JP6354441B2 - Laminated glass manufacturing method - Google Patents

Laminated glass manufacturing method Download PDF

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JP6354441B2
JP6354441B2 JP2014163687A JP2014163687A JP6354441B2 JP 6354441 B2 JP6354441 B2 JP 6354441B2 JP 2014163687 A JP2014163687 A JP 2014163687A JP 2014163687 A JP2014163687 A JP 2014163687A JP 6354441 B2 JP6354441 B2 JP 6354441B2
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laminate
sealing member
glass
plate
laminated
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JP2015171983A (en
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佐藤 雅彦
雅彦 佐藤
伸一 金子
伸一 金子
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Nippon Electric Glass Co Ltd
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本発明は、合わせガラスの製造方法の技術に関する。   The present invention relates to a technique of a method for manufacturing a laminated glass.

従来から、耐貫通性および耐衝撃性などに優れたガラスとして、合わせガラスが知られている。
合わせガラスは、一般的に、積層工程、仮圧着工程、および本圧着工程などからなるACV法(オートクレーブ法)によって製造される。
具体的には、樹脂製中間膜を介在させつつ少なくとも二枚の板ガラスを積層して製造ラインに投入し(積層工程)、投入した板ガラスを加熱して樹脂製中間膜を軟化させて、板ガラスを仮圧着し(仮圧着工程)、仮圧着した板ガラスをオートクレーブによって加熱・加圧処理することで(本圧着工程)、合わせガラスは製造される。
Conventionally, a laminated glass is known as a glass excellent in penetration resistance and impact resistance.
Laminated glass is generally manufactured by an ACV method (autoclave method) including a lamination step, a temporary pressure bonding step, a main pressure bonding step, and the like.
Specifically, at least two plate glasses are laminated while interposing a resin intermediate film, and are put into a production line (lamination process). The supplied plate glass is heated to soften the resin intermediate film and Laminated glass is manufactured by pre-pressing (temporary press-bonding step) and heating / pressurizing the pre-press-bonded plate glass with an autoclave (main press-bonding step).

ところで、前述した本圧着工程においては、例えば、板ガラスと樹脂製中間膜との間に気泡などが残って欠陥商品となるのを防止したり、板ガラスおよび樹脂製中間膜の密着性を高めたりするため、オートクレーブの炉内を加圧するのと同時に、当該オートクレーブの炉内に投入された板ガラスの積層界面を真空引きすることとしている。
ここで、特許文献1には、板ガラスの積層界面を真空引きする際の技術として、合わせガラス製造用の空気吸引除去装置に関する技術が開示されている。
具体的には、特許文献1においては、少なくとも二枚の板ガラスの間に熱可塑性の樹脂製中間膜を挟んだ積層体を製造する際に、該積層体の周縁部に長手方向に切開し周方向に開口する耐熱樹脂チューブの開口部を挿入し、該チューブと前記板ガラスとの当接部を粘着テープで封着して減圧室を設けたことを特徴とする合わせガラス製造用の空気吸引除去装置に関する技術が開示されている。
By the way, in the above-mentioned main press-bonding step, for example, bubbles are prevented from remaining between the plate glass and the resinous intermediate film, and it becomes a defective product, or the adhesion between the plateglass and the resinous intermediate film is increased. Therefore, at the same time as pressurizing the inside of the autoclave furnace, the laminated interface of the plate glass put into the autoclave furnace is evacuated.
Here, Patent Document 1 discloses a technique related to an air suction removal apparatus for producing laminated glass as a technique for evacuating a laminated interface of plate glass.
Specifically, in Patent Document 1, when manufacturing a laminated body in which a thermoplastic resin intermediate film is sandwiched between at least two sheet glasses, a peripheral portion of the laminated body is cut in the longitudinal direction and the periphery is cut. Air suction removal for laminated glass production, characterized in that an opening of a heat-resistant resin tube that opens in a direction is inserted, and a contact portion between the tube and the plate glass is sealed with an adhesive tape to provide a decompression chamber Techniques relating to the apparatus are disclosed.

実公平4−35400号公報No. 4-35400

特許文献1における、合わせガラス製造用の空気吸引除去装置によれば、耐熱樹脂チューブを減圧室として用いることにより、合わせガラスの形状に影響されることなく、合わせガラスの周縁部を完全に密閉することができ、簡易な装置によって、板ガラスの間隙を真空引きすることが可能となる。
しかしながら、板ガラスの周縁部に耐熱樹脂チューブの開口部を挿入する際、耐熱樹脂チューブの挿入動作や真空引き等によって、一対の板ガラスの平面方向の位置ずれが起こりやすく、板ガラスの積層姿勢を保持するための治具などが別途必要となり、耐熱樹脂チューブのみによって板ガラスの積層姿勢を保持しつつ、板ガラスの周縁部に耐熱樹脂チューブの開口部を挿入することは困難であった。
According to the air suction and removal apparatus for producing laminated glass in Patent Document 1, by using the heat-resistant resin tube as the decompression chamber, the peripheral portion of the laminated glass is completely sealed without being affected by the shape of the laminated glass. It is possible to evacuate the gap between the glass sheets with a simple device.
However, when the opening of the heat-resistant resin tube is inserted into the peripheral edge of the plate glass, the positional displacement in the plane direction of the pair of plate glasses is likely to occur due to the insertion operation of the heat-resistant resin tube, evacuation, etc., and the plate glass stacking posture is maintained. Therefore, it is difficult to insert the opening of the heat-resistant resin tube into the peripheral portion of the plate glass while maintaining the laminated posture of the plate glass only by the heat-resistant resin tube.

本発明は、以上に示した現状の問題点を鑑みてなされたものであり、少なくとも二枚の板ガラスの間に樹脂製中間膜を介在させて積層させた積層体に対して、オートクレーブによる加熱・加圧処理を行うと同時に、積層体の周縁部に対して密封部材を嵌装して真空引き処理を行うことにより、板ガラスを互いに圧着させて合わせガラスを製造する、合わせガラスの製造方法であって、積層体に対する密封部材の嵌装作業を、板ガラスの積層姿勢を保持しつつ容易に行うことができ、積層体の真空引き作業の効率化を図ることができる合わせガラスの製造方法を提供することを課題とする。   The present invention has been made in view of the above-described problems of the present situation, and a laminated body obtained by laminating a resin intermediate film between at least two sheet glasses is heated by an autoclave. At the same time as the pressure treatment, a sealing member is fitted to the peripheral edge of the laminated body, and a vacuum drawing process is performed, whereby the glass sheets are pressed together to produce a laminated glass. Thus, a method for manufacturing a laminated glass that can easily perform the fitting operation of the sealing member to the laminated body while maintaining the laminating posture of the plate glass and can improve the efficiency of the vacuuming operation of the laminated body is provided. This is the issue.

本発明の解決しようとする課題は以上の如くであり、次にこの課題を解決するための手段を説明する。   The problem to be solved by the present invention is as described above. Next, means for solving the problem will be described.

即ち、本発明の請求項1に係る合わせガラスの製造方法は、少なくとも二枚の板ガラスの間に樹脂製中間膜を介在させて積層させた積層体に対して、オートクレーブによる加熱・加圧処理を行うと同時に、前記積層体の周縁部に対して密封部材を嵌装して真空引き処理を行うことにより、前記板ガラスを互いに圧着させて合わせガラスを製造する、合わせガラスの製造方法であって、前記密封部材は、前記積層体の周縁部に対して嵌装された状態において、前記積層体の積層界面と連通する減圧通路と、前記積層体の端面と当接する当接部と、前記積層体を厚み方向に挟持する挟持部と、を備え、前記真空引き処理は、前記密封部材を前記積層体の周縁部に対して嵌装することにより、前記当接部を前記積層体の端面に当接させ、前記挟持部により前記積層体を厚み方向に挟持した状態で、前記減圧通路を通じて行われるとともに、前記密封部材は、前記積層体の最外層における前記板ガラスの板面に密着するシール部をさらに備え、前記密封部材を前記積層体の周縁部に対して嵌装することにより、前記シール部を前記積層体の最外層における前記板ガラスの板面に密着させ、前記挟持部と、前記シール部と、前記積層体の最外層における前記板ガラスの板面とによって囲まれた空間部に対しても、前記真空引き処理を行うことを特徴とする。 That is, in the method for producing laminated glass according to claim 1 of the present invention, a heating / pressurizing treatment by an autoclave is performed on a laminated body in which a resin intermediate film is interposed between at least two plate glasses. At the same time, a laminated glass is manufactured by fitting a sealing member to the peripheral portion of the laminate and performing a vacuuming process to press the plate glass together to produce a laminated glass, The sealing member includes a pressure reducing passage communicating with a stacking interface of the stacked body, a contact portion contacting with an end surface of the stacked body, and the stacked body in a state where the sealing member is fitted to a peripheral edge of the stacked body. A holding portion that holds the sealing member in a thickness direction, and the vacuuming process is performed by fitting the sealing member to a peripheral portion of the laminate, so that the contact portion is brought into contact with an end surface of the laminate. The clamping part In a state where more sandwiches the laminate in a thickness direction, with is performed through the vacuum passage, said sealing member further comprises a seal portion in close contact with the plate surface of the plate glass in the outermost layer of the laminate, the sealing member Is attached to the peripheral edge of the laminate, thereby bringing the seal portion into close contact with the plate surface of the plate glass in the outermost layer of the laminate, and the sandwiching portion, the seal portion, and the laminate The vacuuming process is also performed on a space portion surrounded by the plate surface of the plate glass in the outermost layer .

