JP6049713B2 - 溶融製品の製造法 - Google Patents
溶融製品の製造法 Download PDFInfo
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- JP6049713B2 JP6049713B2 JP2014520763A JP2014520763A JP6049713B2 JP 6049713 B2 JP6049713 B2 JP 6049713B2 JP 2014520763 A JP2014520763 A JP 2014520763A JP 2014520763 A JP2014520763 A JP 2014520763A JP 6049713 B2 JP6049713 B2 JP 6049713B2
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- 238000004519 manufacturing process Methods 0.000 title claims description 16
- 238000000034 method Methods 0.000 claims description 56
- 239000002245 particle Substances 0.000 claims description 49
- 238000002844 melting Methods 0.000 claims description 41
- 230000008018 melting Effects 0.000 claims description 41
- 239000000203 mixture Substances 0.000 claims description 37
- 239000011344 liquid material Substances 0.000 claims description 34
- 239000007788 liquid Substances 0.000 claims description 22
- 238000010438 heat treatment Methods 0.000 claims description 18
- 229910052744 lithium Inorganic materials 0.000 claims description 17
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 15
- 238000001816 cooling Methods 0.000 claims description 15
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 14
- 229910052760 oxygen Inorganic materials 0.000 claims description 14
- 239000001301 oxygen Substances 0.000 claims description 14
- 239000002994 raw material Substances 0.000 claims description 12
- 229910052742 iron Inorganic materials 0.000 claims description 11
- 238000006467 substitution reaction Methods 0.000 claims description 10
- 238000000227 grinding Methods 0.000 claims description 9
- 229910052758 niobium Inorganic materials 0.000 claims description 9
- 239000000126 substance Substances 0.000 claims description 9
- 229910052796 boron Inorganic materials 0.000 claims description 7
- 229910052802 copper Inorganic materials 0.000 claims description 7
- 229910052748 manganese Inorganic materials 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 7
- 229910052710 silicon Inorganic materials 0.000 claims description 7
- 239000013078 crystal Substances 0.000 claims description 6
- 229910052749 magnesium Inorganic materials 0.000 claims description 6
- 229910052719 titanium Inorganic materials 0.000 claims description 6
- 229910052727 yttrium Inorganic materials 0.000 claims description 6
- 229910052708 sodium Inorganic materials 0.000 claims description 5
- 229910052717 sulfur Inorganic materials 0.000 claims description 5
- 229910052720 vanadium Inorganic materials 0.000 claims description 5
- 229910052804 chromium Inorganic materials 0.000 claims description 4
- 230000001590 oxidative effect Effects 0.000 claims description 4
- 229910052739 hydrogen Inorganic materials 0.000 claims description 3
- 230000014759 maintenance of location Effects 0.000 claims description 3
- 229910052698 phosphorus Inorganic materials 0.000 claims description 3
- 229910052700 potassium Inorganic materials 0.000 claims description 3
- 150000001450 anions Chemical class 0.000 claims description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 2
- 229910052750 molybdenum Inorganic materials 0.000 claims description 2
- 229910052759 nickel Inorganic materials 0.000 claims description 2
- 239000012071 phase Substances 0.000 description 70
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 45
- 239000000843 powder Substances 0.000 description 30
- 239000012530 fluid Substances 0.000 description 22
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 12
- 239000007787 solid Substances 0.000 description 12
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 11
- 229910052799 carbon Inorganic materials 0.000 description 11
- 150000001875 compounds Chemical class 0.000 description 11
- 229910001416 lithium ion Inorganic materials 0.000 description 11
- 239000007789 gas Substances 0.000 description 10
- 239000011734 sodium Substances 0.000 description 10
- 238000007664 blowing Methods 0.000 description 9
- 239000012535 impurity Substances 0.000 description 9
- 239000011572 manganese Substances 0.000 description 9
- 230000007935 neutral effect Effects 0.000 description 9
- 229910010707 LiFePO 4 Inorganic materials 0.000 description 8
- 239000010949 copper Substances 0.000 description 8
- 238000007711 solidification Methods 0.000 description 7
- 230000008023 solidification Effects 0.000 description 7
