JP6414938B2 - 表面エネルギーを改質した非晶質を使用した溶液からの意図された核形成及び結晶成長 - Google Patents

表面エネルギーを改質した非晶質を使用した溶液からの意図された核形成及び結晶成長 Download PDF

Info

Publication number
JP6414938B2
JP6414938B2 JP2016501740A JP2016501740A JP6414938B2 JP 6414938 B2 JP6414938 B2 JP 6414938B2 JP 2016501740 A JP2016501740 A JP 2016501740A JP 2016501740 A JP2016501740 A JP 2016501740A JP 6414938 B2 JP6414938 B2 JP 6414938B2
Authority
JP
Japan
Prior art keywords
nucleation
substrate
solution
solute
amorphous
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2016501740A
Other languages
English (en)
Japanese (ja)
Other versions
JP2016517387A5 (enExample
JP2016517387A (ja
Inventor
ボンド，アンドリュー，エイチ．
シャーブ，ケビン，エム．
Original Assignee
デノブクス，エルエルシー
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by デノブクス，エルエルシー filed Critical デノブクス，エルエルシー
Publication of JP2016517387A publication Critical patent/JP2016517387A/ja
Publication of JP2016517387A5 publication Critical patent/JP2016517387A5/ja
Application granted granted Critical
Publication of JP6414938B2 publication Critical patent/JP6414938B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C07C69/84—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring of monocyclic hydroxy carboxylic acids, the hydroxy groups and the carboxyl groups of which are bound to carbon atoms of a six-membered aromatic ring
    • C07C69/86—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring of monocyclic hydroxy carboxylic acids, the hydroxy groups and the carboxyl groups of which are bound to carbon atoms of a six-membered aromatic ring with esterified hydroxyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0063—Control or regulation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10—Inorganic compounds or compositions
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/54—Organic compounds
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
    • C30B7/02—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by evaporation of the solvent
    • C30B7/06—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by evaporation of the solvent using non-aqueous solvents
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
    • C30B7/08—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by cooling of the solution

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
JP2016501740A 2013-03-15 2014-03-12 表面エネルギーを改質した非晶質を使用した溶液からの意図された核形成及び結晶成長 Active JP6414938B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201361794821P 2013-03-15 2013-03-15
US61/794,821 2013-03-15
PCT/US2014/025089 WO2014151146A1 (en) 2013-03-15 2014-03-12 Directed nucleation and crystal growth from solution using surface energy modified amorphous materials

Publications (3)

Publication Number Publication Date
JP2016517387A JP2016517387A (ja) 2016-06-16
JP2016517387A5 JP2016517387A5 (enExample) 2017-09-14
JP6414938B2 true JP6414938B2 (ja) 2018-10-31

Family

ID=51530176

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2016501740A Active JP6414938B2 (ja) 2013-03-15 2014-03-12 表面エネルギーを改質した非晶質を使用した溶液からの意図された核形成及び結晶成長

Country Status (8)

Country Link
US (1) US9193664B2 (enExample)
EP (1) EP2969093B8 (enExample)
JP (1) JP6414938B2 (enExample)
CA (1) CA2904340C (enExample)
DK (1) DK2969093T3 (enExample)
ES (1) ES2749603T3 (enExample)
PL (1) PL2969093T3 (enExample)
WO (1) WO2014151146A1 (enExample)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9583187B2 (en) 2015-03-28 2017-02-28 Intel Corporation Multistage set procedure for phase change memory
US9777025B2 (en) * 2015-03-30 2017-10-03 L'Air Liquide, Société pour l'Etude et l'Exploitation des Procédés Georges Claude Si-containing film forming precursors and methods of using the same
CN113373499B (zh) * 2021-05-21 2023-08-15 湖北理工学院 一种观赏性花饰化学艺术晶体的制备方法
CN118248248B (zh) * 2024-05-28 2024-08-23 烟台国工智能科技有限公司 一种无机晶体条件生成分析方法及装置