また、本発明の請求項に係る合わせガラスの製造方法は、前記減圧通路が、断面視半円形状に形成されることを特徴とする。 Moreover, the manufacturing method of the laminated glass which concerns on Claim 2 of this invention is characterized by the said pressure-reduction passage being formed in a cross-sectional view semicircle shape.

また、本発明の請求項に係る合わせガラスの製造方法は、前記積層体が、二枚の板ガラス間に樹脂製中間膜を介在させた積層体であり、前記減圧通路の半径寸法は、前記一対の板ガラスの間隙寸法の、1.5倍以上且つ3倍以下に設定されることを特徴とする。 Moreover, in the method for producing a laminated glass according to claim 3 of the present invention, the laminated body is a laminated body in which a resin intermediate film is interposed between two sheet glasses, and the radial dimension of the decompression passage is It is characterized by being set to 1.5 times or more and 3 times or less the gap dimension of the pair of plate glasses.

また、本発明の請求項に係る合わせガラスの製造方法は、前記空間部に対する真空引き処理は、前記減圧通路とは独立した経路を用いて行うことを特徴とする。 Moreover, the manufacturing method of the laminated glass which concerns on Claim 4 of this invention is characterized by performing the vacuuming process with respect to the said space part using the path | route independent of the said pressure reduction channel | path.

また、本発明の請求項に係る合わせガラスの製造方法は、前記樹脂製中間膜が、フッ素樹脂を含むことを特徴とする。 Moreover, the manufacturing method of the laminated glass which concerns on Claim 5 of this invention is characterized by the said resin-made intermediate film containing a fluororesin.

また、本発明の請求項に係る合わせガラスの製造方法は、前記真空引き処理が、前記加熱・加圧処理の終了後、前記樹脂製中間膜の温度がガラス転移点以下となるまで継続して行われることを特徴とする。 Further, in the method for producing a laminated glass according to claim 6 of the present invention, the evacuation treatment is continued until the temperature of the resinous intermediate film becomes equal to or lower than the glass transition point after the heating / pressurizing treatment. It is characterized by being performed.

本発明の効果として、以下に示すような効果を奏する。   As effects of the present invention, the following effects can be obtained.

本発明の請求項1に係る合わせガラスの製造方法によれば、積層体の周縁部に沿って密封部材が嵌装されることにより、積層体の端面は密封部材と当接し、且つ積層体の周縁部は密封部材によって挟持される。そのため、各板ガラスの平面方向(厚み方向との直交方向)および厚み方向の位置ずれは、密封部材自身によって規制される。
よって、板ガラスの積層姿勢を保持するための治具などを別途設ける必要がなく、密封部材のみによって板ガラスの積層姿勢を保持しつつ、積層体の周縁部に対して容易に密封部材を嵌装させることができる。
従って、積層体に対する密封部材の嵌装作業を、板ガラスの積層姿勢を保持しつつ容易に行うことができ、積層体の真空引き作業の効率化を図ることができる。
また、本発明の合わせガラスの製造方法によれば、積層体の周縁部に沿って密封部材が嵌装されることにより、積層体の最外層における板ガラスの板面にシール部が密着されるため、積層体の周縁部を含む密封部材の内周部が、密閉部材自身によって密封される。
よって、例えば、粘着テープなどを用いて、各板ガラスと密接部材との当接部を封着する必要もなく、積層体の周縁部を容易に密閉することができる。また、粘着テープを用いる場合よりも、気密信頼性を向上させることができる。
従って、積層体に対する密封部材の密封作業を容易に行うことができ、積層体の真空引き作業の密封信頼性の向上を図ることができる。
さらに、本発明の合わせガラスの製造方法によれば、減圧通路の気密性を高めることが可能となり、例えば、樹脂製中間膜の収縮に伴って発生する吸い込み泡を、極力防止することができる。
According to the method for manufacturing a laminated glass according to claim 1 of the present invention, the sealing member is fitted along the peripheral edge of the laminated body, so that the end surface of the laminated body abuts on the sealing member, and the laminated body The peripheral edge is sandwiched between sealing members. Therefore, the positional deviation of each plate glass in the plane direction (direction orthogonal to the thickness direction) and the thickness direction is regulated by the sealing member itself.
Therefore, it is not necessary to separately provide a jig or the like for maintaining the sheet glass stacking posture, and the sealing member can be easily fitted to the peripheral edge of the laminate while maintaining the sheet glass stacking posture only by the sealing member. be able to.
Therefore, it is possible to easily perform the fitting operation of the sealing member to the laminated body while maintaining the laminated posture of the plate glass, and it is possible to improve the efficiency of the vacuuming operation of the laminated body.
Moreover, according to the manufacturing method of the laminated glass of this invention, since a sealing member is fitted along the peripheral part of a laminated body, a sealing part adheres to the plate | board surface of the plate glass in the outermost layer of a laminated body. The inner peripheral part of the sealing member including the peripheral part of the laminate is sealed by the sealing member itself.
Therefore, for example, it is not necessary to seal the contact portion between each plate glass and the close contact member using an adhesive tape or the like, and the peripheral portion of the laminate can be easily sealed. Moreover, airtight reliability can be improved compared with the case where an adhesive tape is used.
Therefore, the sealing operation of the sealing member with respect to the laminate can be easily performed, and the sealing reliability of the vacuuming operation of the laminate can be improved.
Furthermore, according to the method for producing laminated glass of the present invention, it is possible to improve the airtightness of the decompression passage, and for example, it is possible to prevent suction bubbles generated as the resin intermediate film contracts as much as possible.

また、本発明の請求項に係る合わせガラスの製造方法によれば、複雑な断面形状ではなく、比較的容易な断面形状であるため、減圧通路の加工は容易である。 Moreover, according to the method for manufacturing laminated glass according to claim 2 of the present invention, since the cross-sectional shape is relatively easy, not the complicated cross-sectional shape, the processing of the decompression passage is easy.

また、本発明の請求項に係る合わせガラスの製造方法によれば、積層体の真空引きを行う際に、樹脂製中間膜が積層体の端面から突出し過ぎないようにすることが可能となり、合わせガラスの厚みを均一にでき、合わせガラスの品質向上を図ることができる。 In addition, according to the method for producing a laminated glass according to claim 3 of the present invention, it is possible to prevent the resinous intermediate film from protruding too much from the end face of the laminated body when evacuating the laminated body. The thickness of the laminated glass can be made uniform, and the quality of the laminated glass can be improved.

また、本発明の請求項に係る合わせガラスの製造方法によれば、空間部を確実に真空引きすることが可能となり、樹脂製中間膜の収縮に伴って発生する吸い込み泡を、確実に防止することができる。
また、本発明の請求項4に係る合わせガラスの製造方法によれば、例えば、板ガラスの端面より突出された樹脂製中間膜によって、減圧通路内が封鎖されたとしても、前記空間部を真空引きすることが可能となり、積層体の最外層における板ガラスの板面に対して、挟持部およびシール部を、依然として密着させておくことができる。
Moreover, according to the method for manufacturing laminated glass according to claim 4 of the present invention, it is possible to surely evacuate the space, and it is possible to reliably prevent the suction bubbles generated due to the shrinkage of the resin intermediate film. can do.
Further, according to the method for manufacturing a laminated glass according to claim 4 of the present invention, for example, even if the inside of the decompression passage is sealed by the resin intermediate film protruding from the end face of the plate glass, the space portion is evacuated. Thus, the sandwiching portion and the seal portion can be kept in close contact with the plate surface of the plate glass in the outermost layer of the laminate.

また、本発明の請求項に係る合わせガラスの製造方法によれば、フッ素樹脂の特性を生かした、耐熱性や耐燃性などに優れた合わせガラスを製造することができる。 Moreover, according to the manufacturing method of the laminated glass which concerns on Claim 5 of this invention, the laminated glass excellent in heat resistance, flame resistance, etc. which utilized the characteristic of the fluororesin can be manufactured.

また、本発明の請求項に係る合わせガラスの製造方法によれば、例えば、フッ素樹脂からなる樹脂製中間膜のような、冷却により収縮する現象を未然に防ぐことが可能となるため、合わせガラスの品質向上を図ることができる。 Further, according to the method for manufacturing laminated glass according to claim 6 of the present invention, for example, it is possible to prevent a phenomenon of shrinkage due to cooling, such as a resin intermediate film made of a fluororesin. The quality of the glass can be improved.

