JP6261094B2 - 難燃性放射線硬化性組成物 - Google Patents
難燃性放射線硬化性組成物 Download PDFInfo
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- C03C27/00—Joining pieces of glass to pieces of other inorganic material; Joining glass to glass other than by fusing
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- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
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- B32B2307/3065—Flame resistant or retardant, fire resistant or retardant
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Description
(a)3〜90重量%の、1つ以上の(メタ)アクリル基又はビニル基を有する少なくとも1種のオリゴマー、
(b)10〜97重量%の、1つ以上の(メタ)アクリル基又はビニル基を有する少なくとも1種の反応性脂肪族ハロゲン化難燃添加剤、
(c)場合により、0〜87重量%の、少なくとも1種の非反応性ハロゲン化難燃添加剤、及び、
(d)場合により、0〜19重量%の、1つ以上の(メタ)アクリル基又はビニル基を有する少なくとも1種のモノマー。
(a)5〜80重量%の、1つ以上の(メタ)アクリル基又はビニル基を有する少なくとも1種のオリゴマー、
(b)20〜90重量%の、1つ以上の(メタ)アクリル基又はビニル基を有する少なくとも1種の反応性脂肪族ハロゲン化難燃添加剤、
(c)5〜59重量%の、少なくとも1種の非反応性ハロゲン化難燃添加剤。
(a)本発明による難燃性組成物を用意する工程、
(b)セラミック窓ガラス、ホウケイ酸窓ガラス、ソーダ石灰窓ガラス又はガラス風パネルから選択される2枚の窓ガラスの間に当該難燃性組成物を置く工程、
(c)該組成物を硬化して、該窓ガラス間に中間層を形成する工程。
本発明を以下に記す。
[発明1]
以下を含有する放射線硬化性難燃性組成物:
(a)3〜90重量%の、1つ以上の(メタ)アクリル基又はビニル基を有する少なくとも1種のオリゴマー、
(b)10〜97重量%の、1つ以上の(メタ)アクリル基又はビニル基を有する少なくとも1種の反応性脂肪族ハロゲン化難燃添加剤、
(c)場合により、0〜87%の、少なくとも1種の非反応性ハロゲン化難燃添加剤、及び
(d)場合により、0〜19重量%の、1つ以上の(メタ)アクリル基又はビニル基を有する少なくとも1種のモノマー。
[発明2]
以下を含有する、発明1に記載の放射線硬化性組成物:
(a)5〜80重量%の、1つ以上の(メタ)アクリル基又はビニル基を有する少なくとも1種のオリゴマー、
(b)20〜90重量%の、1つ以上の(メタ)アクリル基又はビニル基を有する少なくとも1種の反応性脂肪族ハロゲン化難燃添加剤、
(c)5〜59重量%の、少なくとも1種の非反応性ハロゲン化難燃添加剤。
[発明3]
該オリゴマーがウレタン(メタ)アクリレート、ポリエステル(メタ)アクリレート及びエポキシ(メタ)アクリレートから選択される、発明1又は2に記載の放射線硬化性組成物。
[発明4]
該反応性脂肪族ハロゲン化難燃添加剤が脂肪族ハロゲン化(メタ)アクリレートである、発明1〜3のいずれか一項に記載の放射線硬化性組成物。
[発明5]
該反応性脂肪族ハロゲン化難燃添加剤が脂肪族臭素化(メタ)アクリレートである、発明1〜4のいずれか一項に記載の放射線硬化性組成物。
[発明6]
該反応性脂肪族ハロゲン化難燃添加剤が少なくとも40重量%の臭素含量を有する臭素化難燃添加剤である、発明1〜5のいずれか一項に記載の放射線硬化性組成物。
[発明7]
該反応性臭素化難燃添加剤が式Iのトリブロモネオペンチルアルコールアクリレートである、発明1〜6のいずれか一項に記載の放射線硬化性組成物。
[化1]
[発明8]
該非反応性ハロゲン化難燃剤が20℃のn−ブチルアクリレート中で又はトリブロモネオペンチルアルコールアクリレート中で少なくとも10g/Lの溶解度を有するハロゲン化難燃剤から選択される、発明1〜7のいずれか一項に記載の放射線硬化性組成物。
[発明9]
該非反応性ハロゲン化難燃剤が少なくとも40重量%の臭素含量を示す臭素化難燃剤である、発明1〜8のいずれか一項に記載の放射線硬化性組成物
[発明10]
該非反応性ハロゲン化難燃剤がトリブロモネオペンチルアルコールである、発明1〜9のいずれか一項に記載の放射線硬化性組成物。