- 238000002441 X-ray diffraction Methods 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 6
- 238000005266 casting Methods 0.000 description 6
- 239000010955 niobium Substances 0.000 description 6
- 239000010936 titanium Substances 0.000 description 6
- 229910012425 Li3Fe2 (PO4)3 Inorganic materials 0.000 description 5
- 229910052782 aluminium Inorganic materials 0.000 description 5
- 239000007833 carbon precursor Substances 0.000 description 5
- 239000011651 chromium Substances 0.000 description 5
- 230000006698 induction Effects 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 4
- 239000000460 chlorine Substances 0.000 description 4
- 238000002425 crystallisation Methods 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- 239000006185 dispersion Substances 0.000 description 4
- 238000009826 distribution Methods 0.000 description 4
- 239000011777 magnesium Substances 0.000 description 4
- 238000010309 melting process Methods 0.000 description 4
- 229910018119 Li 3 PO 4 Inorganic materials 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- 239000007772 electrode material Substances 0.000 description 3
- 229910052731 fluorine Inorganic materials 0.000 description 3
- 239000002241 glass-ceramic Substances 0.000 description 3
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 2
- 229910001018 Cast iron Inorganic materials 0.000 description 2
- 229910020599 Co 3 O 4 Inorganic materials 0.000 description 2
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 229910018068 Li 2 O Inorganic materials 0.000 description 2
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 2
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 2
- 229910015621 MoO Inorganic materials 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 2
- 229910004298 SiO 2 Inorganic materials 0.000 description 2
- 229910010413 TiO 2 Inorganic materials 0.000 description 2
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000011737 fluorine Substances 0.000 description 2
- VASIZKWUTCETSD-UHFFFAOYSA-N manganese(II) oxide Inorganic materials [Mn]=O VASIZKWUTCETSD-UHFFFAOYSA-N 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 230000003472 neutralizing effect Effects 0.000 description 2
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 235000021317 phosphate Nutrition 0.000 description 2
- 239000005365 phosphate glass Substances 0.000 description 2
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 2
- 229920001223 polyethylene glycol Polymers 0.000 description 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M potassium hydroxide Inorganic materials [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000000197 pyrolysis Methods 0.000 description 2
- 238000007873 sieving Methods 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 238000005245 sintering Methods 0.000 description 2
- 239000007790 solid phase Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 229910017119 AlPO Inorganic materials 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical class N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- FGUUSXIOTUKUDN-IBGZPJMESA-N C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 Chemical compound C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 FGUUSXIOTUKUDN-IBGZPJMESA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 229920008712 Copo Polymers 0.000 description 1
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910003761 Li1.08Fe0.93PO4 Inorganic materials 0.000 description 1
- 229910011281 LiCoPO 4 Inorganic materials 0.000 description 1
- 229910011861 LiFe0.33Mn0.67PO4 Inorganic materials 0.000 description 1
- 229910052493 LiFePO4 Inorganic materials 0.000 description 1
- 229910015944 LiMn0.8Fe0.2PO4 Inorganic materials 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 229910052769 Ytterbium Inorganic materials 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 229910052787 antimony Inorganic materials 0.000 description 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 229910052797 bismuth Inorganic materials 0.000 description 1
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 1
- 230000005587 bubbling Effects 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000002447 crystallographic data Methods 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 150000002222 fluorine compounds Chemical class 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 229910052733 gallium Inorganic materials 0.000 description 1