本発明に係る合わせガラスの製造方法を具現化する、密封部材の全体的な構成を示した一部断面正面図。The partial cross section front view which showed the whole structure of the sealing member which embodies the manufacturing method of the laminated glass which concerns on this invention. 密封部材の断面形状を示した図であって、図1中の矢印Aの方向から見た拡大断面図。It is the figure which showed the cross-sectional shape of the sealing member, Comprising: The expanded sectional view seen from the direction of the arrow A in FIG. 密封部材の内側に形成される減圧通路を示した図であって、図2中の領域Bによって示された箇所の拡大断面図。It is the figure which showed the pressure-reduction passage formed inside a sealing member, Comprising: The expanded sectional view of the location shown by the area | region B in FIG. フッ素樹脂からなる樹脂製中間膜が介在される一対の板ガラスに対して、オートクレーブによる高温高圧処理を行う際の、一対の板ガラスの状態を示した図であって、(a)はオートクレーブによる高温高圧処理を行う直前の、一対の板ガラスの端部を示した拡大断面図、(b)はオートクレーブによる高温高圧処理を行った直後の、一対の板ガラスの端部を示した拡大断面図。It is the figure which showed the state of a pair of plate glass at the time of performing the high temperature / high pressure process by an autoclave with respect to a pair of plate glass in which the resin-made intermediate film which consists of a fluororesin is interposed, (a) is the high temperature / high pressure by an autoclave The expanded sectional view which showed the edge part of a pair of plate glass just before performing a process, (b) is the expanded sectional view which showed the edge part of a pair of plate glass immediately after performing the high temperature / high pressure process by an autoclave. 別実施形態における密封部材の内側に形成される減圧通路を示した図であって、(a)は幅広の断面形状からなる減圧通路の近傍を示した拡大断面図、(b)は互いに平行に形成された複数の減圧通路の近傍を示した拡大断面図。It is the figure which showed the decompression path formed inside the sealing member in another embodiment, Comprising: (a) is an expanded sectional view which showed the vicinity of the decompression path which consists of a wide cross-sectional shape, (b) is mutually parallel. The expanded sectional view which showed the vicinity of the formed several pressure reduction channel | path. 第五実施形態における密封部材の角部の形状を示した一部断面拡大正面図。The partial cross section enlarged front view which showed the shape of the corner | angular part of the sealing member in 5th embodiment. 第五実施形態における密封部材の断面形状を示した図であって、図6中の矢印Cの方向から見た拡大断面図。FIG. 9 is a diagram showing a cross-sectional shape of a sealing member in a fifth embodiment, and is an enlarged cross-sectional view seen from the direction of arrow C in FIG.

次に、発明の実施の形態を説明する。   Next, embodiments of the invention will be described.

[合わせガラスの製造方法]
先ず、本実施形態によって具現化される合わせガラスの製造方法について、図1および図2を用いて説明する。
なお、以下の説明に関しては便宜上、図1および図2の上下方向を密封部材1の上下方向と規定して記述する。
[Production method of laminated glass]
First, the manufacturing method of the laminated glass embodied by this embodiment is demonstrated using FIG. 1 and FIG.
In the following description, for convenience, the vertical direction in FIGS. 1 and 2 is described as the vertical direction of the sealing member 1.

本実施形態における合わせガラスの製造方法は、図2に示すように、例えば、密封部材1を用いて、合わせガラス50を製造するための方法である。
合わせガラス50は、樹脂製中間膜51と、樹脂製中間膜51を介在させて積層される一対の板ガラス52・52とを備える積層体50Aからなる。
この合わせガラス50は、積層工程、仮圧着工程、および本圧着工程などを有するオートクレーブ法によって製造されるが、本実施形態における合わせガラスの製造方法は、本圧着工程において、オートクレーブ(図示せず)の炉内を加熱・加圧処理して一対の板ガラス52・52を互いに圧着させるのと同時に、炉内に投入された一対の、仮圧着工程後の板ガラス52・52の積層界面53・53に対して真空引きして製造する方法である。
The method for manufacturing a laminated glass in the present embodiment is a method for manufacturing a laminated glass 50 using, for example, the sealing member 1 as shown in FIG.
The laminated glass 50 includes a laminated body 50A including a resin intermediate film 51 and a pair of plate glasses 52 and 52 laminated with the resin intermediate film 51 interposed therebetween.
The laminated glass 50 is manufactured by an autoclave method including a lamination process, a temporary pressure bonding process, a main pressure bonding process, and the like. However, the laminated glass manufacturing method in the present embodiment is an autoclave (not shown) in the main pressure bonding process. At the same time, the pair of plate glasses 52 and 52 are pressure-bonded to each other by heating and pressurizing the inside of the furnace, and at the same time, the laminated interfaces 53 and 53 of the pair of plate glasses 52 and 52 after the temporary press-bonding process. On the other hand, it is a method of manufacturing by vacuuming.

ここで、本実施形態においては、密封部材1を用いて一対の板ガラス52・52の積層界面53・53を真空引きすることとしている。
密封部材1は、詳細は後述するが、内周側が開口した断面視略「コ」字状の枠体形状に形成される。そして、開口部を介して密封部材1が一対の板ガラス52・52の周縁部に沿って嵌装された状態において、一対の板ガラス52・52と樹脂製中間膜51との境界部(積層体50Aの積層界面53)の周縁部は、密封部材1の減圧通路11bと連通される。
Here, in the present embodiment, the sealing interface 1 is used to evacuate the laminated interfaces 53 and 53 of the pair of plate glasses 52 and 52.
As will be described in detail later, the sealing member 1 is formed in a frame shape having a substantially “U” shape in cross section with an inner peripheral side opened. Then, in a state where the sealing member 1 is fitted along the peripheral edge portions of the pair of glass plates 52 and 52 through the openings, the boundary portion between the pair of glass plates 52 and 52 and the resin intermediate film 51 (laminated body 50A). The peripheral edge of the laminated interface 53) communicates with the decompression passage 11b of the sealing member 1.

そして、密封部材1が嵌装された積層体50Aは、本圧着工程において、オートクレーブの炉内へと投入される。
その後、図1に示すように、密封部材1の減圧通路11bは、配管部材21を介して真空ポンプ22などと連結される。
これにより、一対の板ガラス52・52と樹脂製中間膜51との積層界面53・53は、減圧通路11bおよび配管部材21を介して、真空ポンプ22と連結される。
And 50 A of laminated bodies with which the sealing member 1 was mounted are thrown in in the furnace of an autoclave in this crimping | compression-bonding process.
Thereafter, as shown in FIG. 1, the decompression passage 11 b of the sealing member 1 is connected to the vacuum pump 22 or the like via the piping member 21.
Thereby, the lamination | stacking interface 53 * 53 of a pair of plate glass 52 * 52 and the resin-made intermediate film 51 is connected with the vacuum pump 22 via the pressure-reduction channel | path 11b and the piping member 21. FIG.

その後、オートクレーブの炉内において、加熱・加圧処理が行われるのと同時に、真空ポンプ22によって、一対の板ガラス52・52と樹脂製中間膜51との積層界面53・53に対する真空引きが行われ、これらの板ガラス52・52が本圧着される。   Thereafter, in the autoclave furnace, heating and pressurizing processes are performed, and at the same time, the vacuum pump 22 evacuates the laminated interfaces 53 and 53 between the pair of plate glasses 52 and 52 and the resin intermediate film 51. These plate glasses 52 and 52 are finally pressure-bonded.

オートクレーブの炉内温度が所定の処理温度に到達した後、所定時間の経過を待って、加熱・加圧が停止される。
その後、炉内温度が所定の温度以下にまで低下したのを確認し、オートクレーブの炉内より積層体50Aが取出され、真空ポンプ22による真空引きが停止される。
こうして、合わせガラスの製造工程は終了し、完成した合わせガラス50が得られる。
After the autoclave furnace temperature reaches a predetermined treatment temperature, the heating and pressurization are stopped after a predetermined time has elapsed.
Thereafter, it is confirmed that the temperature in the furnace has decreased to a predetermined temperature or less, and the laminated body 50A is taken out from the inside of the furnace of the autoclave, and evacuation by the vacuum pump 22 is stopped.
In this way, the laminated glass manufacturing process is completed, and a finished laminated glass 50 is obtained.

[密封部材1]
次に、密封部材1の構成について、図1乃至図3を用いて詳述する。
なお、以下の説明に関しては便宜上、図3の上下方向を密封部材1の上下方向と規定して記述する。
[Sealing member 1]
Next, the configuration of the sealing member 1 will be described in detail with reference to FIGS. 1 to 3.
In the following description, for convenience, the vertical direction in FIG. 3 is described as the vertical direction of the sealing member 1.

