状は、通常、円形又は楕円形である。   The shape of the heating region 12 may be any shape such as a circle, an ellipse, or a rectangle. The shape of the maximum diameter portion of the pin portion 9 of the rotary tool is usually circular or elliptical.

鋼板の表面において、接合中央線とRS線との間に位置する加熱領域の面積:鋼板の表面における加熱領域の面積の65%以上
鋼板3の摩擦撹拌接合において、塑性流動はアドバンシングサイドを始点として、回転ツール1の回転方向に沿って、接合方向前方、リトリーティングサイド、接合方向後方を通り、アドバンシングサイドが終点となる。アドバンシングサイドは、塑性流動の始点となるので、被加工材である鋼板3の加熱不足が生じ易い。このため、塑性流動が不十分で欠陥が発生する場合には、その殆どがアドバンシングサイドで発生する。従って、鋼板3の表面において、アドバンシングサイドを優先的に加熱し、鋼板を軟化させることで塑性流動を促進し、欠陥の発生を抑え、接合速度の高速度化を図ることができる。
On the surface of the steel plate, the area of the heating region located between the joining center line and the RS wire: 65% or more of the area of the heating region on the surface of the steel plate In the friction stir welding of the steel plate 3, the plastic flow starts from the advanced side As described above, along the rotational direction of the rotary tool 1, it passes through the joining direction front, the retreating side, and the joining direction rear, and the advanced side is the end point. Since the advanced side is the starting point of plastic flow, insufficient heating of the steel plate 3 as the workpiece is likely to occur. For this reason, when plastic flow is insufficient and defects occur, most of them occur on the advanced side. Therefore, on the surface of the steel plate 3, the advancing side is preferentially heated and the steel plate is softened to promote plastic flow, suppress the occurrence of defects, and increase the joining speed.

しかしながら、回転ツール1の素材、もしくは回転ツール1の表面に被覆した素材と被接合材である鋼板3との動摩擦係数が0.6以下である場合は、回転ツール1と鋼板3との間に生じる摩擦熱、塑性流動が小さくなる。アドバンシングサイドは、回転ツール1の前方において塑性流動の始点となる部位であり回転ツール1と鋼板3との間の摩擦熱が大きく発生する領域である。しかしながら、高温状態では動摩擦係数は減少する傾向があるので、この部位を予熱により高温とすると、回転ツール1と鋼板3との動摩擦係数が小さい場合、十分な摩擦発熱が得られない。一方、リトリーティングサイドは、塑性流動の中間に位置するので、この位置での塑性流動が不十分となると、塑性流動の終点となるアドバンシングサイドでの欠陥の発生に大きな影響を及ぼす。特に回転ツール1と鋼板3との動摩擦係数が小さい場合には、十分な塑性流動が得られない。   However, when the dynamic friction coefficient between the material of the rotary tool 1 or the material coated on the surface of the rotary tool 1 and the steel plate 3 to be joined is 0.6 or less, it is between the rotary tool 1 and the steel plate 3. The generated frictional heat and plastic flow are reduced. The advanced side is a region that is a starting point of plastic flow in front of the rotary tool 1 and is a region where frictional heat between the rotary tool 1 and the steel plate 3 is greatly generated. However, since the dynamic friction coefficient tends to decrease in a high temperature state, if this part is heated to a high temperature by preheating, if the dynamic friction coefficient between the rotary tool 1 and the steel plate 3 is small, sufficient frictional heat generation cannot be obtained. On the other hand, since the retreating side is located in the middle of the plastic flow, if the plastic flow at this position becomes insufficient, the occurrence of defects on the advanced side that is the end point of the plastic flow is greatly affected. In particular, when the dynamic friction coefficient between the rotary tool 1 and the steel plate 3 is small, sufficient plastic flow cannot be obtained.

従って、回転ツール1の素材、もしくは回転ツール1の表面に被覆した素材と鋼板3との動摩擦係数が0.6以下である場合には、鋼板3の表面において、加熱領域12の面積の65%以上を、接合中央線10と、接合中央線10に平行なRS線11との間に位置させ、リトリーティングサイドを優先的に加熱する。これにより、塑性流動の始点となるアドバンシングサイドでの摩擦発熱を確保しながら、塑性流動の中間となるリトリーティングサイドでの塑性流動を促進し、欠陥の発生を抑え、接合速度の高速化を図ることができる。接合中央線10とRS線11との間に位置する加熱領域12の面積の範囲は、70%以上であることが好ましく、80%以上であることがより好ましく、100%であってもよい。   Accordingly, when the dynamic friction coefficient between the material of the rotary tool 1 or the material coated on the surface of the rotary tool 1 and the steel plate 3 is 0.6 or less, 65% of the area of the heating region 12 on the surface of the steel plate 3. The above is positioned between the junction center line 10 and the RS wire 11 parallel to the junction center line 10 to preferentially heat the retreating side. This promotes plastic flow on the retreating side, which is the middle of plastic flow, while ensuring frictional heat generation on the advanced side, which is the starting point of plastic flow, suppresses the occurrence of defects, and increases the joining speed. You can plan. The area range of the heating region 12 located between the bonding center line 10 and the RS line 11 is preferably 70% or more, more preferably 80% or more, and may be 100%.

また、リトリーティングサイドを優先的に加熱するという観点からは、加熱領域12の中心を、接合中央線10とRS線11の中間点を通る直線と、RS線11との間に位置させる。換言すれば、加熱領域12の中心を接合中央線10よりもリトリーティングサイドに位置させ、さらに加熱領域12の中心から接合中央線10までの距離を、回転ツールのピン部9における最大半径の0.5倍以上1倍以下とすることが好ましい。   Further, from the viewpoint of preferentially heating the retreating side, the center of the heating region 12 is positioned between the RS line 11 and a straight line passing through an intermediate point between the junction center line 10 and the RS line 11. In other words, the center of the heating region 12 is positioned on the retreating side with respect to the bonding center line 10, and the distance from the center of the heating region 12 to the bonding center line 10 is set to 0 of the maximum radius in the pin portion 9 of the rotary tool. It is preferable to be 5 times or more and 1 time or less.

加熱領域の厚さ方向の領域における温度T:T≧0.8×TA1
前述したように、本実施形態の摩擦撹拌接合方法で接合する鋼板3は、鋼の変態温度であるTA1の80%程度の温度では、常温時の強度の30%程度の強度となる。また、この温度より高くなると、鋼板3の強度は、さらに低下する。よって、加熱領域12の厚さ方向の領域においても、温度を0.8×TA1℃以上として鋼板3を予め軟化させることが好ましい。これにより、回転ツール1にかかる負荷がさらに低減され、接合速度をさらに高速度化できる。従って、加熱領域12の厚さ方向の領域における温度Tが下記式(3)を満足する領域における鋼板3の表面からの深さを加熱領域12の深さDとした。
Temperature T D in the thickness direction region of the heating region: T D ≧ 0.8 × T A1
As described above, the steel plate 3 joined by the friction stir welding method of the present embodiment has a strength of about 30% of the strength at normal temperature at a temperature of about 80% of TA1 , which is the transformation temperature of the steel. Moreover, when it becomes higher than this temperature, the intensity | strength of the steel plate 3 will fall further. Therefore, it is preferable to soften the steel plate 3 in advance in the thickness direction region of the heating region 12 at a temperature of 0.8 × T A1 ° C. or higher. Thereby, the load concerning the rotary tool 1 is further reduced, and the joining speed can be further increased. Accordingly, the temperature T D in the thickness direction of the region of the heating region 12 has the depth D of the following formula (3) heating region 12 a depth from the surface of the steel plate 3 in satisfying region.

≧0.8×TA1・・・(3)
A1(℃)は下記式(2)により求めることができる。
T D ≧ 0.8 × T A1 (3)
T A1 (° C.) can be obtained by the following formula (2).