- 229910052732 germanium Inorganic materials 0.000 description 1
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000011872 intimate mixture Substances 0.000 description 1
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 description 1
- 229910052808 lithium carbonate Inorganic materials 0.000 description 1
- 150000001247 metal acetylides Chemical class 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 150000004767 nitrides Chemical class 0.000 description 1
- 239000010450 olivine Substances 0.000 description 1
- 229910052609 olivine Inorganic materials 0.000 description 1
- 229920000620 organic polymer Polymers 0.000 description 1
- 150000003891 oxalate salts Chemical class 0.000 description 1
- -1 oxynitrides Chemical class 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 229910052712 strontium Inorganic materials 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- 238000004804 winding Methods 0.000 description 1
- 238000004846 x-ray emission Methods 0.000 description 1
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C10/00—Devitrified glass ceramics, i.e. glass ceramics having a crystalline phase dispersed in a glassy phase and constituting at least 50% by weight of the total composition
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Electrochemistry (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Dispersion Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Battery Electrode And Active Subsutance (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1156634A FR2978137A1 (fr) | 2011-07-21 | 2011-07-21 | Produit fondu a base de lithium |
| FR1156634 | 2011-07-21 | ||
| PCT/IB2012/053634 WO2013011452A1 (fr) | 2011-07-21 | 2012-07-16 | Procédé de fabrication d ' un produit fondu |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2014524883A JP2014524883A (ja) | 2014-09-25 |
| JP2014524883A5 JP2014524883A5 (enExample) | 2015-09-03 |
| JP6049713B2 true JP6049713B2 (ja) | 2016-12-21 |
Family
ID=46832532
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014520763A Expired - Fee Related JP6049713B2 (ja) | 2011-07-21 | 2012-07-16 | 溶融製品の製造法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US9620778B2 (enExample) |
| EP (1) | EP2734481A1 (enExample) |
| JP (1) | JP6049713B2 (enExample) |
| KR (1) | KR20140046024A (enExample) |
| CN (1) | CN103813992B (enExample) |
| FR (1) | FR2978137A1 (enExample) |
| WO (1) | WO2013011452A1 (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014191931A2 (fr) | 2013-05-31 | 2014-12-04 | Saint-Gobain Centre De Recherches Et D'etudes Europeen | Produit de phosphore, et de fer et/ou de manganese |
| FR3006306A1 (fr) * | 2013-05-31 | 2014-12-05 | Saint Gobain Ct Recherches | Produit de phosphore, et de fer et/ou de manganese |
| FR3006305A1 (fr) * | 2013-05-31 | 2014-12-05 | Saint Gobain Ct Recherches | Produit de phosphore, et de fer et/ou de manganese |
| CN103794787B (zh) * | 2014-02-21 | 2016-02-17 | 北京亿派通科技有限公司 | 一种高能效锂离子电池正极复合材料的制备方法 |
| JP7164178B2 (ja) * | 2018-12-27 | 2022-11-01 | 株式会社オキサイド | リチウム金属リン酸塩、リチウムイオン二次電池の正極材料、リチウムイオン二次電池 |
| CN111554922B (zh) * | 2020-04-14 | 2022-04-01 | 合肥国轩电池材料有限公司 | 一种倍率型磷酸铁锂的制备方法 |
| CN111675487B (zh) * | 2020-05-26 | 2022-11-04 | 上海大学 | 利用自然原料制备矿渣微晶玻璃的方法及其所制备的矿渣微晶玻璃 |
| CN112851347A (zh) * | 2021-03-09 | 2021-05-28 | 陕西师范大学 | 一种低温烧结低损耗氟氧化物微波介质陶瓷及其制备方法 |
| CN114230173B (zh) * | 2021-12-23 | 2024-02-06 | 亚细亚建筑材料股份有限公司 | 一种降低玻璃熔融温度的固体粉末材料及其制备方法 |
Family Cites Families (34)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1208577A (fr) | 1958-07-07 | 1960-02-24 | Electro Refractaire | Perfectionnements à la fabrication de produits réfractaires électrofondus contenant des oxydes minéraux |
| US3993119A (en) | 1974-11-08 | 1976-11-23 | Norton Company | Progressively or continuously cycled mold for forming and discharging a fine crystalline material |
| US6514640B1 (en) * | 1996-04-23 | 2003-02-04 | Board Of Regents, The University Of Texas System | Cathode materials for secondary (rechargeable) lithium batteries |
| US5674645A (en) * | 1996-09-06 | 1997-10-07 | Bell Communications Research, Inc. | Lithium manganese oxy-fluorides for li-ion rechargeable battery electrodes |
| US6153333A (en) * | 1999-03-23 | 2000-11-28 | Valence Technology, Inc. | Lithium-containing phosphate active materials |