密封部材1は、図2に示すように、樹脂製中間膜51が介在する、一対の板ガラス52・52の周縁部を密封するための部材である。   As shown in FIG. 2, the sealing member 1 is a member for sealing the peripheral portions of a pair of plate glasses 52 and 52 in which a resin intermediate film 51 is interposed.

密封部材1は、例えば、フッ素ゴム、シリコンゴム、またはアクリルゴムなどの、耐熱性を有する弾性部材により形成される。
また、密封部材1は、一対の板ガラス52・52の周縁部に沿った枠体形状に形成され、例えば、図1に示すように、本実施形態においては、矩形状の枠体形状に形成される。
The sealing member 1 is formed of an elastic member having heat resistance such as fluorine rubber, silicon rubber, or acrylic rubber.
Further, the sealing member 1 is formed in a frame shape along the peripheral edges of the pair of plate glasses 52 and 52. For example, as shown in FIG. 1, in the present embodiment, the sealing member 1 is formed in a rectangular frame shape. The

なお、密封部材1の形状については、本実施形態に限定されるものではない。
即ち、一対の板ガラス52・52の周縁部に沿った形状である限り、例えば、円形状や、矩形状以外の多角形状からなる枠体形状であってもよい。
In addition, about the shape of the sealing member 1, it is not limited to this embodiment.
That is, as long as it is the shape along the peripheral part of a pair of plate glass 52 * 52, the frame body shape which consists of polygonal shapes other than circular shape or a rectangular shape may be sufficient, for example.

密封部材1は、略「コ」字状の断面形状となるように形成される。
具体的には、図2に示すように、密封部材1は、各々の板ガラス52・52の端面52a・52a(図2においては、上端面)と当接しつつ端面52a・52aに沿って延設される基部11と、基部11における板ガラス52・52との当接面11aから密封部材1の内周側(図2における下側)へ延出し、板ガラス52・52の厚み方向に所定の間隔を有して対向配置される一対の支持部12・12とを備えている。
The sealing member 1 is formed to have a substantially “U” -shaped cross-sectional shape.
Specifically, as shown in FIG. 2, the sealing member 1 extends along the end surfaces 52 a and 52 a while abutting against the end surfaces 52 a and 52 a (upper end surfaces in FIG. 2) of the respective plate glasses 52 and 52. The base 11 is extended from the contact surface 11a of the base 11 with the plate glass 52/52 to the inner peripheral side (lower side in FIG. 2) of the sealing member 1, and a predetermined interval is provided in the thickness direction of the plate glass 52/52. And a pair of support portions 12 and 12 which are opposed to each other.

基部11の当接面11aの、積層体50Aの厚み方向における中央部には、断面視半円形状の溝形状からなる減圧通路11bが、基部11の延設方向に沿って形成される。
そして、一対の板ガラス52・52の周縁部に沿って密封部材1が嵌装された状態において、基部11の当接面11aが板ガラス52・52の端面52aに密着することにより、減圧通路11bは、一対の板ガラス52・52と樹脂製中間膜51との積層界面53・53と連通する。
A decompression passage 11b having a semicircular groove shape in cross-sectional view is formed along the extending direction of the base 11 at the center of the contact surface 11a of the base 11 in the thickness direction of the stacked body 50A.
Then, in a state where the sealing member 1 is fitted along the peripheral edge portions of the pair of plate glasses 52 and 52, the contact surface 11a of the base portion 11 comes into close contact with the end surface 52a of the plate glasses 52 and 52, whereby the decompression passage 11b is The laminated interfaces 53 and 53 between the pair of plate glasses 52 and 52 and the resin intermediate film 51 communicate with each other.

ここで、図3に示すように、樹脂製中間膜51が介在した状態で積層された板ガラス52・52は、互いに樹脂製中間膜51の厚み寸法分だけ離間しているが、減圧通路11bの半径寸法Rは、一対の板ガラス52・52の離間寸法Waに比べて、およそ1.5倍〜3倍(R=1.5Wa〜3Wa)程度となるように設定されている。
これにより、本圧着工程において、オートクレーブの炉内に投入された積層体50Aの真空引きを行う際に、樹脂製中間膜51が積層体50Aの端面52aから突出しすぎないようにすることが可能となり、合わせガラス50の品質向上を図ることができる。
Here, as shown in FIG. 3, the glass plates 52 and 52 laminated with the resin intermediate film 51 interposed are separated from each other by the thickness dimension of the resin intermediate film 51. The radial dimension R is set to be about 1.5 to 3 times (R = 1.5 Wa to 3 Wa) as compared with the separation dimension Wa of the pair of glass plates 52 and 52.
This makes it possible to prevent the resinous intermediate film 51 from protruding too much from the end surface 52a of the laminated body 50A when evacuating the laminated body 50A put into the autoclave furnace in the main crimping step. The quality of the laminated glass 50 can be improved.

即ち、本圧着工程において、オートクレーブの炉内を加熱・加圧処理するのと同時に、例えば、PVB(ポリビニルブチラール)やEVA(エチレンビニルアセテート)などからなる樹脂製中間膜51が介在する、一対の板ガラス52・52に対して真空引きを行う場合、樹脂製中間膜51は、加熱処理の影響によって軟化するとともに、加圧処理および真空引きの影響によって一対の板ガラス52・52の端面52aから突出しすぎる場合がある。
この際、一対の板ガラス52・52の端面52aから突出した樹脂製中間膜51は、減圧通路11bの内周面に到達した時点で塞き止められ、気泡のみが真空引きされる。
That is, in the main press-bonding step, a pair of intermediate layers 51 made of resin such as PVB (polyvinyl butyral) or EVA (ethylene vinyl acetate) are interposed at the same time as heating and pressurizing the inside of the autoclave furnace. When evacuating the plate glasses 52 and 52, the resin intermediate film 51 is softened by the influence of the heat treatment and excessively protrudes from the end surfaces 52a of the pair of plate glasses 52 and 52 by the influence of the pressure treatment and the evacuation. There is a case.
At this time, the resin intermediate film 51 protruding from the end surfaces 52a of the pair of glass plates 52 and 52 is blocked when reaching the inner peripheral surface of the decompression passage 11b, and only bubbles are evacuated.

その結果、樹脂製中間膜51の突出量が必要以上に多くなることはないため、各々の板ガラス52・52の周縁部において、樹脂製中間膜51の肉厚が薄くなりすぎ、各板ガラス52の側端部が湾曲しすぎて、合わせガラス50の品質が低下するような心配もない。   As a result, since the protrusion amount of the resin intermediate film 51 does not increase more than necessary, the thickness of the resin intermediate film 51 becomes too thin at the peripheral portions of the respective plate glasses 52 and 52, There is no concern that the side edge is too curved and the quality of the laminated glass 50 is degraded.

ところで、図2に示すように、互いに対向して配置される一対の支持部12・12において、各支持部12の内側面(対向面)には、突出部12aが形成される。
突出部12aは、支持部12の延設方向に沿って延設される。
また、突出部12aの突出端面は、基部11の当接面11aに対して直交し、且つ支持部12の延設方向に対して平行な平面形状に形成される。
By the way, as shown in FIG. 2, in a pair of support parts 12 and 12 arrange | positioned facing each other, the protrusion part 12a is formed in the inner surface (opposing surface) of each support part 12. As shown in FIG.
The protruding portion 12 a extends along the extending direction of the support portion 12.
Further, the projecting end surface of the projecting portion 12 a is formed in a planar shape that is orthogonal to the contact surface 11 a of the base portion 11 and parallel to the extending direction of the support portion 12.

そして、一対の支持部12・12において、各々の突出部12a・12a間の間隙寸法は、積層体50Aの厚み寸法(図2中の寸法W)と同程度または若干小さくなっている。   In the pair of support parts 12 and 12, the gap dimension between the projecting parts 12a and 12a is approximately the same as or slightly smaller than the thickness dimension (dimension W in FIG. 2) of the stacked body 50A.

このような形状からなる密封部材1を、一対の板ガラス52・52の周縁部に沿って嵌装する場合、一対の板ガラス52・52は、一対の支持部12・12の突出部12a・12aによって、積層体50Aが厚み方向に挟持されて、板ガラス52・52が厚み方向へ位置決めされることとなり、板ガラス52・52の厚み方向への歪みが発生するのを防止できる。
このように、支持部12・12の突出部12a・12aは、密封部材1を一対の板ガラス52・52の周縁部に嵌装した状態で、積層体50Aを厚み方向に挟持する挟持部としての機能を有している。
When the sealing member 1 having such a shape is fitted along the peripheral edge portions of the pair of plate glasses 52 and 52, the pair of plate glasses 52 and 52 is formed by the protruding portions 12a and 12a of the pair of support portions 12 and 12, respectively. The laminated body 50A is sandwiched in the thickness direction, and the plate glasses 52 and 52 are positioned in the thickness direction, so that the distortion in the thickness direction of the plate glasses 52 and 52 can be prevented.
As described above, the projecting portions 12a and 12a of the support portions 12 and 12 serve as sandwiching portions that sandwich the laminated body 50A in the thickness direction in a state where the sealing member 1 is fitted to the peripheral portions of the pair of glass plates 52 and 52. It has a function.