[発明11]
リン含有難燃添加剤を含有しない、発明1〜10のいずれか一項に記載の放射線硬化性組成物
[発明12]
セラミック窓ガラス、ホウケイ酸窓ガラス、ソーダ石灰窓ガラス又はガラス風パネルから選択される少なくとも1種の窓ガラスと発明1〜11のいずれか一項に記載の組成物から得られる少なくとも1の層とを具備する、ガラス積層物。
[発明13]
該窓ガラスがソーダ石灰窓ガラス、セラミック窓ガラス又はホウケイ酸窓ガラスから選択され、場合により強化されてもよい、発明12に記載のガラス積層物。
[発明14]
ソーダ石灰窓ガラスがセラミック窓ガラスと又はホウケイ酸窓ガラスと組み合わされる、発明12及び13のいずれか一項に記載のガラス積層物。
[発明15]
以下の工程を含む、少なくとも2枚の窓ガラスを具備するガラス積層物を製造する方法:
(a)発明1〜11のいずれか一項に記載の難燃性組成物を用意する工程、
(b)セラミック窓ガラス、ホウケイ酸窓ガラス、ソーダ石灰窓ガラス又はガラス風パネルから選択される2枚の窓ガラスの間に該難燃性組成物を置く工程、
(c)該組成物を硬化して、該窓ガラス間に中間層を形成する工程。
Claims (17)
- 以下を含有する放射線硬化性難燃性組成物:
(a)5〜80重量%の、1つ以上の(メタ)アクリル基を有する少なくとも1種のオリゴマーであって、ウレタン(メタ)アクリレートである、少なくとも1種のオリゴマー、
(b)20〜94重量%の、1つ以上の(メタ)アクリル基を有する少なくとも1種の反応性脂肪族ハロゲン化難燃添加剤であって、脂肪族ハロゲン化(メタ)アクリレートである、少なくとも1種の反応性脂肪族ハロゲン化難燃添加剤、
(c)1〜59重量%の、少なくとも1種の非反応性ハロゲン化難燃添加剤であって、ハロゲン化アルコールである、少なくとも1種の非反応性ハロゲン化難燃添加剤、及び
(d)0〜15重量%の、1つ以上の(メタ)アクリル基を有する少なくとも1種のモノマーであって、モノ−、ジ−、トリ−、及び/又はテトラ−(メタ)アクリレートである、少なくとも1種のモノマー、
であって、(a)〜(d)の合計が100重量%を超えない、
放射線硬化性難燃性組成物。 - 以下を含有する、請求項1に記載の放射線硬化性難燃性組成物:
(a)5〜30重量%の、該1つ以上の(メタ)アクリル基を有する少なくとも1種のオリゴマー、
(b)20〜90重量%の、該1つ以上の(メタ)アクリル基を有する少なくとも1種の反応性脂肪族ハロゲン化難燃添加剤、
(c)5〜59%の、該少なくとも1種の非反応性ハロゲン化難燃添加剤、及び
(d)0〜15重量%の、該1つ以上の(メタ)アクリル基を有する少なくとも1種のモノマー。 - 以下を含有する、請求項1に記載の放射線硬化性難燃性組成物:
(a)5〜30重量%の、該1つ以上の(メタ)アクリル基を有する少なくとも1種のオリゴマー、
(b)20〜90重量%の、該1つ以上の(メタ)アクリル基を有する少なくとも1種の反応性脂肪族ハロゲン化難燃添加剤、
(c)5〜59重量%の、該少なくとも1種の非反応性ハロゲン化難燃添加剤。 - 該少なくとも1種のオリゴマーが1つ以上のアクリル基を有している、請求項1〜3のいずれか一項に記載の放射線硬化性難燃性組成物。
- 該少なくとも1種のオリゴマーが脂肪族ウレタンアクリレートである、請求項1〜4のいずれか一項に記載の放射線硬化性難燃性組成物。
- 該反応性脂肪族ハロゲン化難燃添加剤が脂肪族臭素化(メタ)アクリレートである、請求項1〜5のいずれか一項に記載の放射線硬化性難燃性組成物。
- 該反応性脂肪族ハロゲン化難燃添加剤が少なくとも40重量%の臭素含量を有する臭素化難燃添加剤である、請求項1〜6のいずれか一項に記載の放射線硬化性難燃性組成物。
- 該非反応性ハロゲン化難燃剤が20℃のn−ブチルアクリレート中で又はトリブロモネオペンチルアルコールアクリレート中で少なくとも10g/Lの溶解度を有するハロゲン化難燃剤から選択される、請求項1〜8のいずれか一項に記載の放射線硬化性難燃性組成物。
- 該非反応性ハロゲン化難燃剤が少なくとも40重量%の臭素含量を示す臭素化難燃剤である、請求項1〜9のいずれか一項に記載の放射線硬化性難燃性組成物。
- 該非反応性ハロゲン化難燃剤がトリブロモネオペンチルアルコールである、請求項1〜10のいずれか一項に記載の放射線硬化性難燃性組成物。
- リン含有難燃添加剤を含有しない、請求項1〜11のいずれか一項に記載の放射線硬化性難燃性組成物。
- セラミック窓ガラス、ホウケイ酸窓ガラス、ソーダ石灰窓ガラス又はガラス風パネルから選択される少なくとも1種の窓ガラスと請求項1〜12のいずれか一項に記載の放射線硬化性難燃性組成物から得られる少なくとも1の層とを具備する、ガラス積層物。
- 該窓ガラスがソーダ石灰窓ガラス、セラミック窓ガラス又はホウケイ酸窓ガラスから選択される、請求項13に記載のガラス積層物。