| US7001690B2 (en) * | 2000-01-18 | 2006-02-21 | Valence Technology, Inc. | Lithium-based active materials and preparation thereof |
| US6387568B1 (en) * | 2000-04-27 | 2002-05-14 | Valence Technology, Inc. | Lithium metal fluorophosphate materials and preparation thereof |
| CA2320661A1 (fr) | 2000-09-26 | 2002-03-26 | Hydro-Quebec | Nouveau procede de synthese de materiaux limpo4 a structure olivine |
| US6908710B2 (en) * | 2001-10-09 | 2005-06-21 | Valence Technology, Inc. | Lithiated molybdenum oxide active materials |
| FR2831715B1 (fr) * | 2001-10-25 | 2004-03-19 | Centre Nat Rech Scient | Oxyde de lithium et de vanadium, son utilisation comme matiere active d'electrode |
| DE10336913C9 (de) * | 2003-08-07 | 2019-02-21 | Ivoclar Vivadent Ag | Verwendung eines Lithiumsilicatmaterials |
| CA2906604A1 (en) | 2003-12-23 | 2005-07-07 | Laurent Gauthier | Process for preparing electroactive insertion compounds and electrode materials obtained therefrom |
| JP2006155941A (ja) * | 2004-11-25 | 2006-06-15 | Kyushu Univ | 電極活物質の製造方法 |
| JP5034042B2 (ja) * | 2006-08-15 | 2012-09-26 | 国立大学法人長岡技術科学大学 | リチウム二次電池正極材料及びその製造方法 |
| US8480987B2 (en) * | 2007-04-20 | 2013-07-09 | Sung Yoon Chung | Method of preparing nanoparticles of lithium transition metal phosphates, lithium transition metal phosphates, and method of preparing the same |
| US20090155689A1 (en) * | 2007-12-14 | 2009-06-18 | Karim Zaghib | Lithium iron phosphate cathode materials with enhanced energy density and power performance |
| TW201010944A (en) * | 2008-04-17 | 2010-03-16 | Basf Se | Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials |
| US20110133118A1 (en) * | 2008-05-16 | 2011-06-09 | Tsuyoshi Honma | Crystallized glass and method for producing the same |
| KR100939647B1 (ko) * | 2009-01-22 | 2010-02-03 | 한화석유화학 주식회사 | 전극 활물질인 음이온 부족형 비화학양론 리튬 전이금속 다중산 화합물, 그 제조 방법 및 그를 이용한 전기화학 소자 |
| CN102378738A (zh) | 2009-04-03 | 2012-03-14 | 旭硝子株式会社 | 磷酸铁锂颗粒的制造方法及二次电池的制造方法 |
| JP2011001242A (ja) | 2009-06-22 | 2011-01-06 | Asahi Glass Co Ltd | リン酸鉄リチウム粒子の製造方法とリン酸鉄リチウム粒子 |
| JP2011014373A (ja) * | 2009-07-02 | 2011-01-20 | Hitachi Powdered Metals Co Ltd | 導電性材料及びこれを用いたLiイオン二次電池用正極材料 |
| JP2011086584A (ja) * | 2009-10-19 | 2011-04-28 | Nippon Electric Glass Co Ltd | リチウムイオン二次電池用正極材料 |
| US20120267566A1 (en) * | 2009-10-19 | 2012-10-25 | Tomohiro Nagakane | Lithium ion secondary battery positive electrode material |
| CN102666374A (zh) * | 2009-11-24 | 2012-09-12 | 旭硝子株式会社 | 磷酸化合物的制造方法及二次电池的制造方法 |
| DE102010032206A1 (de) * | 2010-07-26 | 2012-04-05 | Süd-Chemie AG | Gasphasenbeschichtetes Lithium-Übergangsmetallphosphat und Verfahren zu dessen Herstellung |
| FR2969595A1 (fr) * | 2010-12-23 | 2012-06-29 | Saint Gobain Ct Recherches | Procede de fabrication d'un produit lmo. |
| WO2012133581A1 (ja) * | 2011-03-28 | 2012-10-04 | 旭硝子株式会社 | 二次電池用正極活物質、二次電池用正極、および二次電池の製造方法 |
| WO2012133584A1 (ja) * | 2011-03-28 | 2012-10-04 | 旭硝子株式会社 | 二次電池用正極活物質、二次電池用正極、および二次電池の製造方法 |
| JP5451681B2 (ja) * | 2011-05-09 | 2014-03-26 | シャープ株式会社 | 正極活物質、正極及び非水系二次電池 |
| US8765303B2 (en) * | 2012-04-02 | 2014-07-01 | Nanotek Instruments, Inc. | Lithium-ion cell having a high energy density and high power density |
| KR101973052B1 (ko) * | 2012-08-10 | 2019-04-26 | 삼성에스디아이 주식회사 | 리튬 금속인산화물의 제조방법 |
| EP2874227B1 (en) * | 2012-11-21 | 2017-09-06 | LG Chem, Ltd. | Lithium secondary battery |
| WO2015140915A1 (ja) * | 2014-03-18 | 2015-09-24 | 株式会社 東芝 | 電池用活物質、非水電解質電池及び電池パック |
-
2011
- 2011-07-21 FR FR1156634A patent/FR2978137A1/fr not_active Withdrawn
-
2012
- 2012-07-16 WO PCT/IB2012/053634 patent/WO2013011452A1/fr not_active Ceased
- 2012-07-16 US US14/233,954 patent/US9620778B2/en active Active
- 2012-07-16 CN CN201280045901.1A patent/CN103813992B/zh not_active Expired - Fee Related
- 2012-07-16 KR KR1020147003573A patent/KR20140046024A/ko not_active Ceased
- 2012-07-16 EP EP12758618.8A patent/EP2734481A1/fr not_active Withdrawn
- 2012-07-16 JP JP2014520763A patent/JP6049713B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JP2014524883A (ja) | 2014-09-25 |
| US9620778B2 (en) | 2017-04-11 |
| CN103813992A (zh) | 2014-05-21 |
| EP2734481A1 (fr) | 2014-05-28 |
| FR2978137A1 (fr) | 2013-01-25 |
| WO2013011452A1 (fr) | 2013-01-24 |
| CN103813992B (zh) | 2018-02-06 |
| KR20140046024A (ko) | 2014-04-17 |
| US20140158933A1 (en) | 2014-06-12 |
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