また、積層体50Aに対して密封部材1の嵌装作業が完了した後の状態においては、基部11の当接面11aに積層体50Aの端面52aが当接して、板ガラス52・52は板面方向へ位置決めされることとなる。これにより、板ガラス52・52の板面方向への位置ずれが発生するのを、防止することができる。
このように、基部11の当接面11aは、密封部材1を一対の板ガラス52・52の周縁部に嵌装した状態において、積層体50Aの端面52aと当接することにより、板ガラス52・52の板面方向への位置ずれを防止する当接部としての機能を有している。
Further, in a state after the sealing work of the sealing member 1 is completed with respect to the laminated body 50A, the end surface 52a of the laminated body 50A comes into contact with the contact surface 11a of the base 11, and the plate glasses 52 and 52 are made of plate surfaces. It will be positioned in the direction. Thereby, it can prevent that position shift to the plate surface direction of plate glass 52 * 52 occurs.
As described above, the contact surface 11a of the base portion 11 is in contact with the end surface 52a of the laminated body 50A in a state where the sealing member 1 is fitted to the peripheral edge portions of the pair of plate glasses 52 and 52. It has a function as an abutting portion that prevents displacement in the plate surface direction.

一方、各支持部12の先端部(基部11側とは反対側の端部)には、内側(対向方向側)且つ基部11側に向かって「レ」字状に屈曲した折返し部12bが形成される。   On the other hand, a folded portion 12b that is bent in a “let” shape toward the inner side (opposite direction side) and toward the base 11 side is formed at the distal end portion (the end opposite to the base 11 side) of each support portion 12. Is done.

このような形状からなる密封部材1を、積層される一対の板ガラス52・52の周縁部に沿って嵌装する場合、一対の板ガラス52・52の周縁部は、各々の折返し部12b・12bに沿って摺動しながら、一対の支持部12・12の間隙に挿入されることとなる。
これにより、密封部材1が積層体50Aに嵌設された状態において、折返し部12b・12bは、板ガラス52・52の板面に密着することとなり、基部11に形成される減圧通路11b内を外部からシールすることができ、減圧通路11bの気密性を高めることが可能となる。
このように、折返し部12b・12bは、密封部材1を一対の板ガラス52・52の周縁部に嵌装した状態で、減圧通路11bをシールするシール部としての機能を有している。
When the sealing member 1 having such a shape is fitted along the peripheral edges of the pair of laminated glass sheets 52 and 52, the peripheral edges of the pair of glass sheets 52 and 52 are respectively connected to the folded portions 12b and 12b. It slides along, and it will be inserted in the gap | interval of a pair of support part 12 * 12.
Thereby, in the state in which the sealing member 1 is fitted in the laminated body 50A, the folded portions 12b and 12b are in close contact with the plate surfaces of the plate glasses 52 and 52, and the inside of the decompression passage 11b formed in the base portion 11 is externally provided. Thus, the airtightness of the decompression passage 11b can be improved.
As described above, the folded portions 12b and 12b have a function as a seal portion that seals the decompression passage 11b in a state where the sealing member 1 is fitted to the peripheral portions of the pair of plate glasses 52 and 52.

以上のように、本実施形態における密封部材1は、各板ガラス52の周縁部において、板ガラス52の厚み方向への歪みや、板面方向(厚み方向との直交方向)への位置ずれなどを規制可能な断面形状(支持部12の突出部12a、および基部11の当接面11aを参照)を有している。
つまり、一対の板ガラス52・52の周縁部に沿って密封部材1が嵌装されることにより、各々の板ガラス52・52の積層姿勢は、堅固に保持される。
従って、本実施形態においては、例えば、各々の板ガラス52・52の積層姿勢を保持するための治具などを別途設けるような必要もなく、積層体50Aの周縁部に対して、板ガラス52・52の位置ずれを生じさせることなく容易に密封部材1を嵌装させることができる。
As described above, the sealing member 1 according to the present embodiment regulates distortion in the thickness direction of the plate glass 52 and displacement in the plate surface direction (a direction orthogonal to the thickness direction) at the peripheral edge of each plate glass 52. It has a possible cross-sectional shape (see the protrusion 12a of the support 12 and the contact surface 11a of the base 11).
That is, when the sealing member 1 is fitted along the peripheral edges of the pair of plate glasses 52 and 52, the stacked posture of the plate glasses 52 and 52 is firmly maintained.
Therefore, in the present embodiment, for example, it is not necessary to separately provide a jig or the like for maintaining the lamination posture of the respective plate glasses 52 and 52, and the plate glasses 52 and 52 are formed with respect to the peripheral portion of the laminated body 50A. Thus, the sealing member 1 can be easily fitted without causing the positional displacement.

また、本実施形態における密封部材1は、一対の板ガラス52・52の周縁部に沿って嵌装されることにより、内周部の気密性を確保可能な断面形状(支持部12の折返し部12bを参照)を有している。
従って、一対の板ガラス52・52の周縁部に密封部材1が嵌装された後、例えば、粘着テープなどを用いて、板ガラス52と密封部材1との当接部を封着する必要もなく、積層体50Aの周縁部(より具体的には、一対の板ガラス52・52の間隙)を、容易に密閉することができる。
特に、密封部材1においては、内周部の気密性を確保するためのシール部として折返し部12bを形成しているが、それに加えて突出部12aも内周部の気密性を確保するためのシール部として作用するため、2重のシール部を備えていることとなり、減圧通路11bの気密性を確実に確保することが可能となっている。
In addition, the sealing member 1 in the present embodiment is fitted along the peripheral edge portions of the pair of glass plates 52 and 52, so that the airtightness of the inner peripheral portion can be secured (the folded portion 12 b of the support portion 12). For example).
Therefore, after the sealing member 1 is fitted to the peripheral portions of the pair of plate glasses 52 and 52, for example, using an adhesive tape or the like, there is no need to seal the contact portion between the plate glass 52 and the sealing member 1, The peripheral edge of the laminated body 50A (more specifically, the gap between the pair of glass sheets 52 and 52) can be easily sealed.
In particular, in the sealing member 1, the folded portion 12b is formed as a seal portion for ensuring the airtightness of the inner peripheral portion. In addition, the protruding portion 12a is also used for ensuring the airtightness of the inner peripheral portion. Since it acts as a seal portion, it is provided with a double seal portion, so that the airtightness of the decompression passage 11b can be reliably ensured.

以上のことから、本実施形態における合わせガラスの製造方法においては、積層体50Aに対する密封部材1の嵌装作業、および密封作業の双方を容易に行うことができ、積層体50Aの真空引き作業の効率と密封信頼性との向上を図ることができる。   From the above, in the method for manufacturing laminated glass according to the present embodiment, both the fitting work of the sealing member 1 and the sealing work on the laminated body 50A can be easily performed, and the vacuuming work of the laminated body 50A can be performed. Efficiency and sealing reliability can be improved.

[第二の実施形態]
次に、第二の実施形態における合わせガラスの製造方法について、図4を用いて説明する。
[Second Embodiment]
Next, the manufacturing method of the laminated glass in 2nd embodiment is demonstrated using FIG.

前述した合わせガラス50において、樹脂製中間膜51(図2を参照)は、通常PVB、EVAなどにより形成されていた。
これに対して、第二の実施形態の合わせガラス60においては、耐熱性や耐燃性などに優れたフッ素樹脂からなる樹脂製中間膜61と、樹脂製中間膜61を介在させて積層される一対の板ガラス62・62とを備える積層体60Aが用いられる。
In the laminated glass 50 described above, the resin intermediate film 51 (see FIG. 2) is usually formed of PVB, EVA, or the like.
On the other hand, in the laminated glass 60 of the second embodiment, a pair of laminated intermediate films 61 made of a fluororesin excellent in heat resistance and flame resistance, and the intermediate film 61 made of resin. A laminated body 60 </ b> A including the plate glasses 62 and 62 is used.