A1(℃)=723−10.7[%Mn]−16.9[%Ni]+29.1[%Si]+16.9[%Cr]+290[%As]+6.38[%W]・・・(2)
上記[%M]は、被加工材である鋼板3におけるM元素の含有量(質量%)であり、含有しない場合は0とする。
T A1 (° C.) = 723-10.7 [% Mn] −16.9 [% Ni] +29.1 [% Si] +16.9 [% Cr] +290 [% As] +6.38 [% W] · (2)
Said [% M] is content (mass%) of M element in the steel plate 3 which is a workpiece, and is set to 0 when not containing.

ただし、0.8×TA1℃超では温度の上昇と共に鋼板3の強度は低下する傾向があるので、加熱領域12における鋼板3の温度が上昇し過ぎないように調節することが好ましい。具体的に、厚さ方向へ加熱領域12を確保するには加熱領域12の厚さ方向に温度勾配(厚さ方向に沿った温度のばらつき)が存在してもよいが、その場合、加熱領域12における鋼板3の厚さ方向の最も高い温度は1.5×T℃以下であることが好ましい。さらに、接合部4の温度が過度に上昇することによる回転ツール1の損傷や、加熱領域12の周辺のミクロ組織の変質を避けるために、加熱領域12における鋼板3の厚さ方向の温度を、加熱領域12を通過する回転ツール1と接触するまでにT℃未満とすることが好ましい。T(℃)は、被加工材である鋼板3の融点である。However, since the strength of the steel plate 3 tends to decrease as the temperature rises if it exceeds 0.8 × T A1 ° C, it is preferable to adjust so that the temperature of the steel plate 3 in the heating region 12 does not rise too much. Specifically, in order to secure the heating region 12 in the thickness direction, there may be a temperature gradient (temperature variation along the thickness direction) in the thickness direction of the heating region 12, but in that case, the heating region 12 12, the highest temperature in the thickness direction of the steel plate 3 is preferably 1.5 × T M ° C. or less. Furthermore, in order to avoid damage to the rotary tool 1 due to excessive increase in the temperature of the joint 4 and alteration of the microstructure around the heating region 12, the temperature in the thickness direction of the steel plate 3 in the heating region 12 is It is preferable that the temperature is lower than T M ° C. before contacting the rotary tool 1 passing through the heating region 12. T M (° C.) is the melting point of the steel sheet 3 as the workpiece.

加熱領域の深さD:鋼板の厚さtの30%以上
加熱領域12の深さDは、加熱領域12の厚さ方向の温度Tが0.8×TA1℃以上となる領域の鋼板3の表面からの最大深さで規定される。この加熱領域12の深さDは、鋼板3の厚さtの30%以上であることが好ましい。加熱領域12の深さDを鋼板3の厚さtの30%以上とすることで、塑性流動がさらに促進され、回転ツール1にかかる負荷低減および接合速度の高速度化に有利となる。加熱領域12の深さDは、鋼板3の厚さの50%以上であることがより好ましい。
The depth D of the heating zone: depth D of 30% of the thickness t or more heating region 12 of the steel sheet, the steel sheet in the region where the temperature T D in the thickness direction of the heating area 12 is 0.8 × T A1 ° C. or higher 3 is defined by the maximum depth from the surface. The depth D of the heating region 12 is preferably 30% or more of the thickness t of the steel plate 3. By setting the depth D of the heating region 12 to 30% or more of the thickness t of the steel plate 3, plastic flow is further promoted, which is advantageous for reducing the load applied to the rotary tool 1 and increasing the joining speed. The depth D of the heating region 12 is more preferably 50% or more of the thickness of the steel plate 3.

しかしながら、加熱領域12の深さDが、鋼板3の厚さtの90%を超えると、加熱が過多となり、加熱領域12の周辺のミクロ組織の変化が懸念されるので、加熱領域12の深さDは、鋼板3の厚さtの90%以下であることが好ましい。   However, if the depth D of the heating region 12 exceeds 90% of the thickness t of the steel plate 3, the heating becomes excessive, and there is a concern about changes in the microstructure around the heating region 12. The thickness D is preferably 90% or less of the thickness t of the steel plate 3.

上述した条件を実現するために、本実施形態に係る摩擦撹拌接合装置は、制御手段15を備える。制御手段15は、回転ツール1及び加熱手段5の動作を制御する。制御手段15は、後方加熱手段7や冷却手段6等の動作を制御してもよい。   In order to realize the above-described conditions, the friction stir welding apparatus according to this embodiment includes a control unit 15. The control means 15 controls the operations of the rotary tool 1 and the heating means 5. The control means 15 may control operations of the rear heating means 7 and the cooling means 6.

また、予熱処理プロセスで使用する加熱手段5は、特に限定されるものではないが、レーザ加熱装置であることが好ましい。エネルギー密度の高いレーザを熱源に用いることで、予熱処理プロセス条件の制御をより正確に行うことができ、接合継手特性を損なうことなく接合施工性の向上を図ることができる。   Further, the heating means 5 used in the preheat treatment process is not particularly limited, but is preferably a laser heating apparatus. By using a laser having a high energy density as a heat source, it is possible to more accurately control the preheat treatment process conditions, and it is possible to improve the joining workability without impairing the joint characteristics.

上記以外の接合条件については特に限定されず、例えば、予熱処理プロセスで使用する加熱手段5の移動速度は、接合速度と同程度としてよい。また、この加熱手段5にレーザ加熱装置を用いる場合、そのレーザ出力やビーム径は、接合条件に応じて適宜設定してよい。   The joining conditions other than those described above are not particularly limited. For example, the moving speed of the heating means 5 used in the preheat treatment process may be approximately the same as the joining speed. Moreover, when using a laser heating apparatus for this heating means 5, the laser output and beam diameter may be suitably set according to joining conditions.

以上、本実施形態の摩擦撹拌接合方法および装置における予熱処理プロセスについて説明したが、本実施形態の摩擦撹拌接合方法および装置では、接合方向へ移動する回転ツール1の接合方向後方に冷却手段6を設け、その冷却手段6により接合継手強度を改善させてもよい。   The preheat treatment process in the friction stir welding method and apparatus according to the present embodiment has been described above. However, in the friction stir welding method and apparatus according to the present embodiment, the cooling means 6 is disposed behind the rotating tool 1 moving in the joining direction. The joint joint strength may be improved by providing the cooling means 6.

通常、接合完了後、接合部4は自然放冷状態となるので、被加工材である鋼板3の焼入れ性が低い場合は、接合継手の強度が十分に得られない。これに対して、接合方向へ移動する回転ツール1の接合方向後方に冷却手段6を設け、冷却手段6で鋼板3の接合部4を冷却し、冷却速度を適切に制御することで、焼入れによる強度向上を図ることができる。冷却手段6としては、例えば、不活性ガスを噴出する冷却装置を用いることが好ましい。この場合の冷却速度は、例えば、800℃から500℃の範囲において30〜300℃/sであることが好ましい。不活性ガスとしては、例えば、アルゴンガス、ヘリウムガス等を用いることができる。   Usually, after joining is completed, the joint 4 is naturally cooled, so that the strength of the joint joint cannot be sufficiently obtained when the hardenability of the steel plate 3 as the workpiece is low. On the other hand, a cooling means 6 is provided behind the rotating tool 1 moving in the joining direction, and the joining portion 4 of the steel plate 3 is cooled by the cooling means 6 and the cooling rate is appropriately controlled. Strength can be improved. As the cooling means 6, for example, a cooling device that ejects an inert gas is preferably used. The cooling rate in this case is preferably 30 to 300 ° C./s in the range of 800 ° C. to 500 ° C., for example. For example, argon gas or helium gas can be used as the inert gas.