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3146985B2 (ja) * 1996-06-26 2001-03-19 住友金属工業株式会社 結晶成長方法および結晶成長用固体素子
JP3297702B2 (ja) * 1996-09-03 2002-07-02 住友金属工業株式会社 結晶成長用装置
JP3007972B1 (ja) * 1999-03-05 2000-02-14 大阪大学長 有機光学単結晶の形成方法及び有機光学単結晶
GB2362754A (en) 2000-05-25 2001-11-28 Nanogate Ltd A method of growing single crystals
WO2002101127A1 (en) 2001-06-08 2002-12-19 Syrrx, Inc. In situ crystal growth and analysis
US7122083B2 (en) 2002-04-02 2006-10-17 E. I. Du Pont De Nemours And Company Apparatus and process used in growing crystals
JP2006036565A (ja) * 2004-07-23 2006-02-09 Ricoh Co Ltd 有機単結晶付基板の製造方法、有機単結晶付基板及び有機単結晶付基板の製造装置
US7763471B2 (en) * 2006-04-18 2010-07-27 Advanced Liquid Logic, Inc. Method of electrowetting droplet operations for protein crystallization
US9138659B2 (en) 2010-08-23 2015-09-22 Massachusetts Institute Of Technology Compositions, methods, and systems relating to controlled crystallization and/or nucleation of molecular species
US9822467B2 (en) 2011-11-15 2017-11-21 Massachusetts Institute Of Technology Methods and systems relating to the selection of substrates comprising crystalline templates for the controlled crystallization of molecular species

Also Published As

Publication number Publication date
US9193664B2 (en) 2015-11-24
EP2969093B8 (en) 2019-11-27
US20140275611A1 (en) 2014-09-18
EP2969093B1 (en) 2019-07-24
WO2014151146A1 (en) 2014-09-25
JP2016517387A (ja) 2016-06-16
ES2749603T3 (es) 2020-03-23
DK2969093T3 (da) 2019-10-28
EP2969093A1 (en) 2016-01-20
CA2904340A1 (en) 2014-09-25
EP2969093A4 (en) 2016-12-21
PL2969093T3 (pl) 2020-03-31
CA2904340C (en) 2019-09-17

Similar Documents

Publication Publication Date Title
Lovette et al. Crystal shape engineering
Krauss et al. An overview of biological macromolecule crystallization
Diao et al. Gel-induced selective crystallization of polymorphs
Llinàs et al. Polymorph control: past, present and future
Wiencek New strategies for protein crystal growth
JP6414938B2 (ja) 表面エネルギーを改質した非晶質を使用した溶液からの意図された核形成及び結晶成長
Li et al. Hydrogels coupled with self-assembled monolayers: an in vitro matrix to study calcite biomineralization
Yonath et al. Parameters for crystal growth of ribosomal subunits
Anderson et al. Understanding crystal nucleation mechanisms: where do we stand? General discussion
Verma et al. Dependence of heterogeneous nucleation on hydrogen bonding lifetime and complementarity
Fellah et al. Crystallization and Polymorphism under Nanoconfinement
Dela Cruz et al. Influence of volume on the nucleation of model organic molecular crystals through an induction time approach
JP2010220618A (ja) タンパク質の結晶化法
Nicoud et al. The influence of impurities and additives on crystallization
Liang et al. Insights into polymorphic transformation of L-glutamic acid: a combined experimental and simulation study
CN104093698A (zh) 金属辅助和微波加速的蒸发结晶
Langdon et al. The osteopontin-controlled switching of calcium oxalate monohydrate morphologies in artificial urine provides insights into the formation of papillary kidney stones
Arribas Bueno et al. Influence of process parameters on the heterogeneous nucleation of active pharmaceutical ingredients onto excipients
Budayova-Spano et al. A methodology and an instrument for the temperature-controlled optimization of crystal growth
Lee et al. The origin of life and the crystallization of aspartic acid in water
Boerrigter et al. In situ observation of epitaxial polymorphic nucleation of the model steroid methyl analogue 17 norethindrone
Pantaraks et al. Effect of growth rate history on current crystal growth. 2. Crystal growth of sucrose, Al (SO4) 2· 12H2O, KH2PO4, and K2SO4
US20130199439A1 (en) Device and method for crystallizing inorganic or organic substances
Gorelik et al. Detecting crystalline nonequilibrium phases on the nanometer scale
Xu et al. Primary and Secondary Nucleation Threshold of Succinic Acid: From the Perspective of Dimensionless Solid–Liquid Interfacial Tension

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20151110

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20170307

A871 Explanation of circumstances concerning accelerated examination

Free format text: JAPANESE INTERMEDIATE CODE: A871

Effective date: 20170307

A975 Report on accelerated examination

Free format text: JAPANESE INTERMEDIATE CODE: A971005

Effective date: 20170329

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20170424

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20170724

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20170724

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20170904

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20171130

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20180122

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20180521

A911 Transfer to examiner for re-examination before appeal (zenchi)

Free format text: JAPANESE INTERMEDIATE CODE: A911

Effective date: 20180601

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20180903

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20180928

R150 Certificate of patent or registration of utility model

Ref document number: 6414938

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250