ここで、フッ素樹脂は熱可塑性樹脂であり、加熱処理を行うことにより軟化するとともに、冷却に伴い収縮する。
そのため、図4(a)に示すように、例えば、常温時において、樹脂製中間膜61の外形寸法を、板ガラス62の端部より、数ミリ程度はみ出すようなサイズに予め設定していたとしても、図4(b)に示すように、本圧着工程における加熱処理の終了後、樹脂製中間膜61のガラス転移点以下にまで冷却された状態において、樹脂製中間膜61の外形寸法は、板ガラス62の端部より、逆に数ミリ程度内側に入り込むように収縮することがある。
その結果、一対の板ガラス62・62の周縁部においては、空隙が発生し、さらには樹脂製中間膜61の収縮に伴って複数の吸い込み泡が発生して、合わせガラス60の品質低下をもたらすおそれがあった。
Here, the fluororesin is a thermoplastic resin, and is softened by heat treatment and contracts with cooling.
Therefore, as shown in FIG. 4A, for example, the outer dimension of the resin intermediate film 61 may be set in advance to a size that protrudes about several millimeters from the end of the plate glass 62 at room temperature. As shown in FIG. 4 (b), after the heat treatment in the final press-bonding step, the outer dimensions of the resin intermediate film 61 are flat glass in a state where the resin intermediate film 61 is cooled to a temperature below the glass transition point. On the contrary, it may shrink so as to enter the inside by several millimeters from the end of 62.
As a result, gaps are generated at the peripheral edge portions of the pair of glass plates 62 and 62, and a plurality of suction bubbles are generated as the resin intermediate film 61 contracts, and the quality of the laminated glass 60 may be deteriorated. was there.

このようなことから、本実施形態における合わせガラスの製造方法においては、本圧着工程の終了後、オートクレーブの炉内より取出された一対の板ガラス62・62の温度が少なくとも常温にまで冷却されて、軟化した樹脂製中間膜61が硬化するまで、継続して真空引きを行うこととしている。
つまり、本実施形態においては、オートクレーブによる加熱・加圧処理の終了後、積層体60Aの温度が常温となるまで、継続して真空引きが行われる。
これにより、フッ素樹脂からなる樹脂製中間膜61のような、加熱処理により樹脂製中間膜61の外形寸法が収縮する現象を未然に防ぐことが可能となり、合わせガラス60の品質向上を図ることができる。
For this reason, in the method for producing a laminated glass in the present embodiment, the temperature of the pair of glass plates 62 and 62 taken out from the furnace of the autoclave is cooled to at least room temperature after the completion of the main pressure bonding step, The evacuation is continuously performed until the softened resin intermediate film 61 is cured.
That is, in this embodiment, after the heating / pressurizing process by the autoclave is completed, the evacuation is continuously performed until the temperature of the stacked body 60 </ b> A reaches the normal temperature.
This makes it possible to prevent a phenomenon in which the outer dimensions of the resin intermediate film 61 shrink due to heat treatment, such as the resin intermediate film 61 made of fluororesin, and to improve the quality of the laminated glass 60. it can.

[第三及び第四の実施形態]
次に、第三及び第四の実施形態における合わせガラスの製造方法について、図5を用いて説明する。
なお、以下の説明に関しては便宜上、図5の上下方向を密封部材101・201の上下方向と規定して記述する。
[Third and fourth embodiments]
Next, the manufacturing method of the laminated glass in 3rd and 4th embodiment is demonstrated using FIG.
In the following description, for convenience, the vertical direction of FIG. 5 is described as the vertical direction of the sealing members 101 and 201.

第三および第四の実施形態における密封部材101(または、密封部材201)は、前述した密封部材1と略同等な構成を有する一方、減圧通路111b(または、減圧通路211b)の形状について密封部材1と相違する。
よって、以下の説明においては、主に密封部材1との相違点について記載し、密封部材1との同等な構成についての記載は省略する。
The sealing member 101 (or the sealing member 201) in the third and fourth embodiments has a configuration substantially equivalent to that of the above-described sealing member 1, while the shape of the decompression passage 111b (or the decompression passage 211b) is a sealing member. 1 and different.
Therefore, in the following description, differences from the sealing member 1 are mainly described, and descriptions of the same configuration as the sealing member 1 are omitted.

密封部材101(または、密封部材201)は、複数(例えば、本実施形態においては二枚)の樹脂製中間膜151・151が介在する、複数(例えば、本実施形態においては三枚)の積層された板ガラス152・152・152の周縁部を密封するための部材である。
また、密封部材101(または、密封部材201)は、複数の板ガラス152・152・152と複数の樹脂製中間膜151・151との境界部(積層体150Aの積層界面153)と連通する減圧通路111b(または、減圧通路211b)を確保するとともに、減圧通路111b(または、減圧通路211b)を通じて、複数の積層された板ガラス152・152・152の周縁部を真空引きするための部材である。
The sealing member 101 (or the sealing member 201) is a laminate of a plurality (for example, three in the present embodiment) in which a plurality of (for example, two in the present embodiment) resin intermediate films 151 and 151 are interposed. It is a member for sealing the peripheral part of the plate glass 152 * 152 * 152 which was made.
Further, the sealing member 101 (or the sealing member 201) communicates with a boundary portion (a laminated interface 153 of the laminated body 150A) between the plurality of plate glasses 152, 152, 152 and the plurality of resin intermediate films 151, 151. This is a member for securing 111b (or reduced pressure passage 211b) and evacuating the peripheral portions of the plurality of laminated glass sheets 152, 152, and 152 through the reduced pressure passage 111b (or reduced pressure passage 211b).

図5(a)に示すように、第三の実施形態における密封部材101において、基部111の当接面111aの、積層体150Aの厚み方向における中央部には、断面視略半円形状(より具体的には、断面視長半円形状)の溝形状からなる減圧通路111bが、基部111の延設方向に沿って形成される。
ここで、減圧通路111bは、断面視にて、積層される複数の樹脂製中間膜151・151の端部を、同時に覆うことが可能な程度の長手寸法を有して形成される。
As shown in FIG. 5 (a), in the sealing member 101 according to the third embodiment, the central portion of the contact surface 111a of the base 111 in the thickness direction of the laminated body 150A has a substantially semicircular shape (more than Specifically, a decompression passage 111b having a groove shape with a semicircular shape in cross section is formed along the extending direction of the base 111.
Here, the decompression passage 111b is formed to have a longitudinal dimension capable of simultaneously covering the ends of the plurality of laminated resin intermediate films 151 and 151 in a cross-sectional view.

そして、複数の樹脂製中間膜151・151および板ガラス152・152・152からなる積層体150Aの周縁部に沿って密封部材101が嵌装された状態において、基部111の当接面111aが両外側の板ガラス152・152の端面152aに密着することにより、減圧通路111bは、複数の板ガラス152・152・152と複数の樹脂製中間膜151・151との積層境界153と連通することとなる。   In the state in which the sealing member 101 is fitted along the peripheral portion of the laminated body 150A composed of the plurality of resin intermediate films 151 and 151 and the plate glasses 152, 152, and 152, the contact surfaces 111a of the base 111 are on both outer sides. The pressure reducing passage 111b communicates with the laminated boundary 153 of the plurality of plate glasses 152, 152, 152 and the plurality of resin intermediate films 151, 151 by being in close contact with the end surfaces 152a of the plate glasses 152, 152.

一方、図5(b)に示すように、第四の実施形態における密封部材201において、基部211の当接面211aの、積層体150の厚み方向における中央部には、断面視半円形状の溝形状からなる複数(例えば、本実施形態において二箇所)の減圧通路211b・211bが、基部211の延設方向に沿って形成される。
ここで、これらの減圧通路211b・211bは、樹脂製中間膜151・151の枚数分だけ形成され、且つ、断面視にて、これらの樹脂製中間膜151・151の端部と各々対向する位置に配置される。
On the other hand, as shown in FIG. 5B, in the sealing member 201 according to the fourth embodiment, the contact surface 211a of the base 211 has a semicircular shape in cross-sectional view at the center in the thickness direction of the stacked body 150. A plurality of (for example, two places in this embodiment) decompression passages 211b and 211b each having a groove shape are formed along the extending direction of the base 211.
Here, the decompression passages 211b and 211b are formed by the number of the resin intermediate films 151 and 151, and are respectively opposed to the end portions of the resin intermediate films 151 and 151 in a sectional view. Placed in.

そして、複数の樹脂製中間膜151・151および板ガラス152・152・152からなる積層体150Aの周縁部に沿って密封部材201が嵌装された状態において、基部211の当接面211aが両外側の板ガラス152・152の端面152aに密着することにより、複数の減圧通路211b・211bは、複数の板ガラス152・152・152と複数の樹脂製中間膜151・151との積層境界153と連通している。   In the state where the sealing member 201 is fitted along the peripheral edge of the laminated body 150A composed of the plurality of resin intermediate films 151 and 151 and the plate glasses 152, 152, and 152, the contact surfaces 211a of the base 211 are on both outer sides. The plurality of decompression passages 211b and 211b communicate with a laminated boundary 153 of the plurality of plate glasses 152, 152, and 152 and the plurality of resin intermediate films 151 and 151 by being in close contact with the end surfaces 152a of the plate glasses 152 and 152. Yes.