- ガラス積層物が強化されている、請求項14に記載のガラス積層物。
- ソーダ石灰窓ガラスがセラミック窓ガラスと又はホウケイ酸窓ガラスと組み合わされる、請求項13〜15のいずれか一項に記載のガラス積層物。
- 以下の工程を含む、少なくとも2枚の窓ガラスを具備するガラス積層物を製造する方法:
(a)請求項1〜12のいずれか一項に記載の放射線硬化性難燃性組成物を用意する工程、
(b)セラミック窓ガラス、ホウケイ酸窓ガラス、ソーダ石灰窓ガラス又はガラス風パネルから選択される2枚の窓ガラスの間に該放射線硬化性難燃性組成物を置く工程、
(c)該放射線硬化性難燃性組成物を硬化して、該窓ガラス間に中間層を形成する工程。
Applications Claiming Priority (3)
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PCT/EP2012/061896 WO2013189537A1 (en) | 2012-06-20 | 2012-06-20 | Flame retardant radiation curable compositions |
EPPCT/EP2012/061896 | 2012-06-20 | ||
PCT/EP2013/062222 WO2013189821A1 (en) | 2012-06-20 | 2013-06-13 | Flame retardant radiation curable compositions |
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JP2015526540A JP2015526540A (ja) | 2015-09-10 |
JP6261094B2 true JP6261094B2 (ja) | 2018-01-17 |
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US (1) | US20150132584A1 (ja) |
JP (1) | JP6261094B2 (ja) |
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WO (2) | WO2013189537A1 (ja) |
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FR3012072B1 (fr) * | 2013-10-23 | 2021-01-01 | Saint Gobain | Verre feuillete mince pour pare-brise |
FR3012071B1 (fr) * | 2013-10-23 | 2021-01-01 | Saint Gobain | Verre feuillete mince |
NL2015787B1 (nl) * | 2015-11-13 | 2017-06-02 | Air-Craftglass Inc | Laminaat van glas en werkwijze voor het vervaardigen ervan. |
KR102079384B1 (ko) * | 2016-11-02 | 2020-02-19 | 주식회사 케이씨씨 | 난연성 도료 조성물 |
US11479504B2 (en) * | 2018-09-06 | 2022-10-25 | O'keeffe's, Inc. | Fire-rated glass unit |
EP4304833A1 (en) * | 2021-03-10 | 2024-01-17 | 3D Systems, Inc. | Flame resistant build materials and associated printed 3d articles |
EP4369098A1 (en) | 2022-11-14 | 2024-05-15 | Cubicure GmbH | Resin composition |
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JPS5040656A (ja) * | 1973-08-07 | 1975-04-14 | ||
SE423024B (sv) | 1978-03-01 | 1982-04-13 | Bertil Persson | Formningsmaskin |
US4234533A (en) | 1978-10-31 | 1980-11-18 | Mary Frances Theresa Langlands | Method of bonding spaced sheets by molding resin therebetween |