被加工材である鋼板3の焼入れ性が高い場合は、過度に硬化する可能性があり接合継手の靭性を低下させる。これに対して、回転ツール1に近接する後方部分を加熱する後方加熱手段7を回転ツール1の接合方向後方に設け、冷却速度を適切に制御しながら徐冷することで、過度な硬化を抑制できる。後方加熱手段7としては、例えば、高周波誘導加熱、レーザを熱源とした加熱装置を用いることが好ましい。この場合の徐冷速度は、例えば、800℃から500℃の範囲において10〜30℃/sであることが好ましい。   In the case where the hardenability of the steel sheet 3 which is a workpiece is high, there is a possibility that the steel sheet 3 is excessively hardened, which lowers the toughness of the joint joint. In contrast, excessive heating is suppressed by providing a rear heating means 7 for heating a rear portion close to the rotary tool 1 at the rear in the joining direction of the rotary tool 1 and gradually cooling it while appropriately controlling the cooling rate. it can. As the rear heating means 7, it is preferable to use, for example, a high-frequency induction heating or a heating device using a laser as a heat source. The slow cooling rate in this case is preferably 10 to 30 ° C./s in the range of 800 ° C. to 500 ° C., for example.

接合方向へ移動する回転ツールの接合方向後方で、かつ冷却手段6の接合方向後方に後方加熱手段7を設け、後方加熱手段7により鋼板3の接合部4を再加熱してもよい。これにより、接合部4が冷却手段6による冷却で焼入れされ、過度に硬化した場合に、後方加熱手段7で焼き戻しすることにより硬度を抑え、強度と靭性を併せ持つ継手特性が得られる。この場合の冷却速度は、例えば、800℃から500℃の範囲において30〜300℃/sであることが好ましく、再加熱温度として、例えば、550〜650℃であることが好ましい。   The rear heating means 7 may be provided behind the rotating tool moving in the joining direction and behind the cooling means 6, and the joining portion 4 of the steel plate 3 may be reheated by the rear heating means 7. Thereby, when the joining part 4 is quenched by cooling by the cooling means 6 and hardened excessively, the joint characteristics having both strength and toughness can be obtained by suppressing the hardness by tempering by the rear heating means 7. The cooling rate in this case is preferably 30 to 300 ° C./s in the range of 800 ° C. to 500 ° C., for example, and the reheating temperature is preferably 550 to 650 ° C., for example.

さらに、接合方向へ移動する回転ツール1の接合方向後方で、かつ後方加熱手段7の接合方向後方に、冷却手段6を設け、冷却手段6により鋼板3の接合部4を冷却してもよい。   Further, a cooling means 6 may be provided behind the rotating tool 1 moving in the joining direction and behind the rear heating means 7, and the joint 4 of the steel plate 3 may be cooled by the cooling means 6.

この場合には、接合直後において、後方加熱手段7で徐冷を行い、その後、冷却手段6で急冷を行うことで、組織を複合化でき、強度と延性を併せ持つ継手特性が得られる。この場合の冷却速度は、例えば、800℃から600℃の範囲(徐冷の範囲)において10〜30℃/s程度であり、その後、600℃から400℃の範囲(急冷の範囲)において30〜300℃/s程度であることが好ましい。   In this case, immediately after joining, slow cooling is performed by the rear heating means 7 and then rapid cooling is performed by the cooling means 6 so that the structure can be combined, and joint characteristics having both strength and ductility can be obtained. The cooling rate in this case is, for example, about 10 to 30 ° C./s in the range of 800 ° C. to 600 ° C. (gradual cooling range), and then 30 to 30 in the range of 600 ° C. to 400 ° C. (rapid cooling range). It is preferably about 300 ° C./s.

上記以外の接合条件については、常法に従えばよいが、回転ツール1のトルクが大きいほど鋼板3の塑性流動性は低いので、欠陥などが生じ易くなる。   About joining conditions other than the above, a conventional method may be followed. However, the greater the torque of the rotary tool 1, the lower the plastic fluidity of the steel sheet 3, so that defects and the like are likely to occur.

従って、本実施形態の摩擦撹拌接合方法および装置では、回転ツール1の回転数を100〜1000rpmの範囲とし、回転ツール1のトルクを抑え、接合速度を1000mm/min以上に高速化することを目標とする。接合速度を500mm/min超1000mm/min以下に高速化する場合には、回転ツール1のトルクを90N・m以下に抑えることが好ましい。これにより、回転ツール1が接合中に破損する、もしくは未接合部分が残る状態を回避できる。また、接合速度を500mm/min以下にする場合には、回転ツール1のトルクを75N・m未満に抑えることが好ましい。これにより、塑性流動性を確保しつつ回転ツール1の負荷を緩和できる。   Therefore, in the friction stir welding method and apparatus of this embodiment, the rotational speed of the rotary tool 1 is set in the range of 100 to 1000 rpm, the torque of the rotary tool 1 is suppressed, and the target is to increase the welding speed to 1000 mm / min or higher. And When the joining speed is increased from 500 mm / min to 1000 mm / min or less, the torque of the rotary tool 1 is preferably suppressed to 90 N · m or less. As a result, it is possible to avoid a state in which the rotary tool 1 is broken during joining or an unjoined portion remains. Further, when the joining speed is set to 500 mm / min or less, the torque of the rotary tool 1 is preferably suppressed to less than 75 N · m. Thereby, the load of the rotary tool 1 can be eased while ensuring plastic fluidity.

また、本実施形態の摩擦撹拌接合方法の対象鋼種としては、一般的な構造用鋼や炭素鋼、例えば、JIS(日本工業規格) G 3106の溶接構造用圧延鋼材、JIS G 4051の機械構造用炭素鋼などを用いることができる。引張強度が800MPa以上の高強度構造用鋼にも適用でき、接合部4において、鋼板(母材)の引張強度の85%以上の強度、さらには90%以上の強度が得られる。   Moreover, as a target steel type of the friction stir welding method of the present embodiment, general structural steel and carbon steel, for example, rolled steel for welded structure of JIS (Japanese Industrial Standards) G 3106, and for mechanical structure of JIS G 4051 Carbon steel or the like can be used. It can also be applied to high-strength structural steel having a tensile strength of 800 MPa or more, and a strength of 85% or more of the tensile strength of the steel plate (base material), and further a strength of 90% or more can be obtained at the joint 4.

(実施例1)
板厚が1.6mmであって、下記表1に示す化学組成、引張強さの鋼板を用いて、摩擦撹拌接合を実施した。継手突合せ面は、角度をつけない、いわゆるI型開先でフライス加工程度の表面状態により片面1パスで接合を行った。摩擦撹拌接合の接合条件を表2に示す。実施例1では、図4に示した断面寸法形状(肩部直径a:12mm、ピン部の最大径b:4mm、プローブ長さc:1.4mm)の回転ツールを用いた。実施例1で用いた回転ツールは、炭化タングステン(WC)を素材とし、物理蒸着(PVD)により窒化チタン(TiN)の被覆処理が表面に施された回転ツールである。接合時にはアルゴンガスにより接合部をシールドし、表面の酸化を防止した。TiNの被覆処理を表面に施したWCの回転ツールの表面と鋼板との動摩擦係数は、0.6以下であった。
Example 1
Friction stir welding was performed using a steel plate having a plate thickness of 1.6 mm and having a chemical composition and tensile strength shown in Table 1 below. The joint butt surfaces were joined in one pass on one side in a so-called I-shaped groove with no angle, and with a surface condition of the degree of milling. Table 2 shows the welding conditions of the friction stir welding. In Example 1, the rotary tool having the cross-sectional dimensions shown in FIG. 4 (shoulder diameter a: 12 mm, pin portion maximum diameter b: 4 mm, probe length c: 1.4 mm) was used. The rotary tool used in Example 1 is a rotary tool whose surface is coated with titanium nitride (TiN) by physical vapor deposition (PVD) using tungsten carbide (WC) as a raw material. At the time of bonding, the bonded portion was shielded with argon gas to prevent surface oxidation. The coefficient of dynamic friction between the surface of the rotating tool of WC having a TiN coating treatment on the surface and the steel sheet was 0.6 or less.

ツール素材表面と鋼板との動摩擦係数は、以下の測定方法で測定した。ボールオンディスク摩擦摩耗試験機を用いて、対象素材からなるディスクを回転させながら固定された直径6mmの鋼球に荷重5Nで押し付け、回転速度100mm/sで滑り距離300mで試験を行った。試験は室温、無潤滑で行った。試験に用いた鋼球は、JIS G 4805で規定されるSUJ2の化学成分を有する素材から成り、軸受け用鋼球として加工処理された鋼球である。   The dynamic friction coefficient between the tool material surface and the steel sheet was measured by the following measuring method. Using a ball-on-disk friction and wear tester, a disk made of the target material was pressed against a steel ball having a diameter of 6 mm while rotating with a load of 5 N, and the test was performed at a rotational speed of 100 mm / s and a sliding distance of 300 m. The test was performed at room temperature and without lubrication. The steel ball used for the test is a steel ball made of a material having a chemical component of SUJ2 defined by JIS G 4805 and processed as a steel ball for bearings.

Figure 0006493564
Figure 0006493564

Figure 0006493564
Figure 0006493564

また、接合に先立ち、レーザを熱源に用いた予熱による加熱領域を確認するため、表1の鋼板Iに対して、表3に示す各照射条件(レーザ移動速度、レーザ出力およびビーム径)でレーザ光を照射して、表面温度をサーモグラフィにより測定した。さらに、レーザ照射部の断面を観察し、ナイタール腐食液によるミクロ組織観察を行った。   Prior to the bonding, in order to confirm the heating region by preheating using a laser as a heat source, the steel plate I in Table 1 was subjected to laser irradiation under the irradiation conditions (laser moving speed, laser output, and beam diameter) shown in Table 3. Light was irradiated and the surface temperature was measured by thermography. Furthermore, the cross section of the laser irradiation part was observed, and the microstructure was observed with a nital etchant.

Figure 0006493564
Figure 0006493564

ここで、変態点(TA1℃)以上となった領域は最も濃く、その外側に存在する変態点(TA1℃)未満であるが母材中のマルテンサイトなどの高硬度組織が焼き戻される領域は比較的薄くエッチングされるので、変態点(TA1℃)以上となった領域と、変態点(TA1℃)未満での焼き戻し領域と、母材の領域とは、それぞれ識別可能である。さらに、鉄鋼の熱処理の知見より、変態点(TA1℃)未満での焼き戻し領域は、0.8×TA1℃以上かつTA1℃未満の領域と一致することが知られている。このようなナイタール腐食液によるミクロ組織観察より、変態点(TA1℃)以上となった領域の深さD、および0.8×TA1℃以上となった領域の深さ(加熱領域の深さD)を測定した。Here, the region having the transformation point (T A1 ° C) or higher is darkest, and is less than the transformation point (T A1 ° C) existing outside, but a high hardness structure such as martensite in the base material is tempered. Since the region is etched relatively thin, the region where the transformation point (T A1 ° C) or higher, the tempering region below the transformation point (T A1 ° C), and the base material region can be distinguished. is there. Furthermore, from the knowledge of heat treatment of steel, it is known that the tempering region below the transformation point (T A1 ° C) coincides with the region of 0.8 x T A1 ° C or more and less than T A1 ° C. Based on the microstructure observation with such a nital corrosion solution, the depth D 0 of the region where the transformation point (T A1 ° C) or higher and the depth of the region where the temperature becomes 0.8 × T A1 ° C or higher (of the heating region) Depth D) was measured.

これらの測定結果を表4に示す。   These measurement results are shown in Table 4.

Figure 0006493564
Figure 0006493564

表4に示すように、サーモグラフィによる表面温度測定結果から、照射条件Aにおいて、0.8×TA1℃以上となる領域は、直径3.5mmの円形状であった。ここで用いた回転ツールのピン部の最大直径は4.0mmであるので、照射条件Aにおける加熱領域の面積は、回転ツールのピン部の最大径部の面積以下となる。As shown in Table 4, from the surface temperature measurement result by thermography, in the irradiation condition A, the region of 0.8 × T A1 ° C or more was a circular shape having a diameter of 3.5 mm. Since the maximum diameter of the pin portion of the rotating tool used here is 4.0 mm, the area of the heating region in the irradiation condition A is equal to or less than the area of the maximum diameter portion of the pin portion of the rotating tool.

照射条件Bにおいて、0.8×TA1℃以上となる領域は、直径2.0mmの円形状であった。従って、上記と同様に、照射条件Bにおける加熱領域の面積は、回転ツールのピン部の最大径部の面積以下となる。In the irradiation condition B, the region of 0.8 × T A1 ° C. or higher was a circular shape having a diameter of 2.0 mm. Therefore, similarly to the above, the area of the heating region in the irradiation condition B is equal to or smaller than the area of the maximum diameter portion of the pin portion of the rotary tool.

照射条件Cにおいて、0.8×TA1℃以上となる領域は、直径4.5mmの円形状であった。ここで用いた回転ツールのピン部の最大直径は4.0mmであるので、照射条件Cにおける加熱領域の面積は、回転ツールのピン部の最大径部の面積を超えることとなる。In the irradiation condition C, the region of 0.8 × T A1 ° C. or higher was a circular shape with a diameter of 4.5 mm. Since the maximum diameter of the pin part of the rotary tool used here is 4.0 mm, the area of the heating region in the irradiation condition C exceeds the area of the maximum diameter part of the pin part of the rotary tool.

照射条件Dにおいて、0.8×TA1℃以上となる領域は、レーザ移動方向が長径、レーザ移動方向と直角方向が短径となる楕円形となり、長径は3.8mm、短径は3.2mmであった。ここで用いた回転ツールのピン部の最大直径は4.0mmであるので、照射条件Dにおける加熱領域の面積は、回転ツールのピン部の最大径部の面積以下となる。In the irradiation condition D, the region of 0.8 × T A1 ° C. or higher is an ellipse having a major axis in the laser moving direction and a minor axis in the direction perpendicular to the laser moving direction, the major axis is 3.8 mm, and the minor axis is 3. It was 2 mm. Since the maximum diameter of the pin portion of the rotating tool used here is 4.0 mm, the area of the heating region in the irradiation condition D is equal to or less than the area of the maximum diameter portion of the pin portion of the rotating tool.

照射条件Eにおいて、0.8×TA1℃以上となる領域は、レーザ移動方向が長径、レーザ移動方向と直角方向が短径となる楕円形となり、長径は2.2mm、短径は1.8mmであった。従って、上記と同様に、照射条件Eにおける加熱領域の面積は、回転ツールのピン部の最大径部の面積以下となる。In the irradiation condition E, the region where the temperature is 0.8 × T A1 ° C or more is an ellipse having a major axis in the laser moving direction and a minor axis in the direction perpendicular to the laser moving direction. The major axis is 2.2 mm and the minor axis is 1. It was 8 mm. Therefore, similarly to the above, the area of the heating region under the irradiation condition E is equal to or smaller than the area of the maximum diameter portion of the pin portion of the rotary tool.

照射条件Fにおいて、0.8×TA1℃以上となる領域はレーザ移動方向が長径、レーザ移動方向と直角方向が短径となる楕円形となり、長径は4.9mm、短径は4.1mmであった。ここで用いた回転ツールのピン部の最大直径は4.0mmであるので、照射条件Fにおける加熱領域の面積は、回転ツールのピン部の最大径部の面積を超えることとなる。In the irradiation condition F, the region where the temperature is 0.8 × T A1 ° C or more is an ellipse having a major axis in the laser movement direction and a minor axis in the direction perpendicular to the laser movement direction. The major axis is 4.9 mm and the minor axis is 4.1 mm. Met. Since the maximum diameter of the pin part of the rotary tool used here is 4.0 mm, the area of the heating region under the irradiation condition F exceeds the area of the maximum diameter part of the pin part of the rotary tool.

また、表4に示すように、レーザ照射部の断面観察から、照射条件Aにおいて、TA1℃以上となった領域の深さDおよび0.8×TA1℃以上となった領域の深さ(加熱領域の深さD)は、それぞれ0.28mm、0.30mmであった。被加工材である鋼板の厚さtは1.6mmであるので、0.8×TA1℃以上となった領域の深さである加熱領域の深さDは、鋼板の厚さtの約18.8%となる。Further, as shown in Table 4, the cross-section observation of the laser irradiation unit, the irradiation condition A, the depth of the region becomes T A1 ° C. or higher and the depth of the turned region D 0 and 0.8 × T A1 ° C. or higher The depth (depth D of the heating region) was 0.28 mm and 0.30 mm, respectively. Since the thickness t of the steel plate as the workpiece is 1.6 mm, the depth D of the heating region, which is the depth of the region that is 0.8 × T A1 ° C or higher, is about the thickness t of the steel plate. 18.8%.

照射条件Bにおいて、TA1℃以上となった領域の深さDおよび0.8×TA1℃以上となった領域の深さ(加熱領域の深さD)は、それぞれ0.47mm、0.50mmであった。被加工材である鋼板の厚さtは1.6mmであるので、加熱領域の深さDは、鋼板の厚さtの約31.3%となる。Under irradiation condition B, the depth D 0 of the region where T A1 ° C or higher and the depth of the region where 0.8 × T A1 ° C or higher (depth D of the heating region) are 0.47 mm and 0, respectively. .50 mm. Since the thickness t of the steel plate as the workpiece is 1.6 mm, the depth D of the heating region is about 31.3% of the thickness t of the steel plate.

照射条件Cにおいて、TA1℃以上となった領域の深さDおよび0.8×TA1℃以上となった領域の深さ(加熱領域の深さD)は、それぞれ0.09mm、0.10mmであった。被加工材である鋼板の厚さtは1.6mmであるので、加熱領域の深さDは、鋼板の厚さtの約6.3%となる。Under irradiation condition C, the depth D 0 of the region where T A1 ° C or higher and the depth of the region where 0.8 × T A1 ° C or higher (depth D of the heating region) are 0.09 mm and 0, respectively. .10 mm. Since the thickness t of the steel plate that is the workpiece is 1.6 mm, the depth D of the heating region is about 6.3% of the thickness t of the steel plate.

照射条件Dにおいて、TA1℃以上となった領域の深さDおよび0.8×TA1℃以上となった領域の深さ(加熱領域の深さD)は、それぞれ0.30mm、0.32mmであった。被加工材である鋼板の厚さtは1.6mmであるので、0.8×TA1℃以上となった領域の深さである加熱領域の深さDは、鋼板の厚さtの約20.0%となる。Under irradiation condition D, the depth D 0 of the region where T A1 ° C or higher and the depth of 0.8 × T A1 ° C or higher (depth D of the heating region) are 0.30 mm and 0, respectively. .32 mm. Since the thickness t of the steel plate as the workpiece is 1.6 mm, the depth D of the heating region, which is the depth of the region that is 0.8 × T A1 ° C or higher, is about the thickness t of the steel plate. 20.0%.

照射条件Eにおいて、TA1℃以上となった領域の深さDおよび0.8×TA1℃以上となった領域の深さ(加熱領域の深さD)は、それぞれ0.51mm、0.54mmであった。被加工材である鋼板の厚さtは1.6mmであるので、加熱領域の深さDは、鋼板の厚さtの約33.8%となる。Under irradiation condition E, the depth D 0 of the region that is T A1 ° C or higher and the depth of the region that is 0.8 × T A1 ° C or higher (depth D of the heating region) are 0.51 mm and 0, respectively. .54 mm. Since the thickness t of the steel plate as the workpiece is 1.6 mm, the depth D of the heating region is about 33.8% of the thickness t of the steel plate.

照射条件Fにおいて、TA1℃以上となった領域の深さDおよび0.8×TA1℃以上となった領域の深さ(加熱領域の深さD)は、それぞれ0.10mm、0.11mmであった。被加工材である鋼板の厚さtは1.6mmであるので、加熱領域の深さDは、鋼板の厚さtの約6.9%となる。Under irradiation condition F, the depth D 0 of the region that is T A1 ° C or higher and the depth of the region that is 0.8 × T A1 ° C or higher (depth D of the heating region) are 0.10 mm and 0, respectively. .11 mm. Since the thickness t of the steel plate as the workpiece is 1.6 mm, the depth D of the heating region is about 6.9% of the thickness t of the steel plate.

被加工材の接合前に行ったレーザ照射による予熱プロセス条件を表5に示し、接合後に行ったプロセス条件を表6に示す。ここで、接合後に行ったプロセスにおける冷却ではガス噴出による冷却を、加熱(および再加熱)では誘導加熱をそれぞれ行った。   Table 5 shows preheating process conditions by laser irradiation performed before joining the workpieces, and Table 6 shows process conditions performed after joining. Here, in the process performed after joining, cooling by gas ejection was performed, and in the heating (and reheating), induction heating was performed.

表5、表6中、予熱プロセス条件および接合後に行ったプロセス条件における「−」は、それぞれ予熱プロセスおよび冷却や加熱といった接合後のプロセスを行わなかった場合を示す。また、接合中央線から加熱領域中心までの距離における「(AS)」、「(RS)」との記載は、加熱領域の中心が、接合中央線からそれぞれアドバンシングサイド、リトリーティングサイドにあることを示す。   In Tables 5 and 6, “-” in the preheating process condition and the process condition performed after bonding indicates a case where the preheating process and the process after bonding such as cooling and heating are not performed, respectively. In addition, in the description of “(AS)” and “(RS)” in the distance from the junction center line to the center of the heating area, the center of the heating area is located on the advancing side and the retreating side from the junction center line, respectively. Indicates.

Figure 0006493564
Figure 0006493564

Figure 0006493564
Figure 0006493564

また、表7に、接合を実施した際の回転ツールのトルクの測定値と、得られた接合継手の引張強さの測定値を示す。接合継手の引張強さは、JIS Z 3121で規定する1号試験片の寸法の引張試験片を採取し、引張試験を行った結果である。回転ツールのトルクが大きいほど塑性流動性が低く、欠陥などが生じ易くなる。   Table 7 shows the measured value of the torque of the rotating tool when the joining is performed and the measured value of the tensile strength of the obtained joint. The tensile strength of the joint joint is the result of taking a tensile test piece having the size of No. 1 test piece defined in JIS Z 3121 and conducting a tensile test. The greater the torque of the rotating tool, the lower the plastic fluidity and the more likely to cause defects.

Figure 0006493564
Figure 0006493564

表7より、発明例1〜10では、接合速度を400mm/minとした場合であっても、母材となる鋼板の引張強さの90%以上の接合継手強度が得られた。発明例1〜10の回転ツールのトルクは72N・m以下であり、塑性流動性も良好であった。特に、接合後に冷却・再加熱または冷却のみを行った発明例6、7、および8では、母材の引張強さと同等の接合継手強度が得られた。接合後に加熱・冷却または加熱のみを行った発明例9、10では、母材の引張強さの93%以上の接合継手強度が得られた。   From Table 7, in Invention Examples 1 to 10, even when the joining speed was 400 mm / min, a joint strength of 90% or more of the tensile strength of the steel sheet as the base material was obtained. The torque of the rotary tools of Invention Examples 1 to 10 was 72 N · m or less, and the plastic fluidity was also good. In particular, in Invention Examples 6, 7, and 8 in which only cooling / reheating or cooling was performed after joining, joint joint strength equivalent to the tensile strength of the base material was obtained. In Invention Examples 9 and 10 in which only heating / cooling or heating was performed after joining, a joint strength of 93% or more of the tensile strength of the base material was obtained.

一方、比較例1〜6では、回転ツールのトルクが75N・m以上となり、塑性流動性に劣っていた。   On the other hand, in Comparative Examples 1-6, the torque of the rotary tool was 75 N · m or more, and the plastic fluidity was poor.

発明例11〜20では、接合速度を1000mm/minに高速度化した場合であっても、母材の引張強さの85%以上の接合継手強度が得られ、回転ツールのトルクも90N・m以下であった。特に、接合後に冷却・再加熱または冷却のみを行った発明例16、17および18では、母材の引張強さの99%以上の接合継手強度が得られた。接合後に再加熱・冷却または再加熱のみを行った発明例19、20では、母材の引張強さの95%以上の接合継手強度が得られた。   In Invention Examples 11 to 20, even when the joining speed is increased to 1000 mm / min, a joint strength of 85% or more of the tensile strength of the base material is obtained, and the torque of the rotary tool is 90 N · m. It was the following. In particular, in Invention Examples 16, 17, and 18 in which only cooling / reheating or cooling was performed after joining, a joint joint strength of 99% or more of the tensile strength of the base material was obtained. In Invention Examples 19 and 20, in which only reheating / cooling or reheating was performed after joining, a joint joint strength of 95% or more of the tensile strength of the base material was obtained.

一方、比較例7では回転ツールが接合中に破損し、接合できなかった。比較例8〜12は、未接合部分が残る状態となって接合ができず、健全な継手は得られなかった。このため、比較例7〜12では、回転ツールトルク等の測定は行っていない。
(実施例2)
板厚が1.6mmであって、上記表1に示す化学組成、引張強さの鋼板を用いて、摩擦撹拌接合を実施した。継手突合せ面は、角度をつけない、いわゆるI型開先でフライス加工程度の表面状態により片面1パスで接合を行った。摩擦撹拌接合の接合条件を上記表2に示す。実施例2では、図4に示した断面寸法形状(肩部直径a:12mm、ピン部の最大径b:4mm、プローブ長さc:1.4mm)の回転ツールを用いた。実施例2で用いた回転ツールは、炭化タングステン(WC)を素材とし、被覆処理を施していないもの、炭化タングステン(WC)を素材とし、物理蒸着(PVD)により窒化チタン(TiN)の被覆処理を表面に施したもの、炭化タングステン(WC)を素材とし、表面に窒化アルミクロム(AlCrN)の被覆処理を表面に施したもの、または、立方晶窒化ホウ素(CBN)を素材としたものである。
On the other hand, in Comparative Example 7, the rotary tool was damaged during the joining and could not be joined. In Comparative Examples 8 to 12, the unjoined portion remained and could not be joined, and a healthy joint was not obtained. For this reason, in Comparative Examples 7-12, measurement of rotating tool torque etc. is not performed.
(Example 2)
Friction stir welding was performed using a steel plate having a plate thickness of 1.6 mm and a chemical composition and tensile strength shown in Table 1 above. The joint butt surfaces were joined in one pass on one side in a so-called I-shaped groove with no angle, and with a surface condition of the degree of milling. The welding conditions for friction stir welding are shown in Table 2 above. In Example 2, the rotary tool having the cross-sectional dimensions (shoulder diameter a: 12 mm, pin portion maximum diameter b: 4 mm, probe length c: 1.4 mm) shown in FIG. 4 was used. The rotary tool used in Example 2 is made of tungsten carbide (WC) as a raw material and is not subjected to coating treatment, and tungsten carbide (WC) is used as a raw material and is coated with titanium nitride (TiN) by physical vapor deposition (PVD). The surface is made of tungsten carbide (WC), the surface is coated with aluminum nitride nitride (AlCrN), or the material is cubic boron nitride (CBN). .

接合時にはアルゴンガスにより接合部をシールドし、表面の酸化を防止した。回転ツールの表面と鋼板との動摩擦係数は、炭化タングステン(WC)を素材として被覆処理を施していないものの場合は0.7、炭化タングステン(WC)を素材として物理蒸着(PVD)により窒化チタン(TiN)の被覆処理を施したものの場合は0.5、炭化タングステン(WC)を素材として窒化アルミクロム(AlCrN)の被覆処理を施したものの場合は0.4、立方晶窒化ホウ素(CBN)を素材としたものの場合は0.3であった。   At the time of bonding, the bonded portion was shielded with argon gas to prevent surface oxidation. The coefficient of dynamic friction between the surface of the rotating tool and the steel sheet is 0.7 when tungsten carbide (WC) is not used as a raw material, and titanium nitride (PVD) is used as titanium nitride (WC) as a raw material. 0.5 for TiN) coating, 0.4 for tungsten nitride (WC) aluminum nitride (AlCrN) coating, and cubic boron nitride (CBN). In the case of the material, it was 0.3.

ツール素材表面と鋼板との動摩擦係数は、実施例1と同じ測定方法で測定した。   The dynamic friction coefficient between the tool material surface and the steel plate was measured by the same measurement method as in Example 1.

被加工材の接合前に行ったレーザ照射による予熱プロセス条件を表8に示す。   Table 8 shows preheating process conditions by laser irradiation performed before joining the workpieces.

Figure 0006493564
Figure 0006493564

表8中、炭化タングステン(WC)を素材として皮膜処理を施していない回転ツールを「WC」、炭化タングステン(WC)を素材として物理蒸着(PVD)により窒化チタン(TiN)の被覆処理を施した回転ツールを「WC+TiN」、炭化タングステン(WC)を素材として窒化アルミクロム(AlCrN)の被覆処理を施した回転ツールを「WC+AlCrN」、立方晶窒化ホウ素(CBN)を素材とした回転ツールを「CBN」と示す。予熱プロセス条件におけるレーザ照射条件は表3に示す通りであり、また、各レーザ照射条件により形成される加熱領域の表面形状、深さは表4に示す通りである。   In Table 8, “WC” is a rotating tool that is not coated with tungsten carbide (WC) as a material, and titanium nitride (TiN) is coated by physical vapor deposition (PVD) with tungsten carbide (WC) as a material. “WC + TiN” as the rotary tool, “WC + AlCrN” as the rotary tool coated with aluminum chromium nitride (AlCrN) using tungsten carbide (WC) as the raw material, and “CBN” as the rotary tool using cubic boron nitride (CBN) as the raw material. ". The laser irradiation conditions in the preheating process conditions are as shown in Table 3, and the surface shape and depth of the heating region formed by each laser irradiation condition are as shown in Table 4.

実施例2では、接合後のプロセスを行わなかった。接合中央線から加熱領域中心までの距離における「(AS)」、「(RS)」は、加熱領域の中心が、接合中央線からそれぞれアドバンシングサイド、リトリーティングサイドにあることを示す。   In Example 2, the process after joining was not performed. “(AS)” and “(RS)” in the distance from the junction center line to the center of the heating region indicate that the center of the heating region is located on the advansing side and the retreating side from the junction center line, respectively.

表9に、接合を実施した際の回転ツールのトルクの測定値と、得られた接合継手の引張強さの測定値を示す。接合継手の引張強さは、JIS Z 3121で規定する1号試験片の寸法の引張試験片を採取し、引張試験を行った結果である。回転ツールのトルクが大きいほど塑性流動性が低く、欠陥などが生じ易くなる。   Table 9 shows the measured values of the torque of the rotating tool and the measured values of the tensile strength of the obtained joints when the joining is performed. The tensile strength of the joint joint is the result of taking a tensile test piece having the size of No. 1 test piece defined in JIS Z 3121 and conducting a tensile test. The greater the torque of the rotating tool, the lower the plastic fluidity and the more likely to cause defects.

Figure 0006493564
Figure 0006493564

表9より、発明例21〜26では、接合速度を400mm/minとした場合であっても、母材となる鋼板の引張強さの90%以上の接合継手強度が得られた。発明例21〜26の回転ツールのトルクは65N・m以下であり、塑性流動性も良好であった。   From Table 9, in the invention examples 21-26, even if it was a case where a joining speed was 400 mm / min, the joint joint intensity | strength 90% or more of the tensile strength of the steel plate used as a base material was obtained. The torque of the rotary tools of Invention Examples 21 to 26 was 65 N · m or less, and the plastic fluidity was also good.

一方、比較例13、14では、回転ツールのトルクが75N・m以上となり、塑性流動性に劣っていた。   On the other hand, in Comparative Examples 13 and 14, the torque of the rotary tool was 75 N · m or more, and the plastic fluidity was poor.

表9より、発明例27〜32では、接合速度を1000mm/minに高速度化した場合であっても、母材の引張強さの85%以上の接合継手強度が得られ、回転ツールのトルクも81N・m以下であった。   From Table 9, in Invention Examples 27 to 32, even when the joining speed is increased to 1000 mm / min, a joint strength of 85% or more of the tensile strength of the base material is obtained, and the torque of the rotary tool is obtained. Was 81 N · m or less.

一方、比較例15、16では未接合部分が残る状態となって接合ができなかった。このため、比較例15、16では、回転ツールのトルク等の測定は行っていない。   On the other hand, in Comparative Examples 15 and 16, the unbonded portion remained and bonding could not be performed. For this reason, in Comparative Examples 15 and 16, measurement of torque and the like of the rotary tool is not performed.

1 回転ツール
2 回転軸
3 鋼板
4 接合部
5 加熱手段
6 冷却手段
7 後方加熱手段
8 回転ツールの肩部
9 回転ツールのピン部
10 接合中央線
11 RS線
12 加熱領域
13 冷却領域
14 再加熱領域
15 制御手段
a 回転ツールの肩部直径
b 回転ツールのピン部の最大径
c 回転ツールのプローブ長さ
X 加熱領域と回転ツールとの最小距離
D 加熱領域の深さ
t 鋼板の厚さ
α 回転ツールの傾斜角度
DESCRIPTION OF SYMBOLS 1 Rotating tool 2 Rotating shaft 3 Steel plate 4 Joining part 5 Heating means 6 Cooling means 7 Backward heating means 8 Rotating tool shoulder 9 Rotating tool pin part 10 Joining center line 11 RS line 12 Heating area 13 Cooling area 14 Reheating area 15 Control means a Diameter of the shoulder of the rotating tool b Maximum diameter of the pin of the rotating tool c Probe length of the rotating tool X Minimum distance between the heating area and the rotating tool D Depth of the heating area t Thickness of the steel sheet α Rotating tool Tilt angle

Claims (14)

肩部と、該肩部に配され、該肩部と回転軸を共有するピン部と、を含み、前記肩および前記ピン部が被加工材である鋼板よりも硬い材質からなる回転ツールを、鋼板間の未接合部に挿入して回転させながら接合方向に移動させ、前記回転ツールと前記鋼板との摩擦熱により前記鋼板を軟化させつつ、その軟化した部位を前記回転ツールで撹拌することにより塑性流動を生じさせて鋼板同士を接合する摩擦撹拌接合方法であって、
前記回転ツールの素材、もしくは前記回転ツールの表面に被覆された素材と前記鋼板との動摩擦係数は0.6以下であり、
前記回転ツールの接合方向前方に設けられた加熱手段により加熱された前記鋼板の表面の温度T(℃)が下記式(1)を満足する領域を加熱領域としたとき、前記加熱領域と前記回転ツールとの最小距離は、前記回転ツールの肩部の直径以下であり、
前記加熱領域の面積は、前記回転ツールのピン部の最大径部の面積以下であり、
前記加熱領域の面積の65%以上は、前記鋼板の表面における前記回転ツールの回転軸を通り接合方向に平行な直線である接合中央線と、該接合中央線に平行で、かつリトリーティングサイドへ前記回転ツールのピン部の最大半径と同じ距離だけ隔てた直線と、の間に位置する摩擦撹拌接合方法。
≧0.8×TA1・・・(1)
A1は、下記式(2)で示される温度である。
A1(℃)=723−10.7[%Mn]−16.9[%Ni]+29.1[%Si]+16.9[%Cr]+290[%As]+6.38[%W]・・・(2)
上記[%M]は、被加工材である鋼板におけるM元素の含有量(質量%)であり、含有しない場合は0とする。
A rotating tool comprising a shoulder portion and a pin portion arranged on the shoulder portion and sharing the rotation axis with the shoulder portion , wherein the shoulder portion and the pin portion are made of a material harder than a steel plate as a workpiece. , Inserting in the unjoined part between the steel plates and moving in the joining direction while rotating, and softening the steel plate by frictional heat between the rotating tool and the steel plate, stirring the softened part with the rotary tool A friction stir welding method for joining steel plates by causing plastic flow,
The material of the rotating tool, or the dynamic friction coefficient between the steel sheet and the material coated on the surface of the rotating tool is 0.6 or less,
When the region where the surface temperature T S (° C.) of the steel sheet heated by the heating means provided in front of the rotating tool in the joining direction satisfies the following formula (1) is defined as the heating region, the heating region and the The minimum distance to the rotating tool is not more than the diameter of the shoulder of the rotating tool,
The area of the heating region is equal to or less than the area of the maximum diameter portion of the pin portion of the rotary tool,
65% or more of the area of the heating region is a joining center line that is a straight line passing through the rotation axis of the rotating tool on the surface of the steel plate and parallel to the joining direction, parallel to the joining center line, and to the retreating side. A friction stir welding method positioned between a straight line separated by the same distance as the maximum radius of the pin portion of the rotating tool.
T S ≧ 0.8 × T A1 (1)
T A1 is a temperature represented by the following formula (2).
T A1 (° C.) = 723-10.7 [% Mn] −16.9 [% Ni] +29.1 [% Si] +16.9 [% Cr] +290 [% As] +6.38 [% W] · (2)
Said [% M] is content (mass%) of M element in the steel plate which is a workpiece, and is set to 0 when not containing.
前記加熱領域の厚さ方向の温度T(℃)が下記式(3)を満足する領域における前記鋼板の表面からの最大深さを加熱領域の深さDとしたとき、前記加熱領域の深さDは、前記鋼板の厚さの30%以上である請求項1に記載の摩擦撹拌接合方法。
≧0.8×TA1・・・(3)
When the maximum depth from the surface of the steel sheet in the region where the temperature T D (° C.) in the thickness direction of the heating region satisfies the following formula (3) is the depth D of the heating region, the depth of the heating region The friction stir welding method according to claim 1, wherein the thickness D is 30% or more of the thickness of the steel plate.
T D ≧ 0.8 × T A1 (3)
前記加熱手段は、レーザ加熱装置である請求項1または請求項2に記載の摩擦撹拌接合方法。   The friction stir welding method according to claim 1 or 2, wherein the heating means is a laser heating device. 前記回転ツールの接合方向後方には後方加熱手段が設けられており、該後方加熱手段は、前記鋼板の接合部を加熱する請求項1から請求項3のいずれか一項に記載の摩擦撹拌接合方法。   The friction stir welding according to any one of claims 1 to 3, wherein a rear heating unit is provided at a rear side of the rotating tool in a joining direction, and the rear heating unit heats a joint portion of the steel plate. Method. 前記後方加熱手段の接合方向後方には冷却手段が設けられており、該冷却手段は、前記後方加熱手段により加熱された前記接合部を冷却する請求項4に記載の摩擦撹拌接合方法。   The friction stir welding method according to claim 4, wherein a cooling means is provided behind the rear heating means in the joining direction, and the cooling means cools the joint heated by the rear heating means. 前記回転ツールの接合方向後方には冷却手段が設けられており、該冷却手段は、前記鋼板の接合部を冷却する請求項1から請求項3のいずれか一項に記載の摩擦撹拌接合方法。   The friction stir welding method according to any one of claims 1 to 3, wherein a cooling means is provided behind the rotating tool in the joining direction, and the cooling means cools the joining portion of the steel plate. 前記冷却手段の接合方向後方には後方加熱手段が設けられており、該後方加熱手段は、前記冷却手段により冷却された前記接合部を加熱する請求項6に記載の摩擦撹拌接合方法。   The friction stir welding method according to claim 6, wherein a rear heating unit is provided at a rear side of the cooling unit in the joining direction, and the rear heating unit heats the joint portion cooled by the cooling unit. 被加工材である鋼板間の未接合部を接合する摩擦撹拌接合装置であって、
肩部と、該肩部に配され、該肩部と回転軸を共有するピン部と、を含み、前記肩部および前記ピン部は、前記鋼板よりも硬い材質からなり、前記鋼板間の未接合部に挿入された状態で回転しながら接合方向に移動することで、摩擦熱により前記鋼板を軟化させつつ、その軟化した部位を撹拌することにより塑性流動を生じさせる回転ツールと、
該回転ツールの接合方向前方に設けられ、前記鋼板を加熱する加熱手段と、
下記状態1を実現するように前記回転ツール及び前記加熱手段を制御する制御手段と、を有し、
前記回転ツールの素材、もしくは前記回転ツールの表面に被覆した素材と前記鋼板との動摩擦係数は0.6以下である摩擦撹拌接合装置。
(状態1)
前記加熱手段により加熱された前記鋼板の表面の温度T(℃)が下記式(1)を満足する領域を加熱領域としたとき、前記加熱領域と前記回転ツールとの最小距離は、前記回転ツールの肩部の直径以下であり、
前記加熱領域の面積は、前記回転ツールのピン部の最大径部の面積以下であり、
前記加熱領域の面積の65%以上は、前記鋼板の表面における前記回転ツールの回転軸を通り接合方向に平行な直線である接合中央線と、該接合中央線に平行で、かつリトリーティングサイドへ前記回転ツールのピン部の最大半径と同じ距離だけ隔てた直線と、の間に位置する。
≧0.8×TA1・・・(1)
A1は、下記式(2)で示される温度である。
A1(℃)=723−10.7[%Mn]−16.9[%Ni]+29.1[%Si]+16.9[%Cr]+290[%As]+6.38[%W]・・・(2)
上記[%M]は、被加工材である鋼板におけるM元素の含有量(質量%)であり、含有しない場合は0とする。
A friction stir welding apparatus that joins unjoined portions between steel plates that are workpieces,
A shoulder portion and a pin portion arranged on the shoulder portion and sharing the rotation axis with the shoulder portion, and the shoulder portion and the pin portion are made of a material harder than the steel plate, A rotating tool that causes plastic flow by stirring the softened part while softening the steel plate by frictional heat by moving in the joining direction while rotating in a state inserted in the joint part,
A heating means provided in front of the rotating tool in the joining direction, for heating the steel plate;
Control means for controlling the rotating tool and the heating means so as to realize the following state 1;
The friction stir welding apparatus, wherein the dynamic friction coefficient between the steel plate and the material of the rotary tool or the material coated on the surface of the rotary tool is 0.6 or less.
(State 1)
When a region where the surface temperature T S (° C.) of the steel sheet heated by the heating unit satisfies the following formula (1) is a heating region, the minimum distance between the heating region and the rotating tool is the rotation Less than the diameter of the shoulder of the tool,
The area of the heating region is equal to or less than the area of the maximum diameter portion of the pin portion of the rotary tool,
65% or more of the area of the heating region is a joining center line that is a straight line passing through the rotation axis of the rotating tool on the surface of the steel plate and parallel to the joining direction, parallel to the joining center line, and to the retreating side. And a straight line separated by the same distance as the maximum radius of the pin portion of the rotating tool.
T S ≧ 0.8 × T A1 (1)
T A1 is a temperature represented by the following formula (2).
T A1 (° C.) = 723-10.7 [% Mn] −16.9 [% Ni] +29.1 [% Si] +16.9 [% Cr] +290 [% As] +6.38 [% W] · (2)
Said [% M] is content (mass%) of M element in the steel plate which is a workpiece, and is set to 0 when not containing.
前記制御手段は、以下の状態2を実現するように前記回転ツール及び前記加熱手段を制御する請求項8に記載の摩擦撹拌接合装置。
(状態2)
前記加熱領域の厚さ方向の温度T(℃)が下記式(3)を満足する領域における前記鋼板の表面からの最大深さを加熱領域の深さDとしたとき、前記加熱領域の深さDは、前記鋼板の厚さの30%以上である。
≧0.8×TA1・・・(3)
The friction stir welding apparatus according to claim 8, wherein the control means controls the rotary tool and the heating means so as to realize the following state 2.
(State 2)
When the maximum depth from the surface of the steel sheet in the region where the temperature T D (° C.) in the thickness direction of the heating region satisfies the following formula (3) is the depth D of the heating region, the depth of the heating region The thickness D is 30% or more of the thickness of the steel plate.
T D ≧ 0.8 × T A1 (3)
前記加熱手段は、レーザ加熱装置である請求項8または請求項9に記載の摩擦撹拌接合装置。   The friction stir welding apparatus according to claim 8 or 9, wherein the heating means is a laser heating apparatus. 前記鋼板の接合部を加熱する後方加熱手段をさらに有し、
該後方加熱手段は、前記回転ツールの接合方向後方に設けられる請求項8から請求項10のいずれか一項に記載の摩擦撹拌接合装置。
It further has a rear heating means for heating the joined portion of the steel sheet,
The friction stir welding apparatus according to any one of claims 8 to 10, wherein the rear heating means is provided at a rear side in the joining direction of the rotary tool.
前記接合部を冷却する冷却手段をさらに有し、
該冷却手段は、前記後方加熱手段の接合方向後方に設けられる請求項11に記載の摩擦撹拌接合装置。
A cooling means for cooling the joint;
The friction stir welding apparatus according to claim 11, wherein the cooling means is provided at a rear side in the joining direction of the rear heating means.
前記鋼板の接合部を冷却する冷却手段をさらに有し、
該冷却手段は、前記回転ツールの接合方向後方に設けられる請求項8から請求項10のいずれか一項に記載の摩擦撹拌接合装置。
A cooling means for cooling the joint of the steel plates;
The friction stir welding apparatus according to any one of claims 8 to 10, wherein the cooling means is provided behind the rotating tool in the joining direction.
前記接合部を加熱する後方加熱手段をさらに有し、
該後方加熱手段は、前記冷却手段の接合方向後方に設けられる請求項13に記載の摩擦撹拌接合装置。
A rear heating means for heating the joint;
14. The friction stir welding apparatus according to claim 13, wherein the rear heating means is provided behind the cooling means in the joining direction.
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