なお、第四の実施形態における密封部材201において、形成される減圧通路211bの個数については、樹脂製中間膜151の枚数を超える(例えば、本実施形態においては3箇所以上)こととしてもよい。
但し、この場合、樹脂製中間膜151の端面と対向する位置にない減圧通路211bについては、板ガラス152の端面によって確実に閉塞される必要がある。
In the sealing member 201 according to the fourth embodiment, the number of decompression passages 211b formed may exceed the number of resin intermediate films 151 (for example, three or more in this embodiment).
However, in this case, the decompression passage 211 b that is not located at the position facing the end face of the resin intermediate film 151 needs to be reliably closed by the end face of the plate glass 152.

[第五の実施形態]
次に、第五の実施形態における合わせガラスの製造方法について、図6および図7を用いて説明する。
なお、以下の説明に関しては便宜上、図7の上下方向を密封部材301の上下方向と規定して記述する。
[Fifth embodiment]
Next, the manufacturing method of the laminated glass in 5th embodiment is demonstrated using FIG. 6 and FIG.
In addition, regarding the following description, for convenience, the vertical direction in FIG. 7 is described as the vertical direction of the sealing member 301.

第五の実施形態における密封部材301は、前述した密封部材1と略同等な構成を有する一方、一部の角部における断面形状について密封部材1と相違する。
よって、以下の説明においては、主に密封部材1との相違点について記載し、密封部材1との同等な構成についての記載は省略する。
The sealing member 301 in the fifth embodiment has a configuration that is substantially equivalent to the sealing member 1 described above, but differs from the sealing member 1 in the cross-sectional shape at some corners.
Therefore, in the following description, differences from the sealing member 1 are mainly described, and descriptions of the same configuration as the sealing member 1 are omitted.

図6に示すように、本実施形態における密封部材301において、その一部の角部には、配管部材321の一端部と接続可能な接続口315が形成される。
接続口315は、密封部材301の内周側へと延出し、減圧通路311bと連通される。
As shown in FIG. 6, in the sealing member 301 in the present embodiment, a connection port 315 that can be connected to one end of the piping member 321 is formed at a part of the corner.
The connection port 315 extends to the inner peripheral side of the sealing member 301 and communicates with the decompression passage 311b.

そして、配管部材321の他端部は、真空ポンプ322に接続される。
これにより、減圧通路311bは、接続口315および配管部材321を介して、真空ポンプ322と連通される。
The other end of the piping member 321 is connected to the vacuum pump 322.
As a result, the decompression passage 311 b communicates with the vacuum pump 322 via the connection port 315 and the piping member 321.

密封部材301は、略「コ」字状の断面形状となるように形成される。
そして、図7に示すように、基部311と、基部311における板ガラス352・352との当接面311aより延出する支持部312と、板ガラス352とによって囲まれた、突出部312aの上部に位置する第一空間部313、および下部に位置する第二空間部314が形成される。
The sealing member 301 is formed to have a substantially “U” -shaped cross-sectional shape.
Then, as shown in FIG. 7, the base 311, the support portion 312 extending from the contact surface 311 a of the base 311 with the plate glasses 352 and 352, and the plate glass 352 are positioned above the protruding portion 312 a. The first space portion 313 to be formed and the second space portion 314 located at the lower portion are formed.

ここで、接続口315を有した一部の角部において、密封部材301の厚み方向の両側面には、第一凹部316・316が各々形成されるとともに、支持部312・312の突出部312a・312aの突出端面には、第二凹部317・317が各々形成される。   Here, in some corners having the connection port 315, first concave portions 316 and 316 are formed on both side surfaces in the thickness direction of the sealing member 301, respectively, and the protruding portions 312a of the support portions 312 and 312 are formed. Second protrusions 317 and 317 are formed on the protruding end surface of 312a, respectively.

なお、第一凹部316の開口部は、例えば、板状の閉塞部材318によって閉塞されることからり、当該第一凹部316は、密閉された空間部として構成される。
また、第二凹部317は、下方側(折返し部312b側)に向かって延出し、第二空間部314(支持部312の突出部312aと、折返し部312bと、積層体50Aの最外層における板ガラス52の板面とによって囲まれた空間部)と連通される。
In addition, since the opening part of the 1st recessed part 316 is obstruct | occluded by the plate-shaped obstruction | occlusion member 318, the said 1st recessed part 316 is comprised as a sealed space part, for example.
Moreover, the 2nd recessed part 317 is extended toward the downward side (folding part 312b side), and the 2nd space part 314 (the protrusion part 312a of the support part 312, the folding | returning part 312b, and the plate glass in the outermost layer of the laminated body 50A). And a space surrounded by 52 plate surfaces).

そして、第一凹部316の底面316aにおいて、その一端部より接続口315に向かって第一貫通経路319が穿孔されるとともに、その他端部より第二凹部317に向かって第二貫通経路320が穿孔される。   Then, a first through path 319 is drilled from one end of the bottom surface 316a of the first recess 316 toward the connection port 315, and a second through path 320 is drilled from the other end toward the second recess 317. Is done.

このように、本実施形態における密封部材301において、接続口315は、減圧通路311bに連通される一方、第一貫通経路319、第一凹部316、および第二貫通経路320を介して、第二空間部314にも連通される。
つまり、減圧通路311bおよび第二空間部314は、接続口315を介して、互いに独立して真空ポンプ322に連通されており、第二空間部314に対する真空引き処理を、減圧通路311bとは独立した経路となる第一貫通経路319、第一凹部316、および第二貫通経路320を用いて行うことが可能となっている。
Thus, in the sealing member 301 in the present embodiment, the connection port 315 communicates with the decompression passage 311b, while the second through passage 319, the first recess 316, and the second through passage 320 pass through the second. The space portion 314 is also communicated.
That is, the decompression passage 311b and the second space portion 314 are communicated with the vacuum pump 322 independently of each other via the connection port 315, and the vacuuming process for the second space portion 314 is performed independently of the decompression passage 311b. The first through path 319, the first recess 316, and the second through path 320, which are the above-described paths, can be performed.

ところで、第一の実施形態において、密封部材1の減圧通路11bを介して、積層体50Aの積層界面53・53を真空引きすると、前述したように、減圧通路11b内にて、樹脂製中間膜51が、板ガラス52・52の端面52a・52aより突出する。
それによって、樹脂製中間膜51の肉厚が薄くなり、各々の板ガラス52・52の側端部は、互いが近接する方向へ僅かに湾曲する場合がある。
その結果、密封部材1の当接面11aと、板ガラス52・52の端面52a・52aとの間、および板ガラス52・52の表面と突出部12a・12aとの間には、僅かな隙間が形成され、減圧通路11bは、当該隙間を通じて、基部11と、支持部12と、板ガラス52とによって囲まれた、突出部12aの上部に位置する第一空間部13、および下部に位置する第二空間部14と連通されることとなる。
そして、減圧通路11bを介して、第一空間部13および第二空間部14が同時に真空引きされることとなり、突出部12aおよび折返し部12bは、板ガラス52の板面に対してさらに強固に密着され、減圧通路11bの気密性が確保される。
By the way, in 1st embodiment, when the lamination | stacking interface 53 * 53 of 50 A of laminated bodies is evacuated through the pressure reduction channel | path 11b of the sealing member 1, as above-mentioned, in the pressure reduction channel | path 11b, resin-made intermediate films 51 protrudes from the end surfaces 52a and 52a of the plate glass 52 and 52.
Thereby, the thickness of the resin intermediate film 51 is reduced, and the side end portions of the respective plate glasses 52 and 52 may be slightly curved in the direction in which they are close to each other.
As a result, a slight gap is formed between the contact surface 11a of the sealing member 1 and the end surfaces 52a and 52a of the plate glasses 52 and 52, and between the surface of the plate glasses 52 and 52 and the protruding portions 12a and 12a. The decompression passage 11b is surrounded by the base portion 11, the support portion 12, and the plate glass 52 through the gap, and the first space portion 13 located above the protruding portion 12a and the second space located below. The unit 14 communicates with the unit 14.
Then, the first space portion 13 and the second space portion 14 are simultaneously evacuated via the decompression passage 11b, and the protruding portion 12a and the folded portion 12b are more firmly adhered to the plate surface of the plate glass 52. Thus, the air tightness of the decompression passage 11b is ensured.

板ガラス52・52の端面52a・52aより突出した樹脂製中間膜51によって、減圧通路11b内が封鎖された場合、真空ポンプ22(図1を参照)によって、積層体50Aの積層界面53・53を真空引きすることはできず、第一空間部13および第二空間部14を真空引きすることも不可能となる場合がある。
その結果、板ガラス52の板面に対して、突出部12aおよび折返し部12bを密着させることは困難であり、減圧通路11bの気密性を維持することが難しく、樹脂製中間膜51の収縮に伴って複数の吸い込み泡が発生して、合わせガラス50の品質低下をもたらすおそれがあった。
When the inside of the decompression passage 11b is blocked by the resin intermediate film 51 protruding from the end faces 52a and 52a of the plate glasses 52 and 52, the laminated interfaces 53 and 53 of the laminated body 50A are caused to be sealed by the vacuum pump 22 (see FIG. 1). It cannot be evacuated, and it may be impossible to evacuate the first space 13 and the second space 14.
As a result, it is difficult to closely contact the protruding portion 12a and the folded portion 12b with the plate surface of the plate glass 52, and it is difficult to maintain the airtightness of the decompression passage 11b. In some cases, a plurality of sucking bubbles are generated and the quality of the laminated glass 50 is deteriorated.

本実施形態では、上述した構成を有することにより、例えば、板ガラス352・352の端面352a・352aより突出された樹脂製中間膜351によって、減圧通路311b内が封鎖されたとしても、真空ポンプ322(図6を参照)によって、第二空間部314を真空引きすることが可能となり、板ガラス352の板面に対して、突出部312aおよび折返し部312bを密着させておくことができる。
よって、減圧通路311bの気密性を確保することが可能となり、例えば、樹脂製中間膜351の収縮に伴って発生する吸い込み泡を、極力防止することができる。また、一対の支持部312・312の突出部312a・312aによって、積層体350Aが厚み方向に堅固に挟持されることから、積層体350Aの積層姿勢を確実に保持することができる。
その結果、合わせガラス350の品質低下の防止を図ることができる。
In the present embodiment, by having the above-described configuration, for example, even if the inside of the decompression passage 311b is blocked by the resin intermediate film 351 protruding from the end surfaces 352a and 352a of the plate glasses 352 and 352, the vacuum pump 322 ( 6), the second space 314 can be evacuated, and the protruding portion 312a and the folded portion 312b can be brought into close contact with the plate surface of the plate glass 352.
Therefore, it becomes possible to ensure the airtightness of the decompression passage 311b, and for example, it is possible to prevent as much as possible the sucked bubbles generated as the resin intermediate film 351 contracts. In addition, since the stacked body 350A is firmly sandwiched in the thickness direction by the protruding portions 312a and 312a of the pair of support portions 312 and 312, the stacked posture of the stacked body 350A can be reliably maintained.
As a result, it is possible to prevent the quality of the laminated glass 350 from being deteriorated.

なお、密封部材301における、減圧通路311bおよび第二空間部314の構成については、本実施形態に限定されるものではなく、互いに独立して真空ポンプ322に連通される限り、何れのような構成であってもよい。
例えば、減圧通路311bに連通される接続口、および第二空間部314に連通される接続口を各々設け、これらの接続口を介して、互いに独立して真空ポンプ322に連通されるような構成であってもよい。
Note that the configurations of the decompression passage 311b and the second space portion 314 in the sealing member 301 are not limited to the present embodiment, and any configuration as long as they communicate with the vacuum pump 322 independently of each other. It may be.
For example, a connection port that communicates with the decompression passage 311b and a connection port that communicates with the second space portion 314 are provided, and the vacuum pump 322 communicates with each other via these connection ports. It may be.

1 密封部材
11a 当接面(当接部)
11b 減圧通路
12a 突出部(挟持部)
12b 折返し部(シール部)
50 合わせガラス
50A 積層体
51 樹脂製中間膜
52 板ガラス
53 積層界面
60 合わせガラス
60A 積層体
61 樹脂製中間膜
62 板ガラス
101 密封部材
111a 当接面(当接部)
111b 減圧通路
150 合わせガラス
150A 積層体
151 樹脂製中間膜
152 板ガラス
153 積層界面
201 密封部材
211a 当接面(当接部)
211b 減圧通路
1 Sealing member 11a Contact surface (contact portion)
11b Pressure reducing passage 12a Protruding part (clamping part)
12b Folding part (seal part)
DESCRIPTION OF SYMBOLS 50 Laminated glass 50A Laminate body 51 Resin intermediate film 52 Plate glass 53 Laminate interface 60 Laminated glass 60A Laminate body 61 Resin intermediate film 62 Plate glass 101 Sealing member 111a Contact surface (contact part)
111b Decompression passage 150 Laminated glass 150A Laminate 151 Resin intermediate film 152 Sheet glass 153 Lamination interface 201 Sealing member 211a Abutting surface (abutting part)
211b Pressure reducing passage

Claims (6)

少なくとも二枚の板ガラスの間に樹脂製中間膜を介在させて積層させた積層体に対して、オートクレーブによる加熱・加圧処理を行うと同時に、前記積層体の周縁部に対して密封部材を嵌装して真空引き処理を行うことにより、前記板ガラスを互いに圧着させて合わせガラスを製造する、合わせガラスの製造方法であって、
前記密封部材は、
前記積層体の周縁部に対して嵌装された状態において、
前記積層体の積層界面と連通する減圧通路と、
前記積層体の端面と当接する当接部と、
前記積層体を厚み方向に挟持する挟持部と、
を備え、
前記真空引き処理は、
前記密封部材を前記積層体の周縁部に対して嵌装することにより、
前記当接部を前記積層体の端面に当接させ、
前記挟持部により前記積層体を厚み方向に挟持した状態で、
前記減圧通路を通じて行われるとともに、
前記密封部材は、
前記積層体の最外層における前記板ガラスの板面に密着するシール部をさらに備え、
前記密封部材を前記積層体の周縁部に対して嵌装することにより、
前記シール部を前記積層体の最外層における前記板ガラスの板面に密着させ、
前記挟持部と、前記シール部と、前記積層体の最外層における前記板ガラスの板面とによって囲まれた空間部に対しても、前記真空引き処理を行う
ことを特徴とする合わせガラスの製造方法。
At the same time that the laminated body laminated with a resin interlayer between at least two plate glasses is heated and pressurized by an autoclave, a sealing member is fitted to the periphery of the laminated body. A laminated glass manufacturing method for producing laminated glass by pressure-bonding the plate glasses to each other by performing a vacuum drawing process.
The sealing member is
In a state of being fitted to the peripheral edge of the laminate,
A decompression passage communicating with the laminate interface of the laminate;
A contact portion that contacts the end face of the laminate;
A sandwiching section for sandwiching the laminate in the thickness direction;
With
The vacuuming process is
By fitting the sealing member to the peripheral edge of the laminate,
Abutting the abutting part on the end surface of the laminate,
In a state where the laminate is sandwiched in the thickness direction by the sandwiching portion,
Performed through the decompression passage ,
The sealing member is
A seal part that is in close contact with the plate surface of the plate glass in the outermost layer of the laminate,
By fitting the sealing member to the peripheral edge of the laminate,
Adhering the seal part to the plate surface of the plate glass in the outermost layer of the laminate,
The vacuuming process is performed also on the space part surrounded by the sandwiching part, the seal part, and the plate surface of the plate glass in the outermost layer of the laminate ,
The manufacturing method of the laminated glass characterized by the above-mentioned.
前記減圧通路は、断面視半円形状に形成される、
ことを特徴とする、請求項1に記載の合わせガラスの製造方法。
The decompression passage is formed in a semicircular shape in a sectional view.
Wherein the method for producing a laminated glass according to claim 1.
前記積層体は、二枚の板ガラス間に樹脂製中間膜を介在させた積層体であり、
前記減圧通路の半径寸法は、前記一対の板ガラスの間隙寸法の、1.5倍以上且つ3倍以下に設定される、
ことを特徴とする、請求項1または請求項2に記載の合わせガラスの製造方法。
The laminate is a laminate in which a resin intermediate film is interposed between two sheet glasses,
The radial dimension of the decompression passage is set to be 1.5 times or more and 3 times or less the gap dimension of the pair of plate glasses.
The manufacturing method of the laminated glass of Claim 1 or Claim 2 characterized by the above-mentioned.
前記空間部に対する真空引き処理は、
前記減圧通路とは独立した経路を用いて行う、
ことを特徴とする、請求項1〜請求項3の何れか一項に記載の合わせガラスの製造方法。
The vacuuming process for the space part is as follows:
Using a path independent of the decompression passage,
The manufacturing method of the laminated glass as described in any one of Claims 1-3 characterized by the above-mentioned.
前記樹脂製中間膜は、フッ素樹脂を含む、
ことを特徴とする、請求項1〜請求項の何れか一項に記載の合わせガラスの製造方法。
The resin intermediate film includes a fluororesin,
The manufacturing method of the laminated glass as described in any one of Claims 1-4 characterized by the above-mentioned.
前記真空引き処理は、前記加熱・加圧処理の終了後、前記樹脂製中間膜の温度がガラス転移点以下となるまで継続して行われる、
ことを特徴とする、請求項に記載の合わせガラスの製造方法。
The vacuuming process is continuously performed after the heating / pressurizing process is completed until the temperature of the resinous intermediate film is equal to or lower than the glass transition point,
The manufacturing method of the laminated glass of Claim 5 characterized by the above-mentioned.
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