US4591522A (en) * | 1985-01-04 | 1986-05-27 | W. R. Grace & Co. | Liquid photopolymers curable to fire-retardant, hydrolysis resistant compositions |
US4724023A (en) | 1985-04-09 | 1988-02-09 | E M Partners Ag | Method of making laminated glass |
JPS6280602A (ja) * | 1985-10-04 | 1987-04-14 | Toray Ind Inc | 高屈折率プラスチツクレンズ |
NL8503234A (nl) * | 1985-11-25 | 1987-06-16 | Philips Nv | Matrijs. |
US5426166A (en) * | 1994-01-26 | 1995-06-20 | Caschem, Inc. | Urethane adhesive compositions |
US5479555A (en) * | 1994-06-09 | 1995-12-26 | Rot; Alfred | Photopolymerizable compositions for making optical materials and process making them |
JP4707130B2 (ja) * | 2001-04-12 | 2011-06-22 | 第一工業製薬株式会社 | 高分子難燃剤およびそれを含む難燃性熱可塑性樹脂組成物 |
EP1556210A1 (en) | 2002-10-18 | 2005-07-27 | Surface Specialties, S.A. | Flame retardant translucent laminate and method of producing such a laminate |
DE10248843B4 (de) | 2002-10-19 | 2005-01-20 | Daimlerchrysler Ag | Vorrichtung zum Steuern eines Motors oder Getriebes |
CA2510359A1 (en) * | 2002-12-20 | 2004-07-08 | Ciba Specialty Chemicals Holding Inc. | Method for forming functional layers |
EP1624012B2 (en) * | 2003-05-12 | 2015-09-02 | Teijin Chemicals, Ltd. | Sheet-form window member and window structure |
CN1886438A (zh) | 2003-12-02 | 2006-12-27 | 帝斯曼知识产权资产管理有限公司 | 阻燃可辐射固化组合物 |
WO2007007332A1 (en) | 2005-07-12 | 2007-01-18 | H.P.O.P - High Performance Optical Polymers Ltd. | Tribromoneopentyl (meth)acrylate based copolymers and lenses made therefrom |
EP2108508A1 (en) * | 2008-04-07 | 2009-10-14 | Cytec Surface Specialties, S.A. | Flame retardant radiation curable compositions |
DE102008054149A1 (de) * | 2008-10-31 | 2010-05-12 | Schott Ag | Brandschutzgläser mit UV-härtbarer Zwischenschicht |
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2012
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- 2013-06-13 JP JP2015517689A patent/JP6261094B2/ja not_active Expired - Fee Related
- 2013-06-13 US US14/396,195 patent/US20150132584A1/en not_active Abandoned
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WO2013189537A1 (en) | 2013-12-27 |
US20150132584A1 (en) | 2015-05-14